Synthesis of palm oil-based fatty methylhydrazide
Fatty methylydrazides (FMHs) have been successfully synthesized from palm oil. Glycerol was produced as a by-product. The synthesis was carried out by reflux palm oil with methylhydrazine in hexane. FMHs have been characterized using elemental analysis, Fourier transform infrared spectroscopy and 1H...
| Main Authors: | , , , , , , |
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| Format: | Article |
| Language: | English |
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Springer Netherlands
2013
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| Online Access: | http://psasir.upm.edu.my/id/eprint/30010/ http://psasir.upm.edu.my/id/eprint/30010/1/Synthesis%20of%20palm%20oil.pdf |
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| author | Al-Mulla, Emad A. Jaffar Ibrahim, Nor Azowa Al-Karkhi, Isam Hussain T. Shameli, Kamyar Zidan, Mohammed Ahmad, Mansor Wan Yunus, Wan Md. Zin |
| author_facet | Al-Mulla, Emad A. Jaffar Ibrahim, Nor Azowa Al-Karkhi, Isam Hussain T. Shameli, Kamyar Zidan, Mohammed Ahmad, Mansor Wan Yunus, Wan Md. Zin |
| author_sort | Al-Mulla, Emad A. Jaffar |
| building | UPM Institutional Repository |
| collection | Online Access |
| description | Fatty methylydrazides (FMHs) have been successfully synthesized from palm oil. Glycerol was produced as a by-product. The synthesis was carried out by reflux palm oil with methylhydrazine in hexane. FMHs have been characterized
using elemental analysis, Fourier transform infrared spectroscopy and 1H nuclear magnetic resonance technique. The results showed that a 6:1 molar ratio of palm oil
to methylhydrazine, a round 78 % maximum conversion of palm oil into FMHs and a 10 h reaction time are the optimum reaction conditions. |
| first_indexed | 2025-11-15T09:04:37Z |
| format | Article |
| id | upm-30010 |
| institution | Universiti Putra Malaysia |
| institution_category | Local University |
| language | English |
| last_indexed | 2025-11-15T09:04:37Z |
| publishDate | 2013 |
| publisher | Springer Netherlands |
| recordtype | eprints |
| repository_type | Digital Repository |
| spelling | upm-300102016-02-12T07:21:49Z http://psasir.upm.edu.my/id/eprint/30010/ Synthesis of palm oil-based fatty methylhydrazide Al-Mulla, Emad A. Jaffar Ibrahim, Nor Azowa Al-Karkhi, Isam Hussain T. Shameli, Kamyar Zidan, Mohammed Ahmad, Mansor Wan Yunus, Wan Md. Zin Fatty methylydrazides (FMHs) have been successfully synthesized from palm oil. Glycerol was produced as a by-product. The synthesis was carried out by reflux palm oil with methylhydrazine in hexane. FMHs have been characterized using elemental analysis, Fourier transform infrared spectroscopy and 1H nuclear magnetic resonance technique. The results showed that a 6:1 molar ratio of palm oil to methylhydrazine, a round 78 % maximum conversion of palm oil into FMHs and a 10 h reaction time are the optimum reaction conditions. Springer Netherlands 2013-05-05 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/30010/1/Synthesis%20of%20palm%20oil.pdf Al-Mulla, Emad A. Jaffar and Ibrahim, Nor Azowa and Al-Karkhi, Isam Hussain T. and Shameli, Kamyar and Zidan, Mohammed and Ahmad, Mansor and Wan Yunus, Wan Md. Zin (2013) Synthesis of palm oil-based fatty methylhydrazide. Research on Chemical Intermediates, 39 (5). pp. 2133-2139. ISSN 0922-6168; ESSN: 1568-5675 http://dx.doi.org/10.1007/s11164-012-0745-0 10.1007/s11164-012-0745-0 |
| spellingShingle | Al-Mulla, Emad A. Jaffar Ibrahim, Nor Azowa Al-Karkhi, Isam Hussain T. Shameli, Kamyar Zidan, Mohammed Ahmad, Mansor Wan Yunus, Wan Md. Zin Synthesis of palm oil-based fatty methylhydrazide |
| title | Synthesis of palm oil-based fatty methylhydrazide |
| title_full | Synthesis of palm oil-based fatty methylhydrazide |
| title_fullStr | Synthesis of palm oil-based fatty methylhydrazide |
| title_full_unstemmed | Synthesis of palm oil-based fatty methylhydrazide |
| title_short | Synthesis of palm oil-based fatty methylhydrazide |
| title_sort | synthesis of palm oil-based fatty methylhydrazide |
| url | http://psasir.upm.edu.my/id/eprint/30010/ http://psasir.upm.edu.my/id/eprint/30010/ http://psasir.upm.edu.my/id/eprint/30010/ http://psasir.upm.edu.my/id/eprint/30010/1/Synthesis%20of%20palm%20oil.pdf |