Characterization And Properties Of Synthesized And Sintered Carbonated Hydroxyapatite

B-type Carbonated Hydroxyapatite (CHA) was successfully synthesized via nanoemulsion method, through dropwise (DW) and direct pouring (DP) techniques. The carbonate content in DP (8.60%) was higher than DW (7.85%). Both techniques produced nano-sized powders with variation in shapes of particles. I...

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Main Author: Ismail, Yanny Marliana Baba
Format: Thesis
Language:English
Published: 2011
Subjects:
Online Access:http://eprints.usm.my/42852/
http://eprints.usm.my/42852/1/YANNY_MARLIANA.pdf
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author Ismail, Yanny Marliana Baba
author_facet Ismail, Yanny Marliana Baba
author_sort Ismail, Yanny Marliana Baba
building USM Institutional Repository
collection Online Access
description B-type Carbonated Hydroxyapatite (CHA) was successfully synthesized via nanoemulsion method, through dropwise (DW) and direct pouring (DP) techniques. The carbonate content in DP (8.60%) was higher than DW (7.85%). Both techniques produced nano-sized powders with variation in shapes of particles. It was also found that at temperature (≤ 40°C), the CHA powders were angular while above this critical temperature mixture of rods and angular shape was produced. Room temperature synthesis was better as they produced nano-size CHA with larger surface area. Sintering was then performed on pure CHA, CHA+Mg(OH)2, HA and HA+Mg(OH)2, samples which was cooled down with and without wet CO2 atmosphere to produce different type of carbonate substitution in the structure.
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institution Universiti Sains Malaysia
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language English
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publishDate 2011
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spelling usm-428522019-04-12T05:26:36Z http://eprints.usm.my/42852/ Characterization And Properties Of Synthesized And Sintered Carbonated Hydroxyapatite Ismail, Yanny Marliana Baba TN1-997 Mining engineering. Metallurgy B-type Carbonated Hydroxyapatite (CHA) was successfully synthesized via nanoemulsion method, through dropwise (DW) and direct pouring (DP) techniques. The carbonate content in DP (8.60%) was higher than DW (7.85%). Both techniques produced nano-sized powders with variation in shapes of particles. It was also found that at temperature (≤ 40°C), the CHA powders were angular while above this critical temperature mixture of rods and angular shape was produced. Room temperature synthesis was better as they produced nano-size CHA with larger surface area. Sintering was then performed on pure CHA, CHA+Mg(OH)2, HA and HA+Mg(OH)2, samples which was cooled down with and without wet CO2 atmosphere to produce different type of carbonate substitution in the structure. 2011-05 Thesis NonPeerReviewed application/pdf en http://eprints.usm.my/42852/1/YANNY_MARLIANA.pdf Ismail, Yanny Marliana Baba (2011) Characterization And Properties Of Synthesized And Sintered Carbonated Hydroxyapatite. Masters thesis, Universiti Sains Malaysia.
spellingShingle TN1-997 Mining engineering. Metallurgy
Ismail, Yanny Marliana Baba
Characterization And Properties Of Synthesized And Sintered Carbonated Hydroxyapatite
title Characterization And Properties Of Synthesized And Sintered Carbonated Hydroxyapatite
title_full Characterization And Properties Of Synthesized And Sintered Carbonated Hydroxyapatite
title_fullStr Characterization And Properties Of Synthesized And Sintered Carbonated Hydroxyapatite
title_full_unstemmed Characterization And Properties Of Synthesized And Sintered Carbonated Hydroxyapatite
title_short Characterization And Properties Of Synthesized And Sintered Carbonated Hydroxyapatite
title_sort characterization and properties of synthesized and sintered carbonated hydroxyapatite
topic TN1-997 Mining engineering. Metallurgy
url http://eprints.usm.my/42852/
http://eprints.usm.my/42852/1/YANNY_MARLIANA.pdf