Removal of bisphenol A from aqueous media using a highly selective adsorbent of hybridization cyclodextrin with magnetic molecularly imprinted polymer

In this study, a unique magnetic molecularly imprinted polymer (MMIP) adsorbent towards bisphenol A (BPA) as a template molecule was developed by bulk polymerization using β-cyclodextrin (β-CD) as a co-monomer with methacrylic acid (MAA) to form MMIP MAA–βCD as a new adsorbent. β-CD was hybridi...

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Main Authors: Mamman, S., Suah, F. B. M., Raaov, M., Mehamod, F. S., Asman, S., M. Zain, N. N.
Format: Article
Language:English
Published: The Royal Society 2021
Subjects:
Online Access:http://eprints.uthm.edu.my/1814/
http://eprints.uthm.edu.my/1814/1/J12152_a1893f84a39923f956ee525a09bc01a5.pdf
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author Mamman, S.
Suah, F. B. M.
Raaov, M.
Mehamod, F. S.
Asman, S.
M. Zain, N. N.
author_facet Mamman, S.
Suah, F. B. M.
Raaov, M.
Mehamod, F. S.
Asman, S.
M. Zain, N. N.
author_sort Mamman, S.
building UTHM Institutional Repository
collection Online Access
description In this study, a unique magnetic molecularly imprinted polymer (MMIP) adsorbent towards bisphenol A (BPA) as a template molecule was developed by bulk polymerization using β-cyclodextrin (β-CD) as a co-monomer with methacrylic acid (MAA) to form MMIP MAA–βCD as a new adsorbent. β-CD was hybridized with MAA to obtain water-compactible imprinting sites for the effective removal of BPA from aqueous samples. Benzoyl peroxide and trimethylolpropane trimethacrylate were used as the initiator and cross-linker, respectively. The adsorbents were characterized by Fourier transform infrared spectroscopy, scanning electronic microscopy, transmission electron microscopy, vibrating sample magnetometer, Brunauer–Emmett–Teller and X-ray diffraction. 1H nuclear magnetic resonance spectroscopy was used to characterize the MAA–βCD and BPA–MAA–βCD complex. Several parameters influencing the adsorption efficiency of BPA such as adsorbent dosage, pH of sample solution, contact time, initial concentrations and temperature as well as selectivity and reusability study have been evaluated. MMIP MAA–βCD
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publishDate 2021
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spelling uthm-18142021-10-18T03:28:33Z http://eprints.uthm.edu.my/1814/ Removal of bisphenol A from aqueous media using a highly selective adsorbent of hybridization cyclodextrin with magnetic molecularly imprinted polymer Mamman, S. Suah, F. B. M. Raaov, M. Mehamod, F. S. Asman, S. M. Zain, N. N. TP1080-1185 Polymers and polymer manufacture In this study, a unique magnetic molecularly imprinted polymer (MMIP) adsorbent towards bisphenol A (BPA) as a template molecule was developed by bulk polymerization using β-cyclodextrin (β-CD) as a co-monomer with methacrylic acid (MAA) to form MMIP MAA–βCD as a new adsorbent. β-CD was hybridized with MAA to obtain water-compactible imprinting sites for the effective removal of BPA from aqueous samples. Benzoyl peroxide and trimethylolpropane trimethacrylate were used as the initiator and cross-linker, respectively. The adsorbents were characterized by Fourier transform infrared spectroscopy, scanning electronic microscopy, transmission electron microscopy, vibrating sample magnetometer, Brunauer–Emmett–Teller and X-ray diffraction. 1H nuclear magnetic resonance spectroscopy was used to characterize the MAA–βCD and BPA–MAA–βCD complex. Several parameters influencing the adsorption efficiency of BPA such as adsorbent dosage, pH of sample solution, contact time, initial concentrations and temperature as well as selectivity and reusability study have been evaluated. MMIP MAA–βCD The Royal Society 2021 Article PeerReviewed text en http://eprints.uthm.edu.my/1814/1/J12152_a1893f84a39923f956ee525a09bc01a5.pdf Mamman, S. and Suah, F. B. M. and Raaov, M. and Mehamod, F. S. and Asman, S. and M. Zain, N. N. (2021) Removal of bisphenol A from aqueous media using a highly selective adsorbent of hybridization cyclodextrin with magnetic molecularly imprinted polymer. Royal Society Open Science. pp. 1-21. https://doi.org/10.6084/m9.figshare.c. 5323499.
spellingShingle TP1080-1185 Polymers and polymer manufacture
Mamman, S.
Suah, F. B. M.
Raaov, M.
Mehamod, F. S.
Asman, S.
M. Zain, N. N.
Removal of bisphenol A from aqueous media using a highly selective adsorbent of hybridization cyclodextrin with magnetic molecularly imprinted polymer
title Removal of bisphenol A from aqueous media using a highly selective adsorbent of hybridization cyclodextrin with magnetic molecularly imprinted polymer
title_full Removal of bisphenol A from aqueous media using a highly selective adsorbent of hybridization cyclodextrin with magnetic molecularly imprinted polymer
title_fullStr Removal of bisphenol A from aqueous media using a highly selective adsorbent of hybridization cyclodextrin with magnetic molecularly imprinted polymer
title_full_unstemmed Removal of bisphenol A from aqueous media using a highly selective adsorbent of hybridization cyclodextrin with magnetic molecularly imprinted polymer
title_short Removal of bisphenol A from aqueous media using a highly selective adsorbent of hybridization cyclodextrin with magnetic molecularly imprinted polymer
title_sort removal of bisphenol a from aqueous media using a highly selective adsorbent of hybridization cyclodextrin with magnetic molecularly imprinted polymer
topic TP1080-1185 Polymers and polymer manufacture
url http://eprints.uthm.edu.my/1814/
http://eprints.uthm.edu.my/1814/
http://eprints.uthm.edu.my/1814/1/J12152_a1893f84a39923f956ee525a09bc01a5.pdf