Detection of Amorphous Silica in Air-Oxidized Ti3SiC2 at 500–1000°C by NMR and SIMS

The use of secondary-ion mass spectrometry (SIMS), nuclear magnetic resonance (NMR) and transmission electron microscopy (TEM) to detect the existence of amorphous silica in Ti3SiC2 oxidised at 500–1000°C is described. The formation of an amorphous SiO2 layer and its growth in thickness with tempera...

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Main Authors: Pang, W, Low, It Meng, Hanna, J.
Format: Journal Article
Published: Trans Tech Publications 2010
Online Access:http://hdl.handle.net/20.500.11937/38454
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author Pang, W
Low, It Meng
Hanna, J.
author_facet Pang, W
Low, It Meng
Hanna, J.
author_sort Pang, W
building Curtin Institutional Repository
collection Online Access
description The use of secondary-ion mass spectrometry (SIMS), nuclear magnetic resonance (NMR) and transmission electron microscopy (TEM) to detect the existence of amorphous silica in Ti3SiC2 oxidised at 500–1000°C is described. The formation of an amorphous SiO2 layer and its growth in thickness with temperature was monitored using dynamic SIMS. Results of NMR and TEM verify for the first time the direct evidence of amorphous silica formation during the oxidation of Ti3SiC2 at ≤1000°C.
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institution Curtin University Malaysia
institution_category Local University
last_indexed 2025-11-14T08:54:30Z
publishDate 2010
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spelling curtin-20.500.11937-384542017-09-13T14:13:44Z Detection of Amorphous Silica in Air-Oxidized Ti3SiC2 at 500–1000°C by NMR and SIMS Pang, W Low, It Meng Hanna, J. The use of secondary-ion mass spectrometry (SIMS), nuclear magnetic resonance (NMR) and transmission electron microscopy (TEM) to detect the existence of amorphous silica in Ti3SiC2 oxidised at 500–1000°C is described. The formation of an amorphous SiO2 layer and its growth in thickness with temperature was monitored using dynamic SIMS. Results of NMR and TEM verify for the first time the direct evidence of amorphous silica formation during the oxidation of Ti3SiC2 at ≤1000°C. 2010 Journal Article http://hdl.handle.net/20.500.11937/38454 10.4028/www.scientific.net/KEM.434-435.169 Trans Tech Publications restricted
spellingShingle Pang, W
Low, It Meng
Hanna, J.
Detection of Amorphous Silica in Air-Oxidized Ti3SiC2 at 500–1000°C by NMR and SIMS
title Detection of Amorphous Silica in Air-Oxidized Ti3SiC2 at 500–1000°C by NMR and SIMS
title_full Detection of Amorphous Silica in Air-Oxidized Ti3SiC2 at 500–1000°C by NMR and SIMS
title_fullStr Detection of Amorphous Silica in Air-Oxidized Ti3SiC2 at 500–1000°C by NMR and SIMS
title_full_unstemmed Detection of Amorphous Silica in Air-Oxidized Ti3SiC2 at 500–1000°C by NMR and SIMS
title_short Detection of Amorphous Silica in Air-Oxidized Ti3SiC2 at 500–1000°C by NMR and SIMS
title_sort detection of amorphous silica in air-oxidized ti3sic2 at 500–1000°c by nmr and sims
url http://hdl.handle.net/20.500.11937/38454