Synthesis, in vitro evaluation of thymidine phosphorylase inhibitory activity, and in silico study of 1,3,5-triazin-2,4-dione and its fused analogues

Based on structural similarities with the reference compounds, a series of 1,3,5-triazin-2,4-dione and their fused analogues was designed, synthesized and their in vitro thymidine phosphorylase inhibitory potential was evaluated. The monocyclic analogues were found to be inactive. Among the differen...

Full description

Bibliographic Details
Main Authors: Bera, H., Chui, W., Gupta, S., Dolzhenko, Anton, Sun, L.
Format: Journal Article
Published: 2013
Online Access:http://hdl.handle.net/20.500.11937/29884
_version_ 1848752929055440896
author Bera, H.
Chui, W.
Gupta, S.
Dolzhenko, Anton
Sun, L.
author_facet Bera, H.
Chui, W.
Gupta, S.
Dolzhenko, Anton
Sun, L.
author_sort Bera, H.
building Curtin Institutional Repository
collection Online Access
description Based on structural similarities with the reference compounds, a series of 1,3,5-triazin-2,4-dione and their fused analogues was designed, synthesized and their in vitro thymidine phosphorylase inhibitory potential was evaluated. The monocyclic analogues were found to be inactive. Among the different fused derivatives synthesized, compounds having keto group (C=O) at C7/C4 and thioketo group (C=S) at C5/C2 position showed TP inhibitory activity comparable to positive control, 7-deazaxanthine (7-DX) (IC50 value = 42.63 µM). Molecular docking of the target compounds into the enzyme thymidine phosphorylase was performed to illustrate the important structural information on the plausible ligand-enzyme-binding interactions. © 2013 Springer Science+Business Media New York.
first_indexed 2025-11-14T08:16:25Z
format Journal Article
id curtin-20.500.11937-29884
institution Curtin University Malaysia
institution_category Local University
last_indexed 2025-11-14T08:16:25Z
publishDate 2013
recordtype eprints
repository_type Digital Repository
spelling curtin-20.500.11937-298842017-09-13T12:22:58Z Synthesis, in vitro evaluation of thymidine phosphorylase inhibitory activity, and in silico study of 1,3,5-triazin-2,4-dione and its fused analogues Bera, H. Chui, W. Gupta, S. Dolzhenko, Anton Sun, L. Based on structural similarities with the reference compounds, a series of 1,3,5-triazin-2,4-dione and their fused analogues was designed, synthesized and their in vitro thymidine phosphorylase inhibitory potential was evaluated. The monocyclic analogues were found to be inactive. Among the different fused derivatives synthesized, compounds having keto group (C=O) at C7/C4 and thioketo group (C=S) at C5/C2 position showed TP inhibitory activity comparable to positive control, 7-deazaxanthine (7-DX) (IC50 value = 42.63 µM). Molecular docking of the target compounds into the enzyme thymidine phosphorylase was performed to illustrate the important structural information on the plausible ligand-enzyme-binding interactions. © 2013 Springer Science+Business Media New York. 2013 Journal Article http://hdl.handle.net/20.500.11937/29884 10.1007/s00044-013-0589-1 restricted
spellingShingle Bera, H.
Chui, W.
Gupta, S.
Dolzhenko, Anton
Sun, L.
Synthesis, in vitro evaluation of thymidine phosphorylase inhibitory activity, and in silico study of 1,3,5-triazin-2,4-dione and its fused analogues
title Synthesis, in vitro evaluation of thymidine phosphorylase inhibitory activity, and in silico study of 1,3,5-triazin-2,4-dione and its fused analogues
title_full Synthesis, in vitro evaluation of thymidine phosphorylase inhibitory activity, and in silico study of 1,3,5-triazin-2,4-dione and its fused analogues
title_fullStr Synthesis, in vitro evaluation of thymidine phosphorylase inhibitory activity, and in silico study of 1,3,5-triazin-2,4-dione and its fused analogues
title_full_unstemmed Synthesis, in vitro evaluation of thymidine phosphorylase inhibitory activity, and in silico study of 1,3,5-triazin-2,4-dione and its fused analogues
title_short Synthesis, in vitro evaluation of thymidine phosphorylase inhibitory activity, and in silico study of 1,3,5-triazin-2,4-dione and its fused analogues
title_sort synthesis, in vitro evaluation of thymidine phosphorylase inhibitory activity, and in silico study of 1,3,5-triazin-2,4-dione and its fused analogues
url http://hdl.handle.net/20.500.11937/29884