Nano-scale elastic-plastic properties and indentation-induced deformation of single crystal 4H-SiC

The nanoscale elastic-plastic response of single crystal 4H-SiC has been investigated by nanoindentationwith a Berkovich tip. The hardness (H) and elastic modulus (E) determined in the load-independent region were 36±2 GPa and 413±8 GPa, respectively. The indentation size effect (ISE) of hardness wi...

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Main Authors: Nawaz, A., Mao, W., Lu, Chunsheng, Shen, Y.
Format: Journal Article
Published: Elsevier 2017
Online Access:http://hdl.handle.net/20.500.11937/23175
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author Nawaz, A.
Mao, W.
Lu, Chunsheng
Shen, Y.
author_facet Nawaz, A.
Mao, W.
Lu, Chunsheng
Shen, Y.
author_sort Nawaz, A.
building Curtin Institutional Repository
collection Online Access
description The nanoscale elastic-plastic response of single crystal 4H-SiC has been investigated by nanoindentationwith a Berkovich tip. The hardness (H) and elastic modulus (E) determined in the load-independent region were 36±2 GPa and 413±8 GPa, respectively. The indentation size effect (ISE) of hardness within an indentation depth of 60 nm was systematically analyzed by the Nix-Gao model. Pop-in events occurring at a depth of ~23 nm with indentation loads of 0.60-0.65 mN were confirmed to indicate the elastic-plastic transition of the crystal, on the basis of the Hertzian contact theory and Johnson's cavity model. Theoritically calculated maximum tensile strength (13.5 GPa) and cleavage strength (33 GPa) also affirms the deformation due to the first pop-in rather than tensile stresses. Further analyses of deformation behavior across the indent was done in 4H-SiC by a combined technique of focused ion beam and transmission electron microscope, revealing that slippage occurred in the (0001) plane after indentation.
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institution Curtin University Malaysia
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publishDate 2017
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spelling curtin-20.500.11937-231752017-09-13T15:37:03Z Nano-scale elastic-plastic properties and indentation-induced deformation of single crystal 4H-SiC Nawaz, A. Mao, W. Lu, Chunsheng Shen, Y. The nanoscale elastic-plastic response of single crystal 4H-SiC has been investigated by nanoindentationwith a Berkovich tip. The hardness (H) and elastic modulus (E) determined in the load-independent region were 36±2 GPa and 413±8 GPa, respectively. The indentation size effect (ISE) of hardness within an indentation depth of 60 nm was systematically analyzed by the Nix-Gao model. Pop-in events occurring at a depth of ~23 nm with indentation loads of 0.60-0.65 mN were confirmed to indicate the elastic-plastic transition of the crystal, on the basis of the Hertzian contact theory and Johnson's cavity model. Theoritically calculated maximum tensile strength (13.5 GPa) and cleavage strength (33 GPa) also affirms the deformation due to the first pop-in rather than tensile stresses. Further analyses of deformation behavior across the indent was done in 4H-SiC by a combined technique of focused ion beam and transmission electron microscope, revealing that slippage occurred in the (0001) plane after indentation. 2017 Journal Article http://hdl.handle.net/20.500.11937/23175 10.1016/j.jmbbm.2016.11.013 Elsevier restricted
spellingShingle Nawaz, A.
Mao, W.
Lu, Chunsheng
Shen, Y.
Nano-scale elastic-plastic properties and indentation-induced deformation of single crystal 4H-SiC
title Nano-scale elastic-plastic properties and indentation-induced deformation of single crystal 4H-SiC
title_full Nano-scale elastic-plastic properties and indentation-induced deformation of single crystal 4H-SiC
title_fullStr Nano-scale elastic-plastic properties and indentation-induced deformation of single crystal 4H-SiC
title_full_unstemmed Nano-scale elastic-plastic properties and indentation-induced deformation of single crystal 4H-SiC
title_short Nano-scale elastic-plastic properties and indentation-induced deformation of single crystal 4H-SiC
title_sort nano-scale elastic-plastic properties and indentation-induced deformation of single crystal 4h-sic
url http://hdl.handle.net/20.500.11937/23175