1-[(E)-(3-Hydroxy-4-methoxybenzylidene)amino]- 3-methylthiourea
In the title thiosemicarbazone Schiff base compound, C10H13N3O2S, the dihedral angle between the benzene ring and methyl carbothioamide side arm was found to be 17.4 (4)�. The presence of two intramolecular hydrogen bonds is noted, namely hydroxy-O—H� � �O(methoxy) and amine-N—H� � �N(imine). In...
| Main Authors: | , , |
|---|---|
| Format: | Article |
| Language: | English |
| Published: |
International Union of Crystallography
2016
|
| Subjects: | |
| Online Access: | http://eprints.usm.my/37935/ http://eprints.usm.my/37935/1/1-%5B%28E%29-%283-Hydroxy-4-methoxybenzylidene%29amino%5D-.pdf |
| Summary: | In the title thiosemicarbazone Schiff base compound, C10H13N3O2S, the dihedral
angle between the benzene ring and methyl carbothioamide side arm was found
to be 17.4 (4)�. The presence of two intramolecular hydrogen bonds is noted,
namely hydroxy-O—H� � �O(methoxy) and amine-N—H� � �N(imine). In the
crystal, pairwise amine-N—H� � �S hydrogen bonds give rise to centrosymmetric
{� � �HNCS}2 synthons, which lead to dimeric aggregates. |
|---|