Cuprous oxide/Titanium dioxide nanotube-array with coaxial heterogeneous structure synthesized by multiple-cycle chemical adsorption plus reduction method

We report the formation and characterization of Cuprous oxide/Titanium dioxide (Cu2O/TiO2) nanotube-array coaxial heterogeneous structure, which is supposed to have potential applications in photo-induced water decomposition and organic pollutant degradation. Such structure is formed by coating nano...

Full description

Bibliographic Details
Main Authors: Zhu, Wen, chong, baohe, Qin, Ke, Guan, Li, Hou, Xianghui, Chen, George Z.
Format: Article
Published: Royal Society of Chemistry 2016
Online Access:https://eprints.nottingham.ac.uk/34249/
_version_ 1848794807926784000
author Zhu, Wen
chong, baohe
Qin, Ke
Guan, Li
Hou, Xianghui
Chen, George Z.
author_facet Zhu, Wen
chong, baohe
Qin, Ke
Guan, Li
Hou, Xianghui
Chen, George Z.
author_sort Zhu, Wen
building Nottingham Research Data Repository
collection Online Access
description We report the formation and characterization of Cuprous oxide/Titanium dioxide (Cu2O/TiO2) nanotube-array coaxial heterogeneous structure, which is supposed to have potential applications in photo-induced water decomposition and organic pollutant degradation. Such structure is formed by coating nano-particles of Cu2O onto titanium dioxide nanotube-array walls via multiple-cycle chemical adsorption plus reduction method (MC-CAR). The practical deposition technique employs a soaking step to separate the adsorption and reduction processes, thus enhancing the controllability of deposition rate and preventing the clogging of nanotube pores. The size of Cu2O nano-particles is adjusted by changing the glucose concentration in the reaction solutions. As a result, compact nano-particle film with sufficiently small crystal sizes is uniformly covered on the tube walls, resulting in the formation of coaxial heterogeneous structure. The detailed synthesis process and the surface morphology, structure, photoelectric properties, and hydrogen evolution ability of the Cu2O/TiO2 nanotube-array with coaxial heterogeneous structure are systematically investigated. The resulting film shows a stable hydrogen production rate of 3.1 mLcm-2h-1, which can be targeted for energy application in relation with solar energy driven production of hydrogen from water.
first_indexed 2025-11-14T19:22:04Z
format Article
id nottingham-34249
institution University of Nottingham Malaysia Campus
institution_category Local University
last_indexed 2025-11-14T19:22:04Z
publishDate 2016
publisher Royal Society of Chemistry
recordtype eprints
repository_type Digital Repository
spelling nottingham-342492020-05-04T17:56:38Z https://eprints.nottingham.ac.uk/34249/ Cuprous oxide/Titanium dioxide nanotube-array with coaxial heterogeneous structure synthesized by multiple-cycle chemical adsorption plus reduction method Zhu, Wen chong, baohe Qin, Ke Guan, Li Hou, Xianghui Chen, George Z. We report the formation and characterization of Cuprous oxide/Titanium dioxide (Cu2O/TiO2) nanotube-array coaxial heterogeneous structure, which is supposed to have potential applications in photo-induced water decomposition and organic pollutant degradation. Such structure is formed by coating nano-particles of Cu2O onto titanium dioxide nanotube-array walls via multiple-cycle chemical adsorption plus reduction method (MC-CAR). The practical deposition technique employs a soaking step to separate the adsorption and reduction processes, thus enhancing the controllability of deposition rate and preventing the clogging of nanotube pores. The size of Cu2O nano-particles is adjusted by changing the glucose concentration in the reaction solutions. As a result, compact nano-particle film with sufficiently small crystal sizes is uniformly covered on the tube walls, resulting in the formation of coaxial heterogeneous structure. The detailed synthesis process and the surface morphology, structure, photoelectric properties, and hydrogen evolution ability of the Cu2O/TiO2 nanotube-array with coaxial heterogeneous structure are systematically investigated. The resulting film shows a stable hydrogen production rate of 3.1 mLcm-2h-1, which can be targeted for energy application in relation with solar energy driven production of hydrogen from water. Royal Society of Chemistry 2016-06-15 Article PeerReviewed Zhu, Wen, chong, baohe, Qin, Ke, Guan, Li, Hou, Xianghui and Chen, George Z. (2016) Cuprous oxide/Titanium dioxide nanotube-array with coaxial heterogeneous structure synthesized by multiple-cycle chemical adsorption plus reduction method. RSC Advances . ISSN 2046-2069 http://pubs.rsc.org/en/Content/ArticleLanding/2016/RA/C6RA06893F#!divAbstract doi:10.1039/C6RA06893F doi:10.1039/C6RA06893F
spellingShingle Zhu, Wen
chong, baohe
Qin, Ke
Guan, Li
Hou, Xianghui
Chen, George Z.
Cuprous oxide/Titanium dioxide nanotube-array with coaxial heterogeneous structure synthesized by multiple-cycle chemical adsorption plus reduction method
title Cuprous oxide/Titanium dioxide nanotube-array with coaxial heterogeneous structure synthesized by multiple-cycle chemical adsorption plus reduction method
title_full Cuprous oxide/Titanium dioxide nanotube-array with coaxial heterogeneous structure synthesized by multiple-cycle chemical adsorption plus reduction method
title_fullStr Cuprous oxide/Titanium dioxide nanotube-array with coaxial heterogeneous structure synthesized by multiple-cycle chemical adsorption plus reduction method
title_full_unstemmed Cuprous oxide/Titanium dioxide nanotube-array with coaxial heterogeneous structure synthesized by multiple-cycle chemical adsorption plus reduction method
title_short Cuprous oxide/Titanium dioxide nanotube-array with coaxial heterogeneous structure synthesized by multiple-cycle chemical adsorption plus reduction method
title_sort cuprous oxide/titanium dioxide nanotube-array with coaxial heterogeneous structure synthesized by multiple-cycle chemical adsorption plus reduction method
url https://eprints.nottingham.ac.uk/34249/
https://eprints.nottingham.ac.uk/34249/
https://eprints.nottingham.ac.uk/34249/