Measuring 19F shift anisotropies and 1H–19F dipolar interactions with ultrafast MAS NMR

Measuring 19F shift anisotropies and 1H–19F dipolar interactions with ultrafast MAS NMR

A new 19F anisotropic–isotropic shift correlation experiment is described that operates with ultrafast MAS, resulting in good resolution of isotropic 19F shifts in the detection dimension. The new experiment makes use of a recoupling sequence designed using symmetry principles that reintroduces the...

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Bibliographic Details
Main Authors: Martini, Francesca, Miah, Habeeba K., Iuga, Dinu, Geppi, Marco, Titman, Jeremy J.
Format: Article
Published: Elsevier 2015
Subjects:
Chemical shift anisotropy; Ultrafast magic angle spinning; Anisotropic–isotropic shift correlation; Symmetry-based recoupling sequence; Heteronuclear dipolar coupling; Dipole-shift correlation
Online Access:https://eprints.nottingham.ac.uk/30389/

Internet

https://eprints.nottingham.ac.uk/30389/

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