1H CSA parameters by ultrafast MAS NMR: measurement and applications to structure refinement
A 1H anisotropic-isotropic chemical shift correlation experiment which employs symmetry-based recoupling sequences to reintroduce the chemical shift anisotropy in ν1 and ultrafast MAS to resolve 1H sites in ν2 is described. This experiment is used to measure 1H shift parameters for L-ascorbic acid,...
| Main Authors: | , , , |
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| Format: | Article |
| Published: |
Elsevier
2017
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| Online Access: | https://eprints.nottingham.ac.uk/40628/ |