Penyediaan kaca aerosilika daripada sekam padi

The aim of this study is to prepare aerosilica glass from silica aerogel synthesized from rice husk. The study was carried out in order to produce a low thermal conductivity aerosilica glass that can be used as thermal insulator. Aerosilica glasses of nominal composition 5 %-55 % mol of aerogel were...

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Main Author: Abdullah, Rozieyati
Format: Thesis
Language:English
Published: 2004
Subjects:
Online Access:http://eprints.utm.my/5343/
http://eprints.utm.my/5343/1/RozieyatiAbdullahMFS2004.pdf
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author Abdullah, Rozieyati
author_facet Abdullah, Rozieyati
author_sort Abdullah, Rozieyati
building UTeM Institutional Repository
collection Online Access
description The aim of this study is to prepare aerosilica glass from silica aerogel synthesized from rice husk. The study was carried out in order to produce a low thermal conductivity aerosilica glass that can be used as thermal insulator. Aerosilica glasses of nominal composition 5 %-55 % mol of aerogel were prepared using a mixture of aerogel, SiOz with sodium carbonate, Na2C03. The glass samples of (Si02)@a20)1, were produced using liquid melt quenchng method at the melting temperature about 1 100 "C for aerosilica glass and 1400 "C for conventional sodium silicate glass. The study shows aerosilica glass is amorphous and exhibits better properties compared to conventional sodmn silicate glass with an optimum composition.of 20 % mol aerogel with density 2.39 g cm", thermal conductivity value of 1.35 ~ m k ' and Vickers micro hardness value of 412 Hv. According to the infrared spectrum, ths phenomena can be related to the structure of Si-0-Si bonds. The presence of foams by SEM micrograph contributes to the low thermal conductivity of aerosilica glass due to the formation of a new closed pores of 8 pm to 89 pm insize. The MAS-NMR spectra indicate a larger number of bridging 2 3 oxygen with Si atom in aerosilica glass as present Q ,Q and ~"pesies. The differential thermal analyzer shows aerosilica glass can be obtained at a lower temperature range of 8 18-828 "C which is stable against corrosive agents. W-VISNIR analysis shows the samples absorbance in UV light range is related to thermal conductivity.
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spelling utm-53432018-03-07T20:57:49Z http://eprints.utm.my/5343/ Penyediaan kaca aerosilika daripada sekam padi Abdullah, Rozieyati QD Chemistry The aim of this study is to prepare aerosilica glass from silica aerogel synthesized from rice husk. The study was carried out in order to produce a low thermal conductivity aerosilica glass that can be used as thermal insulator. Aerosilica glasses of nominal composition 5 %-55 % mol of aerogel were prepared using a mixture of aerogel, SiOz with sodium carbonate, Na2C03. The glass samples of (Si02)@a20)1, were produced using liquid melt quenchng method at the melting temperature about 1 100 "C for aerosilica glass and 1400 "C for conventional sodium silicate glass. The study shows aerosilica glass is amorphous and exhibits better properties compared to conventional sodmn silicate glass with an optimum composition.of 20 % mol aerogel with density 2.39 g cm", thermal conductivity value of 1.35 ~ m k ' and Vickers micro hardness value of 412 Hv. According to the infrared spectrum, ths phenomena can be related to the structure of Si-0-Si bonds. The presence of foams by SEM micrograph contributes to the low thermal conductivity of aerosilica glass due to the formation of a new closed pores of 8 pm to 89 pm insize. The MAS-NMR spectra indicate a larger number of bridging 2 3 oxygen with Si atom in aerosilica glass as present Q ,Q and ~"pesies. The differential thermal analyzer shows aerosilica glass can be obtained at a lower temperature range of 8 18-828 "C which is stable against corrosive agents. W-VISNIR analysis shows the samples absorbance in UV light range is related to thermal conductivity. 2004-03 Thesis NonPeerReviewed application/pdf en http://eprints.utm.my/5343/1/RozieyatiAbdullahMFS2004.pdf Abdullah, Rozieyati (2004) Penyediaan kaca aerosilika daripada sekam padi. Masters thesis, Universiti Teknologi Malaysia, Faculty of Science.
spellingShingle QD Chemistry
Abdullah, Rozieyati
Penyediaan kaca aerosilika daripada sekam padi
title Penyediaan kaca aerosilika daripada sekam padi
title_full Penyediaan kaca aerosilika daripada sekam padi
title_fullStr Penyediaan kaca aerosilika daripada sekam padi
title_full_unstemmed Penyediaan kaca aerosilika daripada sekam padi
title_short Penyediaan kaca aerosilika daripada sekam padi
title_sort penyediaan kaca aerosilika daripada sekam padi
topic QD Chemistry
url http://eprints.utm.my/5343/
http://eprints.utm.my/5343/1/RozieyatiAbdullahMFS2004.pdf