(3E,5E)-1-Acryloyl-3,5-bis­(2-chloro­benzyl­idene)piperidin-4-one

(3E,5E)-1-Acryloyl-3,5-bis­(2-chloro­benzyl­idene)piperidin-4-one

In the title compound, C22H17Cl2NO2, the asymmetric unit consists of two crystallographically independent mol­ecules and each piperidinone ring adopts an envelope conformation. The dihedral angles between the two chloro­benzene rings are 24.81 (10) and 19.15 (8)° in the two mol­ecules. In the crysta...

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Main Authors: Basiri, Alireza, Murugaiyah, Vikneswaran, Osman, Hasnah, Hemamalini, Madhukar, Fun, Hoong-Kun
Format: Online
Language:English
Published: International Union of Crystallography 2011
Online Access:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3089119/
id pubmed-3089119
recordtype oai_dc
spelling pubmed-30891192011-07-13 (3E,5E)-1-Acryloyl-3,5-bis­(2-chloro­benzyl­idene)piperidin-4-one Basiri, Alireza Murugaiyah, Vikneswaran Osman, Hasnah Hemamalini, Madhukar Fun, Hoong-Kun Organic Papers In the title compound, C22H17Cl2NO2, the asymmetric unit consists of two crystallographically independent mol­ecules and each piperidinone ring adopts an envelope conformation. The dihedral angles between the two chloro­benzene rings are 24.81 (10) and 19.15 (8)° in the two mol­ecules. In the crystal, mol­ecules are connected via weak inter­molecular C—H⋯O hydrogen bonds forming layers perpendicular to the a axis. International Union of Crystallography 2011-04-29 /pmc/articles/PMC3089119/ /pubmed/21754526 http://dx.doi.org/10.1107/S1600536811015042 Text en © Basiri et al. 2011 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
repository_type Open Access Journal
institution_category Foreign Institution
institution US National Center for Biotechnology Information
building NCBI PubMed
collection Online Access
language English
format Online
author Basiri, Alireza
Murugaiyah, Vikneswaran
Osman, Hasnah
Hemamalini, Madhukar
Fun, Hoong-Kun
spellingShingle Basiri, Alireza
Murugaiyah, Vikneswaran
Osman, Hasnah
Hemamalini, Madhukar
Fun, Hoong-Kun
(3E,5E)-1-Acryloyl-3,5-bis­(2-chloro­benzyl­idene)piperidin-4-one
author_facet Basiri, Alireza
Murugaiyah, Vikneswaran
Osman, Hasnah
Hemamalini, Madhukar
Fun, Hoong-Kun
author_sort Basiri, Alireza
title (3E,5E)-1-Acryloyl-3,5-bis­(2-chloro­benzyl­idene)piperidin-4-one
title_short (3E,5E)-1-Acryloyl-3,5-bis­(2-chloro­benzyl­idene)piperidin-4-one
title_full (3E,5E)-1-Acryloyl-3,5-bis­(2-chloro­benzyl­idene)piperidin-4-one
title_fullStr (3E,5E)-1-Acryloyl-3,5-bis­(2-chloro­benzyl­idene)piperidin-4-one
title_full_unstemmed (3E,5E)-1-Acryloyl-3,5-bis­(2-chloro­benzyl­idene)piperidin-4-one
title_sort (3e,5e)-1-acryloyl-3,5-bis­(2-chloro­benzyl­idene)piperidin-4-one
description In the title compound, C22H17Cl2NO2, the asymmetric unit consists of two crystallographically independent mol­ecules and each piperidinone ring adopts an envelope conformation. The dihedral angles between the two chloro­benzene rings are 24.81 (10) and 19.15 (8)° in the two mol­ecules. In the crystal, mol­ecules are connected via weak inter­molecular C—H⋯O hydrogen bonds forming layers perpendicular to the a axis.
publisher International Union of Crystallography
publishDate 2011
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC3089119/
_version_ 1611452281599819776

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