CCVD synthesis of carbon nanotubes (CNTs) using MgO and CaCO3 supports

Carbon nanotubes or CNTs are graphene sheets that are rolled into nano-sized tubes. It has unique physical and electrical properties and has a lot of potential in research and practical applications. In this work, carbon nanotubes have been synthesized using catalytic chemical vapor deposition (CCVD...

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Main Authors: Mohamed Nasir, Mohamed Nuruddin, Buang, Nor Aziah, Ismail, Ahmad Fauzi
Format: Conference or Workshop Item
Language:English
Published: 2005
Subjects:
Online Access:http://eprints.utm.my/5364/
http://eprints.utm.my/5364/1/MohamedNuruddinMohamedNasir2005_CCVDSynthesisOfCarbonNanotubes%28CNTs%29.pdf
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author Mohamed Nasir, Mohamed Nuruddin
Buang, Nor Aziah
Ismail, Ahmad Fauzi
author_facet Mohamed Nasir, Mohamed Nuruddin
Buang, Nor Aziah
Ismail, Ahmad Fauzi
author_sort Mohamed Nasir, Mohamed Nuruddin
building UTeM Institutional Repository
collection Online Access
description Carbon nanotubes or CNTs are graphene sheets that are rolled into nano-sized tubes. It has unique physical and electrical properties and has a lot of potential in research and practical applications. In this work, carbon nanotubes have been synthesized using catalytic chemical vapor deposition (CCVD) method. This method has been identified as one of the most promising methods for large-scale CNT production. The catalysts used are Fe/Co bimetallic catalysts on magnesium oxide and calcium carbonate supports. The carbon source used is the acetylene gas. The nanotubes produced by the CCVD method are then treated with nitric acid in order to remove impurities such as carbonaceous matter, catalyst particles and catalyst support. The as-produced and purified CNTs were analyzed with scanning electron microscope (SEM), field-emission SEM (FE-SEM) and energy dispersive X-ray analysis (EDAX). The analysis results show that Ca and Mg salts are able to become supports in successful CCVD synthesis with Fe/Co catalyst. It also proves that acid treatment is capable of removing the catalyst particles and catalyst support from the magnesium oxide and calcium carbonate-supported CNTs.
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spelling utm-53642017-08-29T06:38:18Z http://eprints.utm.my/5364/ CCVD synthesis of carbon nanotubes (CNTs) using MgO and CaCO3 supports Mohamed Nasir, Mohamed Nuruddin Buang, Nor Aziah Ismail, Ahmad Fauzi T Technology (General) Carbon nanotubes or CNTs are graphene sheets that are rolled into nano-sized tubes. It has unique physical and electrical properties and has a lot of potential in research and practical applications. In this work, carbon nanotubes have been synthesized using catalytic chemical vapor deposition (CCVD) method. This method has been identified as one of the most promising methods for large-scale CNT production. The catalysts used are Fe/Co bimetallic catalysts on magnesium oxide and calcium carbonate supports. The carbon source used is the acetylene gas. The nanotubes produced by the CCVD method are then treated with nitric acid in order to remove impurities such as carbonaceous matter, catalyst particles and catalyst support. The as-produced and purified CNTs were analyzed with scanning electron microscope (SEM), field-emission SEM (FE-SEM) and energy dispersive X-ray analysis (EDAX). The analysis results show that Ca and Mg salts are able to become supports in successful CCVD synthesis with Fe/Co catalyst. It also proves that acid treatment is capable of removing the catalyst particles and catalyst support from the magnesium oxide and calcium carbonate-supported CNTs. 2005 Conference or Workshop Item PeerReviewed application/pdf en http://eprints.utm.my/5364/1/MohamedNuruddinMohamedNasir2005_CCVDSynthesisOfCarbonNanotubes%28CNTs%29.pdf Mohamed Nasir, Mohamed Nuruddin and Buang, Nor Aziah and Ismail, Ahmad Fauzi (2005) CCVD synthesis of carbon nanotubes (CNTs) using MgO and CaCO3 supports. In: The XXII Regional Conference on Solid State Science & Technology (RCSST' 05), 18-21 Dec 2005, Kuantan, Pahang. http://my.masshp.net/conference
spellingShingle T Technology (General)
Mohamed Nasir, Mohamed Nuruddin
Buang, Nor Aziah
Ismail, Ahmad Fauzi
CCVD synthesis of carbon nanotubes (CNTs) using MgO and CaCO3 supports
title CCVD synthesis of carbon nanotubes (CNTs) using MgO and CaCO3 supports
title_full CCVD synthesis of carbon nanotubes (CNTs) using MgO and CaCO3 supports
title_fullStr CCVD synthesis of carbon nanotubes (CNTs) using MgO and CaCO3 supports
title_full_unstemmed CCVD synthesis of carbon nanotubes (CNTs) using MgO and CaCO3 supports
title_short CCVD synthesis of carbon nanotubes (CNTs) using MgO and CaCO3 supports
title_sort ccvd synthesis of carbon nanotubes (cnts) using mgo and caco3 supports
topic T Technology (General)
url http://eprints.utm.my/5364/
http://eprints.utm.my/5364/
http://eprints.utm.my/5364/1/MohamedNuruddinMohamedNasir2005_CCVDSynthesisOfCarbonNanotubes%28CNTs%29.pdf