Synthesis, characterization and optimum reaction conditions of fatty hydrazide from triacylglycerides
Fatty Hydrazide (FH) has been synthesized via reaction of palm olein with hydrazine hydrate by reflux and characterized using spectroscopic methods and CHN analyzer. Optimum reaction conditions were studied in order to optimize the reaction time and hydrazine hydrate/palm olein ratio. When the hydra...
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| Format: | Article |
| Language: | English English |
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Medwell Publishing
2008
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| Online Access: | http://psasir.upm.edu.my/id/eprint/16955/ http://psasir.upm.edu.my/id/eprint/16955/1/Synthesis%2C%20characterization%20and%20potimum%20reaction.pdf |
| _version_ | 1848843105849049088 |
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| author | Al-Mulla, Emad A. Jaffar Wan Yunus, Wan Md. Zin Ibrahim, Nor Azowa Ab. Rahman, Mohamad Zaki |
| author_facet | Al-Mulla, Emad A. Jaffar Wan Yunus, Wan Md. Zin Ibrahim, Nor Azowa Ab. Rahman, Mohamad Zaki |
| author_sort | Al-Mulla, Emad A. Jaffar |
| building | UPM Institutional Repository |
| collection | Online Access |
| description | Fatty Hydrazide (FH) has been synthesized via reaction of palm olein with hydrazine hydrate by reflux and characterized using spectroscopic methods and CHN analyzer. Optimum reaction conditions were studied in order to optimize the reaction time and hydrazine hydrate/palm olein ratio. When the hydrazinolysis reaction was carried out 7:1 molar ratio of hydrazine hydrate to palm olein, the conversion of palm olein was 82% and the maximum of conversion to FH was 84% when the reaction time was 12 h. FH was also prepared from palm stearin and corn oil and then, the conversion percentages of these oils into their fatty hydrazides were investigated to compare with palm olein. |
| first_indexed | 2025-11-15T08:09:45Z |
| format | Article |
| id | upm-16955 |
| institution | Universiti Putra Malaysia |
| institution_category | Local University |
| language | English English |
| last_indexed | 2025-11-15T08:09:45Z |
| publishDate | 2008 |
| publisher | Medwell Publishing |
| recordtype | eprints |
| repository_type | Digital Repository |
| spelling | upm-169552015-12-04T09:04:30Z http://psasir.upm.edu.my/id/eprint/16955/ Synthesis, characterization and optimum reaction conditions of fatty hydrazide from triacylglycerides Al-Mulla, Emad A. Jaffar Wan Yunus, Wan Md. Zin Ibrahim, Nor Azowa Ab. Rahman, Mohamad Zaki Fatty Hydrazide (FH) has been synthesized via reaction of palm olein with hydrazine hydrate by reflux and characterized using spectroscopic methods and CHN analyzer. Optimum reaction conditions were studied in order to optimize the reaction time and hydrazine hydrate/palm olein ratio. When the hydrazinolysis reaction was carried out 7:1 molar ratio of hydrazine hydrate to palm olein, the conversion of palm olein was 82% and the maximum of conversion to FH was 84% when the reaction time was 12 h. FH was also prepared from palm stearin and corn oil and then, the conversion percentages of these oils into their fatty hydrazides were investigated to compare with palm olein. Medwell Publishing 2008 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/16955/1/Synthesis%2C%20characterization%20and%20potimum%20reaction.pdf Al-Mulla, Emad A. Jaffar and Wan Yunus, Wan Md. Zin and Ibrahim, Nor Azowa and Ab. Rahman, Mohamad Zaki (2008) Synthesis, characterization and optimum reaction conditions of fatty hydrazide from triacylglycerides. Research Journal of Applied Sciences, 8 (3). pp. 545-549. ISSN 1815-932X Hydrazines - Synthesis Oils and fats - Analysis Stearin - Analysis English |
| spellingShingle | Hydrazines - Synthesis Oils and fats - Analysis Stearin - Analysis Al-Mulla, Emad A. Jaffar Wan Yunus, Wan Md. Zin Ibrahim, Nor Azowa Ab. Rahman, Mohamad Zaki Synthesis, characterization and optimum reaction conditions of fatty hydrazide from triacylglycerides |
| title | Synthesis, characterization and optimum reaction conditions of fatty hydrazide from triacylglycerides |
| title_full | Synthesis, characterization and optimum reaction conditions of fatty hydrazide from triacylglycerides |
| title_fullStr | Synthesis, characterization and optimum reaction conditions of fatty hydrazide from triacylglycerides |
| title_full_unstemmed | Synthesis, characterization and optimum reaction conditions of fatty hydrazide from triacylglycerides |
| title_short | Synthesis, characterization and optimum reaction conditions of fatty hydrazide from triacylglycerides |
| title_sort | synthesis, characterization and optimum reaction conditions of fatty hydrazide from triacylglycerides |
| topic | Hydrazines - Synthesis Oils and fats - Analysis Stearin - Analysis |
| url | http://psasir.upm.edu.my/id/eprint/16955/ http://psasir.upm.edu.my/id/eprint/16955/1/Synthesis%2C%20characterization%20and%20potimum%20reaction.pdf |