Sonochemistry approach for a new process of biodiesel production from Jatropha Curcas Oil

This thesis presents the sonochemistry approach to reduce required reaction time to convert the Jatropha Curcas oil into biodiesel using an the ultrasound clamp on tubular reactor. The effect of diameter clamp on tubular reactor to remove free fatty acid (FFA) in the esterification process was inves...

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Main Author: Praptijanto, Achmad
Format: Thesis
Language:English
English
English
Published: 2011
Subjects:
Online Access:http://eprints.uthm.edu.my/2581/
http://eprints.uthm.edu.my/2581/1/24p%20ACHMAD%20PRAPTIJANTO.pdf
http://eprints.uthm.edu.my/2581/2/ACHMAD%20PRAPTIJANTO%20COPYRIGHT%20DECLARATION.pdf
http://eprints.uthm.edu.my/2581/3/ACHMAD%20PRAPTIJANTO%20WATERMARK.pdf
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author Praptijanto, Achmad
author_facet Praptijanto, Achmad
author_sort Praptijanto, Achmad
building UTHM Institutional Repository
collection Online Access
description This thesis presents the sonochemistry approach to reduce required reaction time to convert the Jatropha Curcas oil into biodiesel using an the ultrasound clamp on tubular reactor. The effect of diameter clamp on tubular reactor to remove free fatty acid (FFA) in the esterification process was investigated. The concentrations of methanol and catalyst in the transesterification process were clearly observed in this research. While in the purification process, the water concentration to oil, the output power and reaction time were investigated. The tube of diameter 60 mm removed FFA to below 1 % in 5 minutes. The optimum condition of the transesterification process was a molar ratio of methanol to oil of 7:1, catalyst concentration of 1 %, time of reaction of 5 minutes. Meanwhile the optimum condition of the purification process was at water concentration of 10 % (v/v), power output of 240 W, time of reaction of 5 minutes. The reaction time of esterification by clamp on tubular reactor reduces until 96 %, and transesterification reaction reduces until 83 % compared to conventional stirring method. The small pilot plant has been developed in this research according to the optimum condition. The average energy for one kg of biodiesel needed 0.06 kWh and 11 hour time of production process. In the performance engine and emission, this decreased of the brake specific fuel consumption (BSFC) and brake specific energy consumption (BSEC) could be due to lower heating value and higher density compared to diesel fuel. As an average amount of smoke density, was decreased to 60 % compared to diesel fuel. Average lessening of CO2 was determined as same as diesel fuel.
first_indexed 2025-11-15T19:59:46Z
format Thesis
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institution Universiti Tun Hussein Onn Malaysia
institution_category Local University
language English
English
English
last_indexed 2025-11-15T19:59:46Z
publishDate 2011
recordtype eprints
repository_type Digital Repository
spelling uthm-25812021-11-01T02:44:27Z http://eprints.uthm.edu.my/2581/ Sonochemistry approach for a new process of biodiesel production from Jatropha Curcas Oil Praptijanto, Achmad TP Chemical technology TP315-360 Fuel This thesis presents the sonochemistry approach to reduce required reaction time to convert the Jatropha Curcas oil into biodiesel using an the ultrasound clamp on tubular reactor. The effect of diameter clamp on tubular reactor to remove free fatty acid (FFA) in the esterification process was investigated. The concentrations of methanol and catalyst in the transesterification process were clearly observed in this research. While in the purification process, the water concentration to oil, the output power and reaction time were investigated. The tube of diameter 60 mm removed FFA to below 1 % in 5 minutes. The optimum condition of the transesterification process was a molar ratio of methanol to oil of 7:1, catalyst concentration of 1 %, time of reaction of 5 minutes. Meanwhile the optimum condition of the purification process was at water concentration of 10 % (v/v), power output of 240 W, time of reaction of 5 minutes. The reaction time of esterification by clamp on tubular reactor reduces until 96 %, and transesterification reaction reduces until 83 % compared to conventional stirring method. The small pilot plant has been developed in this research according to the optimum condition. The average energy for one kg of biodiesel needed 0.06 kWh and 11 hour time of production process. In the performance engine and emission, this decreased of the brake specific fuel consumption (BSFC) and brake specific energy consumption (BSEC) could be due to lower heating value and higher density compared to diesel fuel. As an average amount of smoke density, was decreased to 60 % compared to diesel fuel. Average lessening of CO2 was determined as same as diesel fuel. 2011-04 Thesis NonPeerReviewed text en http://eprints.uthm.edu.my/2581/1/24p%20ACHMAD%20PRAPTIJANTO.pdf text en http://eprints.uthm.edu.my/2581/2/ACHMAD%20PRAPTIJANTO%20COPYRIGHT%20DECLARATION.pdf text en http://eprints.uthm.edu.my/2581/3/ACHMAD%20PRAPTIJANTO%20WATERMARK.pdf Praptijanto, Achmad (2011) Sonochemistry approach for a new process of biodiesel production from Jatropha Curcas Oil. Masters thesis, Universiti Tun Hussein Malaysia.
spellingShingle TP Chemical technology
TP315-360 Fuel
Praptijanto, Achmad
Sonochemistry approach for a new process of biodiesel production from Jatropha Curcas Oil
title Sonochemistry approach for a new process of biodiesel production from Jatropha Curcas Oil
title_full Sonochemistry approach for a new process of biodiesel production from Jatropha Curcas Oil
title_fullStr Sonochemistry approach for a new process of biodiesel production from Jatropha Curcas Oil
title_full_unstemmed Sonochemistry approach for a new process of biodiesel production from Jatropha Curcas Oil
title_short Sonochemistry approach for a new process of biodiesel production from Jatropha Curcas Oil
title_sort sonochemistry approach for a new process of biodiesel production from jatropha curcas oil
topic TP Chemical technology
TP315-360 Fuel
url http://eprints.uthm.edu.my/2581/
http://eprints.uthm.edu.my/2581/1/24p%20ACHMAD%20PRAPTIJANTO.pdf
http://eprints.uthm.edu.my/2581/2/ACHMAD%20PRAPTIJANTO%20COPYRIGHT%20DECLARATION.pdf
http://eprints.uthm.edu.my/2581/3/ACHMAD%20PRAPTIJANTO%20WATERMARK.pdf