Synthesis And Characterization Of Sb2O3 Nanoparticles By Chemical Reduction Method
Antimony trioxide (Sb2O3) nanoparticles with particle size less than 100 nm, spherical in shape and well distributed were successfully synthesized by chemical reducing method. Antimony trichloride (SbCl3) was reduced by hydrazine in the presence of sodium hydroxide (NaOH) as catalyst in ethylene gly...
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| Format: | Thesis |
| Language: | English |
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2012
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| Online Access: | http://eprints.usm.my/41727/ http://eprints.usm.my/41727/1/CHIN_HUI_SHUN.pdf |
| _version_ | 1848879366293946368 |
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| author | Chin , Hui Shun |
| author_facet | Chin , Hui Shun |
| author_sort | Chin , Hui Shun |
| building | USM Institutional Repository |
| collection | Online Access |
| description | Antimony trioxide (Sb2O3) nanoparticles with particle size less than 100 nm, spherical in shape and well distributed were successfully synthesized by chemical reducing method. Antimony trichloride (SbCl3) was reduced by hydrazine in the presence of sodium hydroxide (NaOH) as catalyst in ethylene glycol (EG) at 120 oC for 60 minutes. In order to synthesis Sb2O3 nanoparticles with smaller particle size (2 - 12 nm), spherical in shape and well distribution, effects of hydrazine concentration ([N2H5OH]/[SbCl3] = 0.75, 5, 10, 20 and 30), NaOH concentration ([NaOH]/[SbCl3] = 0, 1, 3 and 5), precursor concentration ([SbCl3]/[N2H5OH] = 0.05, 0.1, 0.15 and 0.2), reaction temperature (60, 90, 120 and 150oC), reaction time (30, 60, 90 and 120 minutes) and boiling temperature (25, 50, 80 and 110oC) were investigated. |
| first_indexed | 2025-11-15T17:46:05Z |
| format | Thesis |
| id | usm-41727 |
| institution | Universiti Sains Malaysia |
| institution_category | Local University |
| language | English |
| last_indexed | 2025-11-15T17:46:05Z |
| publishDate | 2012 |
| recordtype | eprints |
| repository_type | Digital Repository |
| spelling | usm-417272019-04-12T05:26:22Z http://eprints.usm.my/41727/ Synthesis And Characterization Of Sb2O3 Nanoparticles By Chemical Reduction Method Chin , Hui Shun TN1-997 Mining engineering. Metallurgy Antimony trioxide (Sb2O3) nanoparticles with particle size less than 100 nm, spherical in shape and well distributed were successfully synthesized by chemical reducing method. Antimony trichloride (SbCl3) was reduced by hydrazine in the presence of sodium hydroxide (NaOH) as catalyst in ethylene glycol (EG) at 120 oC for 60 minutes. In order to synthesis Sb2O3 nanoparticles with smaller particle size (2 - 12 nm), spherical in shape and well distribution, effects of hydrazine concentration ([N2H5OH]/[SbCl3] = 0.75, 5, 10, 20 and 30), NaOH concentration ([NaOH]/[SbCl3] = 0, 1, 3 and 5), precursor concentration ([SbCl3]/[N2H5OH] = 0.05, 0.1, 0.15 and 0.2), reaction temperature (60, 90, 120 and 150oC), reaction time (30, 60, 90 and 120 minutes) and boiling temperature (25, 50, 80 and 110oC) were investigated. 2012-03 Thesis NonPeerReviewed application/pdf en http://eprints.usm.my/41727/1/CHIN_HUI_SHUN.pdf Chin , Hui Shun (2012) Synthesis And Characterization Of Sb2O3 Nanoparticles By Chemical Reduction Method. Masters thesis, Universiti Sains Malaysia. |
| spellingShingle | TN1-997 Mining engineering. Metallurgy Chin , Hui Shun Synthesis And Characterization Of Sb2O3 Nanoparticles By Chemical Reduction Method |
| title | Synthesis And Characterization Of Sb2O3 Nanoparticles By Chemical Reduction Method |
| title_full | Synthesis And Characterization Of Sb2O3 Nanoparticles By Chemical Reduction Method |
| title_fullStr | Synthesis And Characterization Of Sb2O3 Nanoparticles By Chemical Reduction Method |
| title_full_unstemmed | Synthesis And Characterization Of Sb2O3 Nanoparticles By Chemical Reduction Method |
| title_short | Synthesis And Characterization Of Sb2O3 Nanoparticles By Chemical Reduction Method |
| title_sort | synthesis and characterization of sb2o3 nanoparticles by chemical reduction method |
| topic | TN1-997 Mining engineering. Metallurgy |
| url | http://eprints.usm.my/41727/ http://eprints.usm.my/41727/1/CHIN_HUI_SHUN.pdf |