Raw Material Characterization And Reductive Leaching Of Low Grade Manganese Ore With Bamboo Sawdust In Sulphuric Acid

This research used two types of raw materials which are synthetic manganese ore and low grade manganese ore. The characterization analysis of raw materials was determined via morphological study and phase identification. The results showed synthetic manganese ore is high grade with 34.32 % Mn and th...

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Main Author: Muthalib, Nurhidayah Abdul
Format: Thesis
Language:English
Published: 2019
Subjects:
Online Access:http://eprints.usm.my/46712/
http://eprints.usm.my/46712/1/Raw%20Material%20Characterization%20And%20Reductive%20Leaching%20Of%20Low%20Grade%20Manganese%20Ore%20With%20Bamboo%20Sawdust%20In%20Sulphuric%20Acid.pdf
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author Muthalib, Nurhidayah Abdul
author_facet Muthalib, Nurhidayah Abdul
author_sort Muthalib, Nurhidayah Abdul
building USM Institutional Repository
collection Online Access
description This research used two types of raw materials which are synthetic manganese ore and low grade manganese ore. The characterization analysis of raw materials was determined via morphological study and phase identification. The results showed synthetic manganese ore is high grade with 34.32 % Mn and the manganese ore is of low grade with 15.26 % Mn. The phase present in synthetic manganese ore is pyrolusite and the low grade manganese ore contains the pyrolusite, goethite and quartz phases. The reductive leaching of synthetic manganese ore and low grade manganese ore were conducted using bamboo sawdust as a reducing agent in sulphuric acid. Synthetic manganese ore was leached acted as a control experiment for the manganese ore. Leaching was conducted for 360 minute. Maximum manganese extraction and the effects of sulphuric acid concentration (2.5 M – 4.0 M) and temperature (70 oC – 100 oC) on manganese extraction were also determined. The results indicated maximum manganese extractions of 96.14 % and 75.48 % were achieved using 4.0 M sulphuric acid concentration at 100 oC for the synthetic manganese ore and low grade manganese ore. The sugar identification of bamboo sawdust and glucose degradation was also determined. Bamboo sawdust which contain cellulose (56.11 %) and hemicellulose (28.6 %) was degraded into glucose as the major sugar. The glucose present in the leaching system was (15-20) %. The glucose produced was used to reduce the Mn ores and degraded into organic acid. The major organic acid formed was formic acid (<0.005 ppm).
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institution Universiti Sains Malaysia
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language English
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publishDate 2019
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spelling usm-467122021-11-17T03:42:12Z http://eprints.usm.my/46712/ Raw Material Characterization And Reductive Leaching Of Low Grade Manganese Ore With Bamboo Sawdust In Sulphuric Acid Muthalib, Nurhidayah Abdul T Technology TA401-492 Materials of engineering and construction. Mechanics of materials This research used two types of raw materials which are synthetic manganese ore and low grade manganese ore. The characterization analysis of raw materials was determined via morphological study and phase identification. The results showed synthetic manganese ore is high grade with 34.32 % Mn and the manganese ore is of low grade with 15.26 % Mn. The phase present in synthetic manganese ore is pyrolusite and the low grade manganese ore contains the pyrolusite, goethite and quartz phases. The reductive leaching of synthetic manganese ore and low grade manganese ore were conducted using bamboo sawdust as a reducing agent in sulphuric acid. Synthetic manganese ore was leached acted as a control experiment for the manganese ore. Leaching was conducted for 360 minute. Maximum manganese extraction and the effects of sulphuric acid concentration (2.5 M – 4.0 M) and temperature (70 oC – 100 oC) on manganese extraction were also determined. The results indicated maximum manganese extractions of 96.14 % and 75.48 % were achieved using 4.0 M sulphuric acid concentration at 100 oC for the synthetic manganese ore and low grade manganese ore. The sugar identification of bamboo sawdust and glucose degradation was also determined. Bamboo sawdust which contain cellulose (56.11 %) and hemicellulose (28.6 %) was degraded into glucose as the major sugar. The glucose present in the leaching system was (15-20) %. The glucose produced was used to reduce the Mn ores and degraded into organic acid. The major organic acid formed was formic acid (<0.005 ppm). 2019-03-01 Thesis NonPeerReviewed application/pdf en http://eprints.usm.my/46712/1/Raw%20Material%20Characterization%20And%20Reductive%20Leaching%20Of%20Low%20Grade%20Manganese%20Ore%20With%20Bamboo%20Sawdust%20In%20Sulphuric%20Acid.pdf Muthalib, Nurhidayah Abdul (2019) Raw Material Characterization And Reductive Leaching Of Low Grade Manganese Ore With Bamboo Sawdust In Sulphuric Acid. Masters thesis, Universiti Sains Malaysia.
spellingShingle T Technology
TA401-492 Materials of engineering and construction. Mechanics of materials
Muthalib, Nurhidayah Abdul
Raw Material Characterization And Reductive Leaching Of Low Grade Manganese Ore With Bamboo Sawdust In Sulphuric Acid
title Raw Material Characterization And Reductive Leaching Of Low Grade Manganese Ore With Bamboo Sawdust In Sulphuric Acid
title_full Raw Material Characterization And Reductive Leaching Of Low Grade Manganese Ore With Bamboo Sawdust In Sulphuric Acid
title_fullStr Raw Material Characterization And Reductive Leaching Of Low Grade Manganese Ore With Bamboo Sawdust In Sulphuric Acid
title_full_unstemmed Raw Material Characterization And Reductive Leaching Of Low Grade Manganese Ore With Bamboo Sawdust In Sulphuric Acid
title_short Raw Material Characterization And Reductive Leaching Of Low Grade Manganese Ore With Bamboo Sawdust In Sulphuric Acid
title_sort raw material characterization and reductive leaching of low grade manganese ore with bamboo sawdust in sulphuric acid
topic T Technology
TA401-492 Materials of engineering and construction. Mechanics of materials
url http://eprints.usm.my/46712/
http://eprints.usm.my/46712/1/Raw%20Material%20Characterization%20And%20Reductive%20Leaching%20Of%20Low%20Grade%20Manganese%20Ore%20With%20Bamboo%20Sawdust%20In%20Sulphuric%20Acid.pdf