Sample-displacement correction for whole-pattern profile fitting of powder diffraction data collected in capillary geometry

Abstract: Recent in situ experimentation at the Australian Synchrotron resulted in the nucleation and crystallization of material on the walls of the capillary reaction vessels. This lining of the capillary walls, without filling the bulk of the capillary volume, produced an artefact in the diffract...

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Bibliographic Details
Main Authors: Scarlett, N., Rowles, Matthew, Wallwork, K., Madsen, I.
Format: Journal Article
Published: BLACKWELL PUBLISHING 2011
Online Access:http://hdl.handle.net/20.500.11937/15939