Synthesis and characterisation of 3-vinyl[33](1,2,4) ferrocenophane

Synthesis and characterisation of 3-vinyl[33](1,2,4) ferrocenophane

Treatment of [33](1,2,4)ferrocenophane (1) with N-methylformanilide and phosphorus oxychloride gave 3-formyl[33](1,2,4)ferrocenophane (2) in 96% yield. Subsequently, (2) was reacted with an ylid in THF and 3-vinyl[33](1,2,4)ferrocenophane (3) was obtained in 88% yield.

Bibliographic Details
Main Authors: Lu, J., Baker, M., Brown, David
Format: Journal Article
Published: Elsevier 2006
Subjects:
Ferrocenophane
Bridged ferrocene
Ferrocene
Online Access:http://hdl.handle.net/20.500.11937/31060

Internet

http://hdl.handle.net/20.500.11937/31060

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