Proton exchange membranes prepared by simultaneous radiation grafting of styrene onto poly(tetrafluoroethylene-co-hexafluoropropylene) films. II. Properties of sulfonated membranes

Proton exchange membranes were prepared by radiation-induced grafting of styrene onto commercial poly(tetrafluoroethylene-co-hexafluoropropylene) films using a simultaneous irradiation technique followed by a sulfonation reaction. The resulting membranes were characterized by measuring their physico...

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Main Authors: Nasef, Mohamed Mahmoud, Saidi, Hamdani, Mohd Nor, Hussin, Ooi, Mun Foo
Format: Article
Language:English
Published: John Wiley & Sons, Inc. 2000
Subjects:
Online Access:http://eprints.utm.my/3678/
http://eprints.utm.my/3678/1/Nasef2000_ProtonExchangeMembranesSimultaneousRadiationII.pdf
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author Nasef, Mohamed Mahmoud
Saidi, Hamdani
Mohd Nor, Hussin
Ooi, Mun Foo
author_facet Nasef, Mohamed Mahmoud
Saidi, Hamdani
Mohd Nor, Hussin
Ooi, Mun Foo
author_sort Nasef, Mohamed Mahmoud
building UTeM Institutional Repository
collection Online Access
description Proton exchange membranes were prepared by radiation-induced grafting of styrene onto commercial poly(tetrafluoroethylene-co-hexafluoropropylene) films using a simultaneous irradiation technique followed by a sulfonation reaction. The resulting membranes were characterized by measuring their physicochemical properties such as water uptake, ion exchange capacity, hydration number, and proton conductivity as a function of the degree of grafting. The thermal properties (melting and glass transition temperatures) and thermal stability of the membrane were also investigated using differential scanning calorimetry and thermal gravimetric analysis, respectively. Membranes having degrees of grafting of 16%and above showed proton conductivity of the magnitude of 1022 V21 cm21 at room temperature, as well as thermal stability at up to 290°C under an oxygen atmosphere.
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publishDate 2000
publisher John Wiley & Sons, Inc.
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spelling utm-36782010-06-01T03:11:22Z http://eprints.utm.my/3678/ Proton exchange membranes prepared by simultaneous radiation grafting of styrene onto poly(tetrafluoroethylene-co-hexafluoropropylene) films. II. Properties of sulfonated membranes Nasef, Mohamed Mahmoud Saidi, Hamdani Mohd Nor, Hussin Ooi, Mun Foo TP Chemical technology Proton exchange membranes were prepared by radiation-induced grafting of styrene onto commercial poly(tetrafluoroethylene-co-hexafluoropropylene) films using a simultaneous irradiation technique followed by a sulfonation reaction. The resulting membranes were characterized by measuring their physicochemical properties such as water uptake, ion exchange capacity, hydration number, and proton conductivity as a function of the degree of grafting. The thermal properties (melting and glass transition temperatures) and thermal stability of the membrane were also investigated using differential scanning calorimetry and thermal gravimetric analysis, respectively. Membranes having degrees of grafting of 16%and above showed proton conductivity of the magnitude of 1022 V21 cm21 at room temperature, as well as thermal stability at up to 290°C under an oxygen atmosphere. John Wiley & Sons, Inc. 2000 Article PeerReviewed application/pdf en http://eprints.utm.my/3678/1/Nasef2000_ProtonExchangeMembranesSimultaneousRadiationII.pdf Nasef, Mohamed Mahmoud and Saidi, Hamdani and Mohd Nor, Hussin and Ooi, Mun Foo (2000) Proton exchange membranes prepared by simultaneous radiation grafting of styrene onto poly(tetrafluoroethylene-co-hexafluoropropylene) films. II. Properties of sulfonated membranes. Journal of Applied Polymer Science, 78 . pp. 2443-2453.
spellingShingle TP Chemical technology
Nasef, Mohamed Mahmoud
Saidi, Hamdani
Mohd Nor, Hussin
Ooi, Mun Foo
Proton exchange membranes prepared by simultaneous radiation grafting of styrene onto poly(tetrafluoroethylene-co-hexafluoropropylene) films. II. Properties of sulfonated membranes
title Proton exchange membranes prepared by simultaneous radiation grafting of styrene onto poly(tetrafluoroethylene-co-hexafluoropropylene) films. II. Properties of sulfonated membranes
title_full Proton exchange membranes prepared by simultaneous radiation grafting of styrene onto poly(tetrafluoroethylene-co-hexafluoropropylene) films. II. Properties of sulfonated membranes
title_fullStr Proton exchange membranes prepared by simultaneous radiation grafting of styrene onto poly(tetrafluoroethylene-co-hexafluoropropylene) films. II. Properties of sulfonated membranes
title_full_unstemmed Proton exchange membranes prepared by simultaneous radiation grafting of styrene onto poly(tetrafluoroethylene-co-hexafluoropropylene) films. II. Properties of sulfonated membranes
title_short Proton exchange membranes prepared by simultaneous radiation grafting of styrene onto poly(tetrafluoroethylene-co-hexafluoropropylene) films. II. Properties of sulfonated membranes
title_sort proton exchange membranes prepared by simultaneous radiation grafting of styrene onto poly(tetrafluoroethylene-co-hexafluoropropylene) films. ii. properties of sulfonated membranes
topic TP Chemical technology
url http://eprints.utm.my/3678/
http://eprints.utm.my/3678/1/Nasef2000_ProtonExchangeMembranesSimultaneousRadiationII.pdf