1H CSA parameters by ultrafast MAS NMR: measurement and applications to structure refinement

1H CSA parameters by ultrafast MAS NMR: measurement and applications to structure refinement

A 1H anisotropic-isotropic chemical shift correlation experiment which employs symmetry-based recoupling sequences to reintroduce the chemical shift anisotropy in ν1 and ultrafast MAS to resolve 1H sites in ν2 is described. This experiment is used to measure 1H shift parameters for L-ascorbic acid,...

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Bibliographic Details
Main Authors: Miah, Habeeba K., Cresswell, Rosalie, Iuga, Dinu, Titman, Jeremy J.
Format: Article
Published: Elsevier 2017
Online Access:https://eprints.nottingham.ac.uk/40628/

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