Enzymatic Synthesis of Palm Based Fatty Monoethanolamide

Fatty monoethanolamides, derived from a reaction between triglyceride, palm kernel olein (PKL) or free fatty acids and primary amine alcohol, monoethanolamine (MEA) can be synthesised enzymatically, under milder conditions than the energy intensive chemical reaction. Mixture of palm based fatty m...

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Main Author: Abdul Rahim, Rashidah
Format: Thesis
Language:English
English
Published: 2002
Online Access:http://psasir.upm.edu.my/id/eprint/9523/
http://psasir.upm.edu.my/id/eprint/9523/1/FSAS_2002_53.pdf
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author Abdul Rahim, Rashidah
author_facet Abdul Rahim, Rashidah
author_sort Abdul Rahim, Rashidah
building UPM Institutional Repository
collection Online Access
description Fatty monoethanolamides, derived from a reaction between triglyceride, palm kernel olein (PKL) or free fatty acids and primary amine alcohol, monoethanolamine (MEA) can be synthesised enzymatically, under milder conditions than the energy intensive chemical reaction. Mixture of palm based fatty monoethanolamide was successfully obtained from the reaction between PKL and MEA in the presence of enzyme with better yield than the control experiment (without enzyme). The various individual fatty monoethanolamides were also obtained from the reaction between free fatty acids (ClOCIS) and MEA after the isolation and purification processes. The various fatty monoethanolamides were used as standards for the analysis of product mixture. Fatty monoethanolamides were characterised by infra-red spectroscopy (IR), thin-layer chromatography (TLC), nuclear magnetic resonance (NMR) and gas chromatography (GC). Gas chromatograph was also used for the quantitative analysis to calculate percent yield by using internal standard method.
first_indexed 2025-11-15T07:38:58Z
format Thesis
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institution Universiti Putra Malaysia
institution_category Local University
language English
English
last_indexed 2025-11-15T07:38:58Z
publishDate 2002
recordtype eprints
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spelling upm-95232024-03-06T08:49:53Z http://psasir.upm.edu.my/id/eprint/9523/ Enzymatic Synthesis of Palm Based Fatty Monoethanolamide Abdul Rahim, Rashidah Fatty monoethanolamides, derived from a reaction between triglyceride, palm kernel olein (PKL) or free fatty acids and primary amine alcohol, monoethanolamine (MEA) can be synthesised enzymatically, under milder conditions than the energy intensive chemical reaction. Mixture of palm based fatty monoethanolamide was successfully obtained from the reaction between PKL and MEA in the presence of enzyme with better yield than the control experiment (without enzyme). The various individual fatty monoethanolamides were also obtained from the reaction between free fatty acids (ClOCIS) and MEA after the isolation and purification processes. The various fatty monoethanolamides were used as standards for the analysis of product mixture. Fatty monoethanolamides were characterised by infra-red spectroscopy (IR), thin-layer chromatography (TLC), nuclear magnetic resonance (NMR) and gas chromatography (GC). Gas chromatograph was also used for the quantitative analysis to calculate percent yield by using internal standard method. 2002-07 Thesis NonPeerReviewed text en http://psasir.upm.edu.my/id/eprint/9523/1/FSAS_2002_53.pdf Abdul Rahim, Rashidah (2002) Enzymatic Synthesis of Palm Based Fatty Monoethanolamide. Doctoral thesis, Universiti Putra Malaysia. English
spellingShingle Abdul Rahim, Rashidah
Enzymatic Synthesis of Palm Based Fatty Monoethanolamide
title Enzymatic Synthesis of Palm Based Fatty Monoethanolamide
title_full Enzymatic Synthesis of Palm Based Fatty Monoethanolamide
title_fullStr Enzymatic Synthesis of Palm Based Fatty Monoethanolamide
title_full_unstemmed Enzymatic Synthesis of Palm Based Fatty Monoethanolamide
title_short Enzymatic Synthesis of Palm Based Fatty Monoethanolamide
title_sort enzymatic synthesis of palm based fatty monoethanolamide
url http://psasir.upm.edu.my/id/eprint/9523/
http://psasir.upm.edu.my/id/eprint/9523/1/FSAS_2002_53.pdf