Stabilization and release of palm tocotrienol emulsion fabricated using pH-sensitive calcium carbonate

Calcium carbonate (CaCO3) has been utilized as a pH-responsive component in various products. In this present work, palm tocotrienols-rich fraction (TRF) was successfully entrapped in a self-assembled oil-in-water (O/W) emulsion system by using CaCO3 as the stabilizer. The emulsion droplet size, vis...

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Main Authors: Phui, Yee Tan, Beng, Ti Tey, Eng, Seng Chan, Lai, Oi Ming, Hon, Weng Chang, Tai, Boon Tan, Liu, Yuanfa, Wang, Yong, Chin, Ping Tan
Format: Article
Language:English
Published: MDPI AG 2021
Online Access:http://psasir.upm.edu.my/id/eprint/95143/
http://psasir.upm.edu.my/id/eprint/95143/1/Stabilization%20and%20release%20of%20palm%20tocotrienol%20emulsion%20fabricated%20using%20pH-sensitive%20calcium%20carbonate.pdf
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author Phui, Yee Tan
Beng, Ti Tey
Eng, Seng Chan
Lai, Oi Ming
Hon, Weng Chang
Tai, Boon Tan
Liu, Yuanfa
Wang, Yong
Chin, Ping Tan
author_facet Phui, Yee Tan
Beng, Ti Tey
Eng, Seng Chan
Lai, Oi Ming
Hon, Weng Chang
Tai, Boon Tan
Liu, Yuanfa
Wang, Yong
Chin, Ping Tan
author_sort Phui, Yee Tan
building UPM Institutional Repository
collection Online Access
description Calcium carbonate (CaCO3) has been utilized as a pH-responsive component in various products. In this present work, palm tocotrienols-rich fraction (TRF) was successfully entrapped in a self-assembled oil-in-water (O/W) emulsion system by using CaCO3 as the stabilizer. The emulsion droplet size, viscosity and tocotrienols entrapment efficiency (EE) were strongly affected by varying the processing (homogenization speed and time) and formulation (CaCO3 and TRF concentrations) parameters. Our findings indicated that the combination of 5000 rpm homogenization speed, 15 min homogenization time, 0.75% CaCO3 concentration and 2% TRF concentration resulted in a high EE of tocotrienols (92.59–99.16%) and small droplet size (18.83 ± 1.36 µm). The resulting emulsion system readily released the entrapped tocotrienols across the pH range tested (pH 1–9); with relatively the highest release observed at pH 3. The current study presents a potential pH-sensitive emulsion system for the entrapment and delivery of palm tocotrienols.
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institution Universiti Putra Malaysia
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language English
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publishDate 2021
publisher MDPI AG
recordtype eprints
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spelling upm-951432023-01-04T09:04:52Z http://psasir.upm.edu.my/id/eprint/95143/ Stabilization and release of palm tocotrienol emulsion fabricated using pH-sensitive calcium carbonate Phui, Yee Tan Beng, Ti Tey Eng, Seng Chan Lai, Oi Ming Hon, Weng Chang Tai, Boon Tan Liu, Yuanfa Wang, Yong Chin, Ping Tan Calcium carbonate (CaCO3) has been utilized as a pH-responsive component in various products. In this present work, palm tocotrienols-rich fraction (TRF) was successfully entrapped in a self-assembled oil-in-water (O/W) emulsion system by using CaCO3 as the stabilizer. The emulsion droplet size, viscosity and tocotrienols entrapment efficiency (EE) were strongly affected by varying the processing (homogenization speed and time) and formulation (CaCO3 and TRF concentrations) parameters. Our findings indicated that the combination of 5000 rpm homogenization speed, 15 min homogenization time, 0.75% CaCO3 concentration and 2% TRF concentration resulted in a high EE of tocotrienols (92.59–99.16%) and small droplet size (18.83 ± 1.36 µm). The resulting emulsion system readily released the entrapped tocotrienols across the pH range tested (pH 1–9); with relatively the highest release observed at pH 3. The current study presents a potential pH-sensitive emulsion system for the entrapment and delivery of palm tocotrienols. MDPI AG 2021 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/95143/1/Stabilization%20and%20release%20of%20palm%20tocotrienol%20emulsion%20fabricated%20using%20pH-sensitive%20calcium%20carbonate.pdf Phui, Yee Tan and Beng, Ti Tey and Eng, Seng Chan and Lai, Oi Ming and Hon, Weng Chang and Tai, Boon Tan and Liu, Yuanfa and Wang, Yong and Chin, Ping Tan (2021) Stabilization and release of palm tocotrienol emulsion fabricated using pH-sensitive calcium carbonate. Foods, 10 (2). art. no. 358. pp. 1-15. ISSN 2304-8158 https://www.mdpi.com/2304-8158/10/2/358/htm 10.3390/foods10020358
spellingShingle Phui, Yee Tan
Beng, Ti Tey
Eng, Seng Chan
Lai, Oi Ming
Hon, Weng Chang
Tai, Boon Tan
Liu, Yuanfa
Wang, Yong
Chin, Ping Tan
Stabilization and release of palm tocotrienol emulsion fabricated using pH-sensitive calcium carbonate
title Stabilization and release of palm tocotrienol emulsion fabricated using pH-sensitive calcium carbonate
title_full Stabilization and release of palm tocotrienol emulsion fabricated using pH-sensitive calcium carbonate
title_fullStr Stabilization and release of palm tocotrienol emulsion fabricated using pH-sensitive calcium carbonate
title_full_unstemmed Stabilization and release of palm tocotrienol emulsion fabricated using pH-sensitive calcium carbonate
title_short Stabilization and release of palm tocotrienol emulsion fabricated using pH-sensitive calcium carbonate
title_sort stabilization and release of palm tocotrienol emulsion fabricated using ph-sensitive calcium carbonate
url http://psasir.upm.edu.my/id/eprint/95143/
http://psasir.upm.edu.my/id/eprint/95143/
http://psasir.upm.edu.my/id/eprint/95143/
http://psasir.upm.edu.my/id/eprint/95143/1/Stabilization%20and%20release%20of%20palm%20tocotrienol%20emulsion%20fabricated%20using%20pH-sensitive%20calcium%20carbonate.pdf