Synergistic effects of intermolecular copigmentation and high-pressure processing on stabilizing mangosteen pericarp anthocyanins

The mangosteen pericarp contains unstable non-acylated ACNs, rendering it prone to degradation. Therefore, intermolecular copigmentation of semi-purified ACNs (SPA) with tartaric acid (SPA-TA), sinapic acid (SPA-SA), catechin (SPA-CE), and sucrose (SPA-SU) in 1:5 and 1:10 M ratios were used to incre...

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Main Authors: Ijod, Giroon, Mohamed Nawawi, Nur Izzati, Qoms, Mohammed S., Rashedi Ismail Fitry, Mohammad, Abd Rahim, Muhamad Hafiz, Charalampopoulos, Dimitris, Sulaiman, Rabiha, Mohd Adzahan, Noranizan, Mohamad Azman, Ezzat
Format: Article
Language:English
Published: Elsevier 2025
Online Access:http://psasir.upm.edu.my/id/eprint/117430/
http://psasir.upm.edu.my/id/eprint/117430/1/117430.pdf
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author Ijod, Giroon
Mohamed Nawawi, Nur Izzati
Qoms, Mohammed S.
Rashedi Ismail Fitry, Mohammad
Abd Rahim, Muhamad Hafiz
Charalampopoulos, Dimitris
Sulaiman, Rabiha
Mohd Adzahan, Noranizan
Mohamad Azman, Ezzat
author_facet Ijod, Giroon
Mohamed Nawawi, Nur Izzati
Qoms, Mohammed S.
Rashedi Ismail Fitry, Mohammad
Abd Rahim, Muhamad Hafiz
Charalampopoulos, Dimitris
Sulaiman, Rabiha
Mohd Adzahan, Noranizan
Mohamad Azman, Ezzat
author_sort Ijod, Giroon
building UPM Institutional Repository
collection Online Access
description The mangosteen pericarp contains unstable non-acylated ACNs, rendering it prone to degradation. Therefore, intermolecular copigmentation of semi-purified ACNs (SPA) with tartaric acid (SPA-TA), sinapic acid (SPA-SA), catechin (SPA-CE), and sucrose (SPA-SU) in 1:5 and 1:10 M ratios were used to increase their stability during storage for 77 days at 25 ± 1 °C in pH 3 buffer solution. The SPA-TA1:5 complex showed the significant highest stability of total monomeric ACN content (TMAC) with a half-life (t1/2) = 56.9 days, cyanidin-3-O-sophoroside (C3S) with t1/2 = 48.1 days and color retention (69.80 %) compare to SPA with TMAC (t1/2 = 37.4), C3S (t1/2 = 13.3) and color retention (57.2 %) after 49 days (p < 0.05). The thermal stability of SPA-TA1:5 at 60 °C improved after high-pressure processing (HPP) at 300 and 500 MPa for 10 min. Fourier-transform infrared spectroscopy (FT-IR) and molecular docking indicate copigmentation interactions, including hydrogen bonding and π-π interactions. This study demonstrates a sustainable method to stabilize non-acylated ACNs, offering a natural alternative to synthetic dyes for food and beverage applications.
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institution Universiti Putra Malaysia
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spelling upm-1174302025-05-22T02:27:44Z http://psasir.upm.edu.my/id/eprint/117430/ Synergistic effects of intermolecular copigmentation and high-pressure processing on stabilizing mangosteen pericarp anthocyanins Ijod, Giroon Mohamed Nawawi, Nur Izzati Qoms, Mohammed S. Rashedi Ismail Fitry, Mohammad Abd Rahim, Muhamad Hafiz Charalampopoulos, Dimitris Sulaiman, Rabiha Mohd Adzahan, Noranizan Mohamad Azman, Ezzat The mangosteen pericarp contains unstable non-acylated ACNs, rendering it prone to degradation. Therefore, intermolecular copigmentation of semi-purified ACNs (SPA) with tartaric acid (SPA-TA), sinapic acid (SPA-SA), catechin (SPA-CE), and sucrose (SPA-SU) in 1:5 and 1:10 M ratios were used to increase their stability during storage for 77 days at 25 ± 1 °C in pH 3 buffer solution. The SPA-TA1:5 complex showed the significant highest stability of total monomeric ACN content (TMAC) with a half-life (t1/2) = 56.9 days, cyanidin-3-O-sophoroside (C3S) with t1/2 = 48.1 days and color retention (69.80 %) compare to SPA with TMAC (t1/2 = 37.4), C3S (t1/2 = 13.3) and color retention (57.2 %) after 49 days (p < 0.05). The thermal stability of SPA-TA1:5 at 60 °C improved after high-pressure processing (HPP) at 300 and 500 MPa for 10 min. Fourier-transform infrared spectroscopy (FT-IR) and molecular docking indicate copigmentation interactions, including hydrogen bonding and π-π interactions. This study demonstrates a sustainable method to stabilize non-acylated ACNs, offering a natural alternative to synthetic dyes for food and beverage applications. Elsevier 2025 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/117430/1/117430.pdf Ijod, Giroon and Mohamed Nawawi, Nur Izzati and Qoms, Mohammed S. and Rashedi Ismail Fitry, Mohammad and Abd Rahim, Muhamad Hafiz and Charalampopoulos, Dimitris and Sulaiman, Rabiha and Mohd Adzahan, Noranizan and Mohamad Azman, Ezzat (2025) Synergistic effects of intermolecular copigmentation and high-pressure processing on stabilizing mangosteen pericarp anthocyanins. Food Chemistry, 480. art. no. 143888. pp. 1-13. ISSN 0308-8146; eISSN: 1873-7072 https://linkinghub.elsevier.com/retrieve/pii/S0308814625011392 10.1016/j.foodchem.2025.143888
spellingShingle Ijod, Giroon
Mohamed Nawawi, Nur Izzati
Qoms, Mohammed S.
Rashedi Ismail Fitry, Mohammad
Abd Rahim, Muhamad Hafiz
Charalampopoulos, Dimitris
Sulaiman, Rabiha
Mohd Adzahan, Noranizan
Mohamad Azman, Ezzat
Synergistic effects of intermolecular copigmentation and high-pressure processing on stabilizing mangosteen pericarp anthocyanins
title Synergistic effects of intermolecular copigmentation and high-pressure processing on stabilizing mangosteen pericarp anthocyanins
title_full Synergistic effects of intermolecular copigmentation and high-pressure processing on stabilizing mangosteen pericarp anthocyanins
title_fullStr Synergistic effects of intermolecular copigmentation and high-pressure processing on stabilizing mangosteen pericarp anthocyanins
title_full_unstemmed Synergistic effects of intermolecular copigmentation and high-pressure processing on stabilizing mangosteen pericarp anthocyanins
title_short Synergistic effects of intermolecular copigmentation and high-pressure processing on stabilizing mangosteen pericarp anthocyanins
title_sort synergistic effects of intermolecular copigmentation and high-pressure processing on stabilizing mangosteen pericarp anthocyanins
url http://psasir.upm.edu.my/id/eprint/117430/
http://psasir.upm.edu.my/id/eprint/117430/
http://psasir.upm.edu.my/id/eprint/117430/
http://psasir.upm.edu.my/id/eprint/117430/1/117430.pdf