3D analysis of creep voids in hydrogen reformer tubes

An ex-service hydrogen reformer tube composed of Fe-0.45% C-25% Cr-35% Ni-1.0% Si-1.5% Nb-1.0% Mn (approximate wt.%) was examined via serial sectioning and 3D reconstruction to characterize creep voids in terms of their size, location, and surrounding precipitates. In addition, electron backscatter...

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Main Authors: Wahab, A.A., Kral, M.V.
Format: Article
Published: Elsevier B.V 2005
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Online Access:http://eprints.utp.edu.my/2215/
id utp-2215
recordtype eprints
spelling utp-22152010-05-21T07:24:40Z 3D analysis of creep voids in hydrogen reformer tubes Wahab, A.A. Kral, M.V. TJ Mechanical engineering and machinery An ex-service hydrogen reformer tube composed of Fe-0.45% C-25% Cr-35% Ni-1.0% Si-1.5% Nb-1.0% Mn (approximate wt.%) was examined via serial sectioning and 3D reconstruction to characterize creep voids in terms of their size, location, and surrounding precipitates. In addition, electron backscatter diffraction (EBSD) technique was used to investigate any crystallographic influence on the location of these voids. Observations in 3D show that void distribution is not uniform in terms of size, shape, and location. Most of the voids are oblong and occur at grain edges and corners. In addition, all observed voids were in contact with the Cr-rich M23C6 precipitates. EBSD results showed that 80% of the M23C6 precipitates surrounding these voids have an irrational crystallographic orientation relationship (OR) with the austenite matrix, contrary to the expectation that grain boundary precipitates nearly always obtain rational OR with respect to one adjacent grain. Elsevier B.V 2005-12-05 Article PeerReviewed Wahab, A.A. and Kral, M.V. (2005) 3D analysis of creep voids in hydrogen reformer tubes. Materials Science and Engineering: A, 412 (1-2). pp. 222-229. ISSN 0921-5093 http://eprints.utp.edu.my/2215/
institution Universiti Teknologi Petronas
Universiti Teknologi Petronas
repository_type Digital Repository
institution_category Local University
building UTP Repository
collection Online Access
topic TJ Mechanical engineering and machinery
spellingShingle TJ Mechanical engineering and machinery
Wahab, A.A.
Kral, M.V.
3D analysis of creep voids in hydrogen reformer tubes
description An ex-service hydrogen reformer tube composed of Fe-0.45% C-25% Cr-35% Ni-1.0% Si-1.5% Nb-1.0% Mn (approximate wt.%) was examined via serial sectioning and 3D reconstruction to characterize creep voids in terms of their size, location, and surrounding precipitates. In addition, electron backscatter diffraction (EBSD) technique was used to investigate any crystallographic influence on the location of these voids. Observations in 3D show that void distribution is not uniform in terms of size, shape, and location. Most of the voids are oblong and occur at grain edges and corners. In addition, all observed voids were in contact with the Cr-rich M23C6 precipitates. EBSD results showed that 80% of the M23C6 precipitates surrounding these voids have an irrational crystallographic orientation relationship (OR) with the austenite matrix, contrary to the expectation that grain boundary precipitates nearly always obtain rational OR with respect to one adjacent grain.
format Article
author Wahab, A.A.
Kral, M.V.
author_facet Wahab, A.A.
Kral, M.V.
author_sort Wahab, A.A.
title 3D analysis of creep voids in hydrogen reformer tubes
title_short 3D analysis of creep voids in hydrogen reformer tubes
title_full 3D analysis of creep voids in hydrogen reformer tubes
title_fullStr 3D analysis of creep voids in hydrogen reformer tubes
title_full_unstemmed 3D analysis of creep voids in hydrogen reformer tubes
title_sort 3d analysis of creep voids in hydrogen reformer tubes
publisher Elsevier B.V
publishDate 2005
url http://eprints.utp.edu.my/2215/
first_indexed 2018-09-08T10:09:36Z
last_indexed 2018-09-08T10:09:36Z
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