EFFECT OF DIFFERENT COMPACTION PRESSURE AND DIFFERENT SINTERING ROUTE ON K0.5Na0.5NBO₃ PHYSICAL AND DIELECTRIC PROPERTIES

Alkaline niobate known as K0.5Na0.5NbO3 (KNN), a lead-free piezoelectric ceramic was synthesized via a solid state reaction method. The samples were compacted at different pressures (100, 200, 300 and 400 MPa) and sintered using two different techniques (conventional furnace and hot isostatic pres...

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Main Authors: Bahanurddin, Nor Fatin Khairah, Ahmad, Zainal Arifin, Mohamed, Julie Juliewatty
Format: Article
Language:English
Published: University of Chemistry and Technology, Prague & Institute of Rock Structure and Mechanics of the ASCR, v.v.i. 2016
Subjects:
Online Access:http://eprints.usm.my/36911/
http://eprints.usm.my/36911/1/%28EFFECT_OF_DIFFERENT_COMPACTION_PRESSURE%29_Bahanurddin_CS_2016_0033.pdf
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author Bahanurddin, Nor Fatin Khairah
Ahmad, Zainal Arifin
Mohamed, Julie Juliewatty
author_facet Bahanurddin, Nor Fatin Khairah
Ahmad, Zainal Arifin
Mohamed, Julie Juliewatty
author_sort Bahanurddin, Nor Fatin Khairah
building USM Institutional Repository
collection Online Access
description Alkaline niobate known as K0.5Na0.5NbO3 (KNN), a lead-free piezoelectric ceramic was synthesized via a solid state reaction method. The samples were compacted at different pressures (100, 200, 300 and 400 MPa) and sintered using two different techniques (conventional furnace and hot isostatic pressing (HIP)). The effect of compaction pressure and sintering technique on physical and dielectric properties was studied. The optimum compaction pressure (300 MPa) and sintering via HIP (at 1080°C for 30 min) increased the density and grain size (range 30 - 300 nm) and improved its dielectric properties. Therefore, the combination of suitable compaction pressure and sintering technique has produced larger grain size and higher density of KNN which resulted in outstanding dielectric properties. At room temperature, excellent values of ɛr (5517.35) and tan δ (0.954), recorded at 1 MHz were measured for the KNN300HIP sample with highest density (4.4885 g∙cm-3).
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publishDate 2016
publisher University of Chemistry and Technology, Prague & Institute of Rock Structure and Mechanics of the ASCR, v.v.i.
recordtype eprints
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spelling usm-369112017-10-04T01:14:59Z http://eprints.usm.my/36911/ EFFECT OF DIFFERENT COMPACTION PRESSURE AND DIFFERENT SINTERING ROUTE ON K0.5Na0.5NBO₃ PHYSICAL AND DIELECTRIC PROPERTIES Bahanurddin, Nor Fatin Khairah Ahmad, Zainal Arifin Mohamed, Julie Juliewatty TN1-997 Mining engineering. Metallurgy Alkaline niobate known as K0.5Na0.5NbO3 (KNN), a lead-free piezoelectric ceramic was synthesized via a solid state reaction method. The samples were compacted at different pressures (100, 200, 300 and 400 MPa) and sintered using two different techniques (conventional furnace and hot isostatic pressing (HIP)). The effect of compaction pressure and sintering technique on physical and dielectric properties was studied. The optimum compaction pressure (300 MPa) and sintering via HIP (at 1080°C for 30 min) increased the density and grain size (range 30 - 300 nm) and improved its dielectric properties. Therefore, the combination of suitable compaction pressure and sintering technique has produced larger grain size and higher density of KNN which resulted in outstanding dielectric properties. At room temperature, excellent values of ɛr (5517.35) and tan δ (0.954), recorded at 1 MHz were measured for the KNN300HIP sample with highest density (4.4885 g∙cm-3). University of Chemistry and Technology, Prague & Institute of Rock Structure and Mechanics of the ASCR, v.v.i. 2016 Article PeerReviewed application/pdf en http://eprints.usm.my/36911/1/%28EFFECT_OF_DIFFERENT_COMPACTION_PRESSURE%29_Bahanurddin_CS_2016_0033.pdf Bahanurddin, Nor Fatin Khairah and Ahmad, Zainal Arifin and Mohamed, Julie Juliewatty (2016) EFFECT OF DIFFERENT COMPACTION PRESSURE AND DIFFERENT SINTERING ROUTE ON K0.5Na0.5NBO₃ PHYSICAL AND DIELECTRIC PROPERTIES. Ceramics-Silikáty, 60 (3). pp. 220-225. ISSN 0862-5468 https://doi.org/10.13168/cs.2016.0033
spellingShingle TN1-997 Mining engineering. Metallurgy
Bahanurddin, Nor Fatin Khairah
Ahmad, Zainal Arifin
Mohamed, Julie Juliewatty
EFFECT OF DIFFERENT COMPACTION PRESSURE AND DIFFERENT SINTERING ROUTE ON K0.5Na0.5NBO₃ PHYSICAL AND DIELECTRIC PROPERTIES
title EFFECT OF DIFFERENT COMPACTION PRESSURE AND DIFFERENT SINTERING ROUTE ON K0.5Na0.5NBO₃ PHYSICAL AND DIELECTRIC PROPERTIES
title_full EFFECT OF DIFFERENT COMPACTION PRESSURE AND DIFFERENT SINTERING ROUTE ON K0.5Na0.5NBO₃ PHYSICAL AND DIELECTRIC PROPERTIES
title_fullStr EFFECT OF DIFFERENT COMPACTION PRESSURE AND DIFFERENT SINTERING ROUTE ON K0.5Na0.5NBO₃ PHYSICAL AND DIELECTRIC PROPERTIES
title_full_unstemmed EFFECT OF DIFFERENT COMPACTION PRESSURE AND DIFFERENT SINTERING ROUTE ON K0.5Na0.5NBO₃ PHYSICAL AND DIELECTRIC PROPERTIES
title_short EFFECT OF DIFFERENT COMPACTION PRESSURE AND DIFFERENT SINTERING ROUTE ON K0.5Na0.5NBO₃ PHYSICAL AND DIELECTRIC PROPERTIES
title_sort effect of different compaction pressure and different sintering route on k0.5na0.5nbo₃ physical and dielectric properties
topic TN1-997 Mining engineering. Metallurgy
url http://eprints.usm.my/36911/
http://eprints.usm.my/36911/
http://eprints.usm.my/36911/1/%28EFFECT_OF_DIFFERENT_COMPACTION_PRESSURE%29_Bahanurddin_CS_2016_0033.pdf