Development of Alumina Based Feedstock For Fused Deposition Modelling 3D Printer

Alumina is ceramics with excellent properties such as chemical inertness, high hardness, and thermal stability. However, alumina product forming process like powder metallurgy, casting, and plastic forming could be troublesome as alumina shape manipulation is inflexible. Integration of additive manu...

Full description

Bibliographic Details
Main Author: Tan, Roe Djer
Format: Final Year Project / Dissertation / Thesis
Published: 2020
Subjects:
Online Access:http://eprints.utar.edu.my/4113/
http://eprints.utar.edu.my/4113/1/1505057_fyp_report_%2D_ROE_DJER_TAN.pdf
_version_ 1848886079982141440
author Tan, Roe Djer
author_facet Tan, Roe Djer
author_sort Tan, Roe Djer
building UTAR Institutional Repository
collection Online Access
description Alumina is ceramics with excellent properties such as chemical inertness, high hardness, and thermal stability. However, alumina product forming process like powder metallurgy, casting, and plastic forming could be troublesome as alumina shape manipulation is inflexible. Integration of additive manufacturing (AM) with alumina formulation is a potential game changer that revitalize the alumina forming industry due to flexibility and customizability of AM. In fact, there have been studies done regarding to alumina 3D printing. However, question still remain on the development of alumina-based feedstock for fused deposition modelling (FDM) 3D printing due to very few studies in this sector. Therefore, alumina-based feedstock for FDM 3D printer was developed and investigated in this study. The in-depth understandings provided in this study could guide the alumina manufacturing industry in formulation of complex shape alumina such as body armour as well as rapid alumina prototyping. This work was initiated with doping of 1 wt% Titanium dioxide (TiO2) into alumina powder to reduce the sintering temperature of alumina. Cellulose acetate (CA) as a binder was then mixed with acetone with concentration of 100 g/L, 150 g/L, and 200 g/L to form a transparent solution. The transparent solution was mixed with alumina powder with binder-solvent volume occupation up to 90 vol% to form a slurry. It was followed by preparation of green samples from the slurry and they were debinded and pressureless sintered at 1400 ºC for an hour. Characteristic tests were done to determine the flow curve of the slurries as well as the bulk density and the hardness of the sintered samples. X-ray diffraction (XRD) and microstructure analyses were conducted to further reflect the properties of the samples. Sample prepared by CA-acetone concentration of 200 g/L with 80 vol% binder exhibited the highest bulk density of 2.963 g/cc (75 % relative density), the highest microstructural compaction, and appropriate slurry viscosity as required by FDM. As a result, it is feasible to apply alumina-based feedstock with CA as binder in FDM 3D printer.
first_indexed 2025-11-15T19:32:48Z
format Final Year Project / Dissertation / Thesis
id utar-4113
institution Universiti Tunku Abdul Rahman
institution_category Local University
last_indexed 2025-11-15T19:32:48Z
publishDate 2020
recordtype eprints
repository_type Digital Repository
spelling utar-41132021-06-11T22:55:11Z Development of Alumina Based Feedstock For Fused Deposition Modelling 3D Printer Tan, Roe Djer TJ Mechanical engineering and machinery Alumina is ceramics with excellent properties such as chemical inertness, high hardness, and thermal stability. However, alumina product forming process like powder metallurgy, casting, and plastic forming could be troublesome as alumina shape manipulation is inflexible. Integration of additive manufacturing (AM) with alumina formulation is a potential game changer that revitalize the alumina forming industry due to flexibility and customizability of AM. In fact, there have been studies done regarding to alumina 3D printing. However, question still remain on the development of alumina-based feedstock for fused deposition modelling (FDM) 3D printing due to very few studies in this sector. Therefore, alumina-based feedstock for FDM 3D printer was developed and investigated in this study. The in-depth understandings provided in this study could guide the alumina manufacturing industry in formulation of complex shape alumina such as body armour as well as rapid alumina prototyping. This work was initiated with doping of 1 wt% Titanium dioxide (TiO2) into alumina powder to reduce the sintering temperature of alumina. Cellulose acetate (CA) as a binder was then mixed with acetone with concentration of 100 g/L, 150 g/L, and 200 g/L to form a transparent solution. The transparent solution was mixed with alumina powder with binder-solvent volume occupation up to 90 vol% to form a slurry. It was followed by preparation of green samples from the slurry and they were debinded and pressureless sintered at 1400 ºC for an hour. Characteristic tests were done to determine the flow curve of the slurries as well as the bulk density and the hardness of the sintered samples. X-ray diffraction (XRD) and microstructure analyses were conducted to further reflect the properties of the samples. Sample prepared by CA-acetone concentration of 200 g/L with 80 vol% binder exhibited the highest bulk density of 2.963 g/cc (75 % relative density), the highest microstructural compaction, and appropriate slurry viscosity as required by FDM. As a result, it is feasible to apply alumina-based feedstock with CA as binder in FDM 3D printer. 2020 Final Year Project / Dissertation / Thesis NonPeerReviewed application/pdf http://eprints.utar.edu.my/4113/1/1505057_fyp_report_%2D_ROE_DJER_TAN.pdf Tan, Roe Djer (2020) Development of Alumina Based Feedstock For Fused Deposition Modelling 3D Printer. Final Year Project, UTAR. http://eprints.utar.edu.my/4113/
spellingShingle TJ Mechanical engineering and machinery
Tan, Roe Djer
Development of Alumina Based Feedstock For Fused Deposition Modelling 3D Printer
title Development of Alumina Based Feedstock For Fused Deposition Modelling 3D Printer
title_full Development of Alumina Based Feedstock For Fused Deposition Modelling 3D Printer
title_fullStr Development of Alumina Based Feedstock For Fused Deposition Modelling 3D Printer
title_full_unstemmed Development of Alumina Based Feedstock For Fused Deposition Modelling 3D Printer
title_short Development of Alumina Based Feedstock For Fused Deposition Modelling 3D Printer
title_sort development of alumina based feedstock for fused deposition modelling 3d printer
topic TJ Mechanical engineering and machinery
url http://eprints.utar.edu.my/4113/
http://eprints.utar.edu.my/4113/1/1505057_fyp_report_%2D_ROE_DJER_TAN.pdf