Scale-Up Design & Safety Analysis Of Palm Kernel Oil Extraction Using Supercritical Carbon Dioxide System

In recent years, supercritical carbon dioxide technology has been widely used as an alternative extraction method. However, improper plan in upscaling can lead to inefficient process and hazards. Therefore, the objective of the study is to focus on the layout of using the scale-up criteria for the p...

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Main Author: Sofian, Asmah Mohamed
Format: Thesis
Language:English
Published: Universiti Sains Malaysia 2020
Subjects:
Online Access:http://eprints.usm.my/49613/
http://eprints.usm.my/49613/1/SCALE-UP%20DESIGN%20_%20SAFETY%20ANALYSIS%20OF%20PALM%20KERNEL%20OIL%20EXTRACTION%20USING%20SUPERCRITICAL%20CARBON%20DIOXIDE%20SYSTEM%20cut.pdf
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author Sofian, Asmah Mohamed
author_facet Sofian, Asmah Mohamed
author_sort Sofian, Asmah Mohamed
building USM Institutional Repository
collection Online Access
description In recent years, supercritical carbon dioxide technology has been widely used as an alternative extraction method. However, improper plan in upscaling can lead to inefficient process and hazards. Therefore, the objective of the study is to focus on the layout of using the scale-up criteria for the principle of similarity in upscaling and the safety analysis as a preliminary assessment for a large scale that would highly be beneficial for future works. Four dimensionless groups were selected and calculated as the suitable scale-up criteria by relevancy evaluation and expert system, as constant mfmB gave the highest strength, while dpdint had the lowest with 7.488 and 3.98, respectively. Constant combination of mfmB & Re was the best criteria for 0.57 L – 50 L scale during the scale-up simulation due to the highest total fast extraction rate and kf, while for 40 ML – 50 L scale, the lowest was obtained from constant dpdint and constant Re. The safety assessment of the system was evaluated by fault tree analysis where 25 minimal cut sets led to overpressure mainly caused by leakage of the piping and connector. The calculated top-level failure probabilities for probabilities analysis and Monte Carlo simulation were 1.241485×10−1 and 1.237203×10−1 respectively.
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institution Universiti Sains Malaysia
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language English
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spelling usm-496132021-09-09T07:10:52Z http://eprints.usm.my/49613/ Scale-Up Design & Safety Analysis Of Palm Kernel Oil Extraction Using Supercritical Carbon Dioxide System Sofian, Asmah Mohamed T11.95-12.5 Industrial directories In recent years, supercritical carbon dioxide technology has been widely used as an alternative extraction method. However, improper plan in upscaling can lead to inefficient process and hazards. Therefore, the objective of the study is to focus on the layout of using the scale-up criteria for the principle of similarity in upscaling and the safety analysis as a preliminary assessment for a large scale that would highly be beneficial for future works. Four dimensionless groups were selected and calculated as the suitable scale-up criteria by relevancy evaluation and expert system, as constant mfmB gave the highest strength, while dpdint had the lowest with 7.488 and 3.98, respectively. Constant combination of mfmB & Re was the best criteria for 0.57 L – 50 L scale during the scale-up simulation due to the highest total fast extraction rate and kf, while for 40 ML – 50 L scale, the lowest was obtained from constant dpdint and constant Re. The safety assessment of the system was evaluated by fault tree analysis where 25 minimal cut sets led to overpressure mainly caused by leakage of the piping and connector. The calculated top-level failure probabilities for probabilities analysis and Monte Carlo simulation were 1.241485×10−1 and 1.237203×10−1 respectively. Universiti Sains Malaysia 2020-08 Thesis NonPeerReviewed application/pdf en http://eprints.usm.my/49613/1/SCALE-UP%20DESIGN%20_%20SAFETY%20ANALYSIS%20OF%20PALM%20KERNEL%20OIL%20EXTRACTION%20USING%20SUPERCRITICAL%20CARBON%20DIOXIDE%20SYSTEM%20cut.pdf Sofian, Asmah Mohamed (2020) Scale-Up Design & Safety Analysis Of Palm Kernel Oil Extraction Using Supercritical Carbon Dioxide System. Masters thesis, UNSPECIFIED.
spellingShingle T11.95-12.5 Industrial directories
Sofian, Asmah Mohamed
Scale-Up Design & Safety Analysis Of Palm Kernel Oil Extraction Using Supercritical Carbon Dioxide System
title Scale-Up Design & Safety Analysis Of Palm Kernel Oil Extraction Using Supercritical Carbon Dioxide System
title_full Scale-Up Design & Safety Analysis Of Palm Kernel Oil Extraction Using Supercritical Carbon Dioxide System
title_fullStr Scale-Up Design & Safety Analysis Of Palm Kernel Oil Extraction Using Supercritical Carbon Dioxide System
title_full_unstemmed Scale-Up Design & Safety Analysis Of Palm Kernel Oil Extraction Using Supercritical Carbon Dioxide System
title_short Scale-Up Design & Safety Analysis Of Palm Kernel Oil Extraction Using Supercritical Carbon Dioxide System
title_sort scale-up design & safety analysis of palm kernel oil extraction using supercritical carbon dioxide system
topic T11.95-12.5 Industrial directories
url http://eprints.usm.my/49613/
http://eprints.usm.my/49613/1/SCALE-UP%20DESIGN%20_%20SAFETY%20ANALYSIS%20OF%20PALM%20KERNEL%20OIL%20EXTRACTION%20USING%20SUPERCRITICAL%20CARBON%20DIOXIDE%20SYSTEM%20cut.pdf