Metabolite profiles of red and yellow watermelon (Citrullus lanatus) cultivars by 1H-NMR metabolomics approach

Watermelon, a widely commercialized fruit, is famous for its thirst-quenching property. The broad range of cultivars, which give rise to distinct color and taste, can be attributed to the differences in their chemical profile, especially that of the carotenoids and volatile compounds. In order to un...

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Main Authors: Sulaiman, Fadzil, Ahmad Azam, Amalina, Ahamad Bustamam, Muhammad Safwan, Fakurazi, Sharida, Abas, Faridah, Yee, Xuan Lee, Ismail, Atira Adriana, Mohd Faudzi, Siti Munirah, Ismail, Intan Safinar
Format: Article
Language:English
Published: Multidisciplinary Digital Publishing Institute 2020
Online Access:http://psasir.upm.edu.my/id/eprint/86729/
http://psasir.upm.edu.my/id/eprint/86729/1/Metabolite%20profiles%20of%20red%20and%20yellow%20watermelon.pdf
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author Sulaiman, Fadzil
Ahmad Azam, Amalina
Ahamad Bustamam, Muhammad Safwan
Fakurazi, Sharida
Abas, Faridah
Yee, Xuan Lee
Ismail, Atira Adriana
Mohd Faudzi, Siti Munirah
Ismail, Intan Safinar
author_facet Sulaiman, Fadzil
Ahmad Azam, Amalina
Ahamad Bustamam, Muhammad Safwan
Fakurazi, Sharida
Abas, Faridah
Yee, Xuan Lee
Ismail, Atira Adriana
Mohd Faudzi, Siti Munirah
Ismail, Intan Safinar
author_sort Sulaiman, Fadzil
building UPM Institutional Repository
collection Online Access
description Watermelon, a widely commercialized fruit, is famous for its thirst-quenching property. The broad range of cultivars, which give rise to distinct color and taste, can be attributed to the differences in their chemical profile, especially that of the carotenoids and volatile compounds. In order to understand this distribution properly, water extracts of red and yellow watermelon pulps with predominantly polar metabolites were subjected to proton nuclear magnetic resonance (1H-NMR) analysis. Deuterium oxide (D2O) and deuterated chloroform (CDCl3) solvents were used to capture both polar and non-polar metabolites from the same sample. Thirty-six metabolites, of which six are carotenoids, were identified from the extracts. The clustering of the compounds was determined using unsupervised principal component analysis (PCA) and further grouping was achieved using supervised orthogonal partial least squares discriminant analysis (OPLS-DA). The presence of lycopene, β-carotene, lutein, and prolycopene in the red watermelon plays an important role in its differentiation from the yellow cultivar. A marked difference in metabolite distribution was observed between the NMR solvents used as evidenced from the PCA model. OPLS-DA and relative quantification of the metabolites, on the other hand, helped in uncovering the discriminating metabolites of the red and yellow watermelon cultivars from the same solvent system.
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spelling upm-867292021-11-10T07:50:45Z http://psasir.upm.edu.my/id/eprint/86729/ Metabolite profiles of red and yellow watermelon (Citrullus lanatus) cultivars by 1H-NMR metabolomics approach Sulaiman, Fadzil Ahmad Azam, Amalina Ahamad Bustamam, Muhammad Safwan Fakurazi, Sharida Abas, Faridah Yee, Xuan Lee Ismail, Atira Adriana Mohd Faudzi, Siti Munirah Ismail, Intan Safinar Watermelon, a widely commercialized fruit, is famous for its thirst-quenching property. The broad range of cultivars, which give rise to distinct color and taste, can be attributed to the differences in their chemical profile, especially that of the carotenoids and volatile compounds. In order to understand this distribution properly, water extracts of red and yellow watermelon pulps with predominantly polar metabolites were subjected to proton nuclear magnetic resonance (1H-NMR) analysis. Deuterium oxide (D2O) and deuterated chloroform (CDCl3) solvents were used to capture both polar and non-polar metabolites from the same sample. Thirty-six metabolites, of which six are carotenoids, were identified from the extracts. The clustering of the compounds was determined using unsupervised principal component analysis (PCA) and further grouping was achieved using supervised orthogonal partial least squares discriminant analysis (OPLS-DA). The presence of lycopene, β-carotene, lutein, and prolycopene in the red watermelon plays an important role in its differentiation from the yellow cultivar. A marked difference in metabolite distribution was observed between the NMR solvents used as evidenced from the PCA model. OPLS-DA and relative quantification of the metabolites, on the other hand, helped in uncovering the discriminating metabolites of the red and yellow watermelon cultivars from the same solvent system. Multidisciplinary Digital Publishing Institute 2020-07-15 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/86729/1/Metabolite%20profiles%20of%20red%20and%20yellow%20watermelon.pdf Sulaiman, Fadzil and Ahmad Azam, Amalina and Ahamad Bustamam, Muhammad Safwan and Fakurazi, Sharida and Abas, Faridah and Yee, Xuan Lee and Ismail, Atira Adriana and Mohd Faudzi, Siti Munirah and Ismail, Intan Safinar (2020) Metabolite profiles of red and yellow watermelon (Citrullus lanatus) cultivars by 1H-NMR metabolomics approach. Molecules, 25 (14). pp. 1-13. ISSN 1420-3049 https://www.mdpi.com/1420-3049/25/14/3235 10.3390/molecules25143235
spellingShingle Sulaiman, Fadzil
Ahmad Azam, Amalina
Ahamad Bustamam, Muhammad Safwan
Fakurazi, Sharida
Abas, Faridah
Yee, Xuan Lee
Ismail, Atira Adriana
Mohd Faudzi, Siti Munirah
Ismail, Intan Safinar
Metabolite profiles of red and yellow watermelon (Citrullus lanatus) cultivars by 1H-NMR metabolomics approach
title Metabolite profiles of red and yellow watermelon (Citrullus lanatus) cultivars by 1H-NMR metabolomics approach
title_full Metabolite profiles of red and yellow watermelon (Citrullus lanatus) cultivars by 1H-NMR metabolomics approach
title_fullStr Metabolite profiles of red and yellow watermelon (Citrullus lanatus) cultivars by 1H-NMR metabolomics approach
title_full_unstemmed Metabolite profiles of red and yellow watermelon (Citrullus lanatus) cultivars by 1H-NMR metabolomics approach
title_short Metabolite profiles of red and yellow watermelon (Citrullus lanatus) cultivars by 1H-NMR metabolomics approach
title_sort metabolite profiles of red and yellow watermelon (citrullus lanatus) cultivars by 1h-nmr metabolomics approach
url http://psasir.upm.edu.my/id/eprint/86729/
http://psasir.upm.edu.my/id/eprint/86729/
http://psasir.upm.edu.my/id/eprint/86729/
http://psasir.upm.edu.my/id/eprint/86729/1/Metabolite%20profiles%20of%20red%20and%20yellow%20watermelon.pdf