Synthesis and characterization of nickel zinc ferrite nanoparticles prepared by thermal treatment method

Cubic structured nickel-zinc ferrite nanoparticles Ni1-xZnxFe2O4(x = 0, 0.25, 0.5, 0.75 and 1) have been synthesized by thermal-treatment method. The Fourier trans form in infrared spectroscopy was used to confirm the presence of metal oxide bands at all temperatures and the removal of organic matte...

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Main Author: Poh, Lin Leng
Format: Thesis
Language:English
Published: 2013
Subjects:
Online Access:http://psasir.upm.edu.my/id/eprint/91218/
http://psasir.upm.edu.my/id/eprint/91218/1/FS%202013%2083%20IR.pdf
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author Poh, Lin Leng
author_facet Poh, Lin Leng
author_sort Poh, Lin Leng
building UPM Institutional Repository
collection Online Access
description Cubic structured nickel-zinc ferrite nanoparticles Ni1-xZnxFe2O4(x = 0, 0.25, 0.5, 0.75 and 1) have been synthesized by thermal-treatment method. The Fourier trans form in infrared spectroscopy was used to confirm the presence of metal oxide bands at all temperatures and the removal of organic matters at 873 K. The structure and particle size were characterized by X-ray powder diffraction and transmission electron microscopy. The magnetic properties were determined by vibrating sample magnetometer and electron paramagnetic resonance electron paramagnetic resonance at room temperature. By increasing the calcinations temperatures from 723 to 873 K showed an increase of the lattice parameter, the particles size, coercivity, saturation magnetization, peak to peak line width and the value of g- factor. When the concentration of Zinc increased; the lattice parameter increased while the particles size, coercivity, peak to peak line width and the value of g-factor decreased.
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format Thesis
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institution Universiti Putra Malaysia
institution_category Local University
language English
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publishDate 2013
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spelling upm-912182021-11-03T04:04:00Z http://psasir.upm.edu.my/id/eprint/91218/ Synthesis and characterization of nickel zinc ferrite nanoparticles prepared by thermal treatment method Poh, Lin Leng Cubic structured nickel-zinc ferrite nanoparticles Ni1-xZnxFe2O4(x = 0, 0.25, 0.5, 0.75 and 1) have been synthesized by thermal-treatment method. The Fourier trans form in infrared spectroscopy was used to confirm the presence of metal oxide bands at all temperatures and the removal of organic matters at 873 K. The structure and particle size were characterized by X-ray powder diffraction and transmission electron microscopy. The magnetic properties were determined by vibrating sample magnetometer and electron paramagnetic resonance electron paramagnetic resonance at room temperature. By increasing the calcinations temperatures from 723 to 873 K showed an increase of the lattice parameter, the particles size, coercivity, saturation magnetization, peak to peak line width and the value of g- factor. When the concentration of Zinc increased; the lattice parameter increased while the particles size, coercivity, peak to peak line width and the value of g-factor decreased. 2013-07 Thesis NonPeerReviewed text en http://psasir.upm.edu.my/id/eprint/91218/1/FS%202013%2083%20IR.pdf Poh, Lin Leng (2013) Synthesis and characterization of nickel zinc ferrite nanoparticles prepared by thermal treatment method. Masters thesis, Universiti Putra Malaysia. Thermal analysis
spellingShingle Thermal analysis
Poh, Lin Leng
Synthesis and characterization of nickel zinc ferrite nanoparticles prepared by thermal treatment method
title Synthesis and characterization of nickel zinc ferrite nanoparticles prepared by thermal treatment method
title_full Synthesis and characterization of nickel zinc ferrite nanoparticles prepared by thermal treatment method
title_fullStr Synthesis and characterization of nickel zinc ferrite nanoparticles prepared by thermal treatment method
title_full_unstemmed Synthesis and characterization of nickel zinc ferrite nanoparticles prepared by thermal treatment method
title_short Synthesis and characterization of nickel zinc ferrite nanoparticles prepared by thermal treatment method
title_sort synthesis and characterization of nickel zinc ferrite nanoparticles prepared by thermal treatment method
topic Thermal analysis
url http://psasir.upm.edu.my/id/eprint/91218/
http://psasir.upm.edu.my/id/eprint/91218/1/FS%202013%2083%20IR.pdf