Effect Of Stand-Off Distance And Plasma Current On The Properties Of Hydroxyapatite Coatings Produced By Plasma Spray

Plasma sprayed hydroxyapatite (HA) coatings on metallic implants for biomedical applications are attracted significant researchers interest due to accelerated rate of bone bonding that occurs following their implantation. This present work aims to produce plasma sprayed HA coatings with varying s...

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Main Author: Sulaiman, Wan Ruzaini Wan
Format: Thesis
Language:English
Published: 2014
Subjects:
Online Access:http://eprints.usm.my/62357/
http://eprints.usm.my/62357/1/24%20Pages%20from%2000001785126.pdf
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author Sulaiman, Wan Ruzaini Wan
author_facet Sulaiman, Wan Ruzaini Wan
author_sort Sulaiman, Wan Ruzaini Wan
building USM Institutional Repository
collection Online Access
description Plasma sprayed hydroxyapatite (HA) coatings on metallic implants for biomedical applications are attracted significant researchers interest due to accelerated rate of bone bonding that occurs following their implantation. This present work aims to produce plasma sprayed HA coatings with varying spray parameters (i.e.; stand-off distance, SOD and plasma current, PC) in order to control the coatings crystallinity. The substrate used is 316L stainless steel. Five SODs were selected i.e. 80 mm, 100 mm, 120 mm, 140 mm and 160 mm combined with two different PCs (500 A and 600 A), respectively. The coatings then divided into two groups (as sprayed and heat treated). Both coating was subjected to in vitro test through immersion in SBF solution up to 28 days to determine their bioactivity. The coating properties before and after immersion in SBF were analyzed using FESEM and XRD. The analysis showed coatings morphology consists of type III, V and VIII splats with lamella and non-lamella structures. The crystallinity of as-sprayed coatings is in vicinity of 50%. However, the crystallinity increases more than 90% after heat treatment process. The in vitro analysis proved that the highest apatite layer precipitations on surface with coatings surface was from the assprayed coatings rather than the one being heat treated. Therefore, the quality of HA coating via plasma spray coating technique can be modified through the suitable combination is at SOD 120 mm and PC 600 A.
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format Thesis
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institution Universiti Sains Malaysia
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language English
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publishDate 2014
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spelling usm-623572025-05-28T02:13:27Z http://eprints.usm.my/62357/ Effect Of Stand-Off Distance And Plasma Current On The Properties Of Hydroxyapatite Coatings Produced By Plasma Spray Sulaiman, Wan Ruzaini Wan TN1-997 Mining engineering. Metallurgy Plasma sprayed hydroxyapatite (HA) coatings on metallic implants for biomedical applications are attracted significant researchers interest due to accelerated rate of bone bonding that occurs following their implantation. This present work aims to produce plasma sprayed HA coatings with varying spray parameters (i.e.; stand-off distance, SOD and plasma current, PC) in order to control the coatings crystallinity. The substrate used is 316L stainless steel. Five SODs were selected i.e. 80 mm, 100 mm, 120 mm, 140 mm and 160 mm combined with two different PCs (500 A and 600 A), respectively. The coatings then divided into two groups (as sprayed and heat treated). Both coating was subjected to in vitro test through immersion in SBF solution up to 28 days to determine their bioactivity. The coating properties before and after immersion in SBF were analyzed using FESEM and XRD. The analysis showed coatings morphology consists of type III, V and VIII splats with lamella and non-lamella structures. The crystallinity of as-sprayed coatings is in vicinity of 50%. However, the crystallinity increases more than 90% after heat treatment process. The in vitro analysis proved that the highest apatite layer precipitations on surface with coatings surface was from the assprayed coatings rather than the one being heat treated. Therefore, the quality of HA coating via plasma spray coating technique can be modified through the suitable combination is at SOD 120 mm and PC 600 A. 2014-12 Thesis NonPeerReviewed application/pdf en http://eprints.usm.my/62357/1/24%20Pages%20from%2000001785126.pdf Sulaiman, Wan Ruzaini Wan (2014) Effect Of Stand-Off Distance And Plasma Current On The Properties Of Hydroxyapatite Coatings Produced By Plasma Spray. Masters thesis, Perpustakaan Hamzah Sendut.
spellingShingle TN1-997 Mining engineering. Metallurgy
Sulaiman, Wan Ruzaini Wan
Effect Of Stand-Off Distance And Plasma Current On The Properties Of Hydroxyapatite Coatings Produced By Plasma Spray
title Effect Of Stand-Off Distance And Plasma Current On The Properties Of Hydroxyapatite Coatings Produced By Plasma Spray
title_full Effect Of Stand-Off Distance And Plasma Current On The Properties Of Hydroxyapatite Coatings Produced By Plasma Spray
title_fullStr Effect Of Stand-Off Distance And Plasma Current On The Properties Of Hydroxyapatite Coatings Produced By Plasma Spray
title_full_unstemmed Effect Of Stand-Off Distance And Plasma Current On The Properties Of Hydroxyapatite Coatings Produced By Plasma Spray
title_short Effect Of Stand-Off Distance And Plasma Current On The Properties Of Hydroxyapatite Coatings Produced By Plasma Spray
title_sort effect of stand-off distance and plasma current on the properties of hydroxyapatite coatings produced by plasma spray
topic TN1-997 Mining engineering. Metallurgy
url http://eprints.usm.my/62357/
http://eprints.usm.my/62357/1/24%20Pages%20from%2000001785126.pdf