Photocatalytic Removal Of Methylene Blue From Aqueous Solution By Ag And La Doped Tio2 And Zeolite Supported Tio2 Under Visible Light

In the present study titanium dioxide (tio2) nanoparticles (nps) were modified via ag, la and ag-la doping using low cost and facile liquid impregnation (li) method, immobilization on zeolite, and at different calcination temperatures (500, 700 and 900 °c). The unsupported tio2 nps (tio2, ag/tio2...

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Main Author: Us Saqib, Najm
Format: Thesis
Language:English
Published: 2017
Subjects:
Online Access:http://eprints.usm.my/63058/
http://eprints.usm.my/63058/1/Pages%20from%202-PHS18020965.pdf
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author Us Saqib, Najm
author_facet Us Saqib, Najm
author_sort Us Saqib, Najm
building USM Institutional Repository
collection Online Access
description In the present study titanium dioxide (tio2) nanoparticles (nps) were modified via ag, la and ag-la doping using low cost and facile liquid impregnation (li) method, immobilization on zeolite, and at different calcination temperatures (500, 700 and 900 °c). The unsupported tio2 nps (tio2, ag/tio2, ag-la/tio2, and la/tio2) prepared at different calcination temperatures, showed dominant anatase phase (96 to 98 wt%), reduction of band gap energy from 3.2 to 2.88 ev, and phpzc between 6.2 to 7.3. The zeolite supported samples (z@tio2, z@ag/tio2, z@ag-la/tio2, and z@la/tio2) prepared at different calcination temperatures, showed the appearance of rutile and brookite phases which reached up to 20 wt% with the increase in calcination temperature, less reduction in band gap energy (3.11 to 2.90 ev) and higher ph/>zc values (7.1 to 7.8) as compared to the unsupported tio2 nps. The photocatalytic degradation of mb by unsupported and zeolite supported tio2 nps were performed under normal laboratory condition which is at ambient ph, room temperature (25±2 °c) and compact fluorescent light.
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spelling usm-630582025-10-24T07:15:40Z http://eprints.usm.my/63058/ Photocatalytic Removal Of Methylene Blue From Aqueous Solution By Ag And La Doped Tio2 And Zeolite Supported Tio2 Under Visible Light Us Saqib, Najm QD1-999 Chemistry In the present study titanium dioxide (tio2) nanoparticles (nps) were modified via ag, la and ag-la doping using low cost and facile liquid impregnation (li) method, immobilization on zeolite, and at different calcination temperatures (500, 700 and 900 °c). The unsupported tio2 nps (tio2, ag/tio2, ag-la/tio2, and la/tio2) prepared at different calcination temperatures, showed dominant anatase phase (96 to 98 wt%), reduction of band gap energy from 3.2 to 2.88 ev, and phpzc between 6.2 to 7.3. The zeolite supported samples (z@tio2, z@ag/tio2, z@ag-la/tio2, and z@la/tio2) prepared at different calcination temperatures, showed the appearance of rutile and brookite phases which reached up to 20 wt% with the increase in calcination temperature, less reduction in band gap energy (3.11 to 2.90 ev) and higher ph/>zc values (7.1 to 7.8) as compared to the unsupported tio2 nps. The photocatalytic degradation of mb by unsupported and zeolite supported tio2 nps were performed under normal laboratory condition which is at ambient ph, room temperature (25±2 °c) and compact fluorescent light. 2017-08 Thesis NonPeerReviewed application/pdf en http://eprints.usm.my/63058/1/Pages%20from%202-PHS18020965.pdf Us Saqib, Najm (2017) Photocatalytic Removal Of Methylene Blue From Aqueous Solution By Ag And La Doped Tio2 And Zeolite Supported Tio2 Under Visible Light. PhD thesis, Perpustakaan Hamzah Sendut.
spellingShingle QD1-999 Chemistry
Us Saqib, Najm
Photocatalytic Removal Of Methylene Blue From Aqueous Solution By Ag And La Doped Tio2 And Zeolite Supported Tio2 Under Visible Light
title Photocatalytic Removal Of Methylene Blue From Aqueous Solution By Ag And La Doped Tio2 And Zeolite Supported Tio2 Under Visible Light
title_full Photocatalytic Removal Of Methylene Blue From Aqueous Solution By Ag And La Doped Tio2 And Zeolite Supported Tio2 Under Visible Light
title_fullStr Photocatalytic Removal Of Methylene Blue From Aqueous Solution By Ag And La Doped Tio2 And Zeolite Supported Tio2 Under Visible Light
title_full_unstemmed Photocatalytic Removal Of Methylene Blue From Aqueous Solution By Ag And La Doped Tio2 And Zeolite Supported Tio2 Under Visible Light
title_short Photocatalytic Removal Of Methylene Blue From Aqueous Solution By Ag And La Doped Tio2 And Zeolite Supported Tio2 Under Visible Light
title_sort photocatalytic removal of methylene blue from aqueous solution by ag and la doped tio2 and zeolite supported tio2 under visible light
topic QD1-999 Chemistry
url http://eprints.usm.my/63058/
http://eprints.usm.my/63058/1/Pages%20from%202-PHS18020965.pdf