Aerosolized niosome formulation containing gemcitabine and cisplatin for lung cancer treatment: optimization, characterization and in vitro evaluation

Gemcitabine (Gem) and cisplatin (Cis) are currently being used for lung cancer treatment, but they are highly toxic in high dosages. This research aimed to develop a niosome formulation containing a low-dosage Gem and Cis (NGC), as an alternative formulation for lung cancer treatment. NGC was prepar...

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Main Authors: Mohamad Saimi, Norfatin Izzatie, Salim, Norazlinaliza, Ahmad, Noraini, Abdulmalek, Emilia, Abdul Rahman, Mohd Basyaruddin
Format: Article
Published: Multidisciplinary Digital Publishing Institute 2021
Online Access:http://psasir.upm.edu.my/id/eprint/95735/
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author Mohamad Saimi, Norfatin Izzatie
Salim, Norazlinaliza
Ahmad, Noraini
Abdulmalek, Emilia
Abdul Rahman, Mohd Basyaruddin
author_facet Mohamad Saimi, Norfatin Izzatie
Salim, Norazlinaliza
Ahmad, Noraini
Abdulmalek, Emilia
Abdul Rahman, Mohd Basyaruddin
author_sort Mohamad Saimi, Norfatin Izzatie
building UPM Institutional Repository
collection Online Access
description Gemcitabine (Gem) and cisplatin (Cis) are currently being used for lung cancer treatment, but they are highly toxic in high dosages. This research aimed to develop a niosome formulation containing a low-dosage Gem and Cis (NGC), as an alternative formulation for lung cancer treatment. NGC was prepared using a very simple heating method and was further optimized by D-optimal mixture design. The optimum NGC formulation with particle size, polydispersity index (PDI), and zeta potential of 166.45 nm, 0.16, and -15.28 mV, respectively, was obtained and remained stable at 27 °C with no phase separation for up to 90 days. The aerosol output was 96.22%, which indicates its suitability as aerosolized formulation. An in vitro drug release study using the dialysis bag diffusion technique showed controlled release for both drugs up to 24 h penetration. A cytotoxicity study against normal lung (MRC5) and lung cancer (A549) cell lines was investigated. The results showed that the optimized NGC had reduced cytotoxicity effects against both MRC5 and A549 when compared with the control (Gem + Cis alone) from very toxic (IC50 < 1.56 µg/mL) to weakly toxic (IC50 280.00 µg/mL) and moderately toxic (IC50 = 46.00 µg/mL), respectively, after 72 h of treatment. These findings revealed that the optimized NGC has excellent potential and is a promising prospect in aerosolized delivery systems to treat lung cancer that warrants further investigation.
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institution Universiti Putra Malaysia
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spelling upm-957352023-04-06T07:10:20Z http://psasir.upm.edu.my/id/eprint/95735/ Aerosolized niosome formulation containing gemcitabine and cisplatin for lung cancer treatment: optimization, characterization and in vitro evaluation Mohamad Saimi, Norfatin Izzatie Salim, Norazlinaliza Ahmad, Noraini Abdulmalek, Emilia Abdul Rahman, Mohd Basyaruddin Gemcitabine (Gem) and cisplatin (Cis) are currently being used for lung cancer treatment, but they are highly toxic in high dosages. This research aimed to develop a niosome formulation containing a low-dosage Gem and Cis (NGC), as an alternative formulation for lung cancer treatment. NGC was prepared using a very simple heating method and was further optimized by D-optimal mixture design. The optimum NGC formulation with particle size, polydispersity index (PDI), and zeta potential of 166.45 nm, 0.16, and -15.28 mV, respectively, was obtained and remained stable at 27 °C with no phase separation for up to 90 days. The aerosol output was 96.22%, which indicates its suitability as aerosolized formulation. An in vitro drug release study using the dialysis bag diffusion technique showed controlled release for both drugs up to 24 h penetration. A cytotoxicity study against normal lung (MRC5) and lung cancer (A549) cell lines was investigated. The results showed that the optimized NGC had reduced cytotoxicity effects against both MRC5 and A549 when compared with the control (Gem + Cis alone) from very toxic (IC50 < 1.56 µg/mL) to weakly toxic (IC50 280.00 µg/mL) and moderately toxic (IC50 = 46.00 µg/mL), respectively, after 72 h of treatment. These findings revealed that the optimized NGC has excellent potential and is a promising prospect in aerosolized delivery systems to treat lung cancer that warrants further investigation. Multidisciplinary Digital Publishing Institute 2021 Article PeerReviewed Mohamad Saimi, Norfatin Izzatie and Salim, Norazlinaliza and Ahmad, Noraini and Abdulmalek, Emilia and Abdul Rahman, Mohd Basyaruddin (2021) Aerosolized niosome formulation containing gemcitabine and cisplatin for lung cancer treatment: optimization, characterization and in vitro evaluation. Pharmaceutics, 13 (1). art. no. 59. pp. 1-19. ISSN 1999-4923 https://www.mdpi.com/1999-4923/13/1/59 10.3390/pharmaceutics13010059
spellingShingle Mohamad Saimi, Norfatin Izzatie
Salim, Norazlinaliza
Ahmad, Noraini
Abdulmalek, Emilia
Abdul Rahman, Mohd Basyaruddin
Aerosolized niosome formulation containing gemcitabine and cisplatin for lung cancer treatment: optimization, characterization and in vitro evaluation
title Aerosolized niosome formulation containing gemcitabine and cisplatin for lung cancer treatment: optimization, characterization and in vitro evaluation
title_full Aerosolized niosome formulation containing gemcitabine and cisplatin for lung cancer treatment: optimization, characterization and in vitro evaluation
title_fullStr Aerosolized niosome formulation containing gemcitabine and cisplatin for lung cancer treatment: optimization, characterization and in vitro evaluation
title_full_unstemmed Aerosolized niosome formulation containing gemcitabine and cisplatin for lung cancer treatment: optimization, characterization and in vitro evaluation
title_short Aerosolized niosome formulation containing gemcitabine and cisplatin for lung cancer treatment: optimization, characterization and in vitro evaluation
title_sort aerosolized niosome formulation containing gemcitabine and cisplatin for lung cancer treatment: optimization, characterization and in vitro evaluation
url http://psasir.upm.edu.my/id/eprint/95735/
http://psasir.upm.edu.my/id/eprint/95735/
http://psasir.upm.edu.my/id/eprint/95735/