Microwave-assisted green synthesis of Ag nanoparticles using leaves of Melia Dubia (Neem) and its antibacterial activities

The biosynthesis methods of nanosilver are of interest due to its low cost and environmental friendliness compared with chemical and physical methods. This study will conduct a green synthesis of nanosilver by decreasing the AgNO3 using leaf extract with the presence of stabilized microwave irradiat...

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Main Authors: Mudhafar, Mustafa, Zainol, Ismail, Jaafar, Che Nor Aiza, H. A., Alsailawi, Majhool, Alhussein Arkan
Format: Article
Language:English
Published: Akademia Baru Publishing 2020
Online Access:http://psasir.upm.edu.my/id/eprint/86759/
http://psasir.upm.edu.my/id/eprint/86759/1/Microwave%20assisted%20green.pdf
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author Mudhafar, Mustafa
Zainol, Ismail
Jaafar, Che Nor Aiza
H. A., Alsailawi
Majhool, Alhussein Arkan
author_facet Mudhafar, Mustafa
Zainol, Ismail
Jaafar, Che Nor Aiza
H. A., Alsailawi
Majhool, Alhussein Arkan
author_sort Mudhafar, Mustafa
building UPM Institutional Repository
collection Online Access
description The biosynthesis methods of nanosilver are of interest due to its low cost and environmental friendliness compared with chemical and physical methods. This study will conduct a green synthesis of nanosilver by decreasing the AgNO3 using leaf extract with the presence of stabilized microwave irradiation and collagen. Melia dubia leaves, and hydrolyzed fish scale collagen were utilized as reducing and stabilizing agents, respectively. Ag nanoparticles (AgNPs) were synthesized and characterized via Uv-Vis spectroscopy, scanning electron microscope (SEM) that attached with energydispersive X-ray, X-ray diffraction (XRD), and antibacterial activities. Results showed that the spherical shape of AgNPs was formed with particle size ranging from 72 nm and 100 nm. UV–vis analysis revealed that the absorbance peak was observed at 446 nm, which corresponded to AgNPs. XRD analysis confirmed the natural crystalline of AgNPs with a particle size of 84.8 nm. The antimicrobial analysis was conducted using Staphylococcus aureus and Escherichia coli as Gram-positive and -negative bacteria, respectively. Results showed the inhibition zone against both bacteria, which indicated excellent antimicrobial properties of the samples.
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institution Universiti Putra Malaysia
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language English
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publishDate 2020
publisher Akademia Baru Publishing
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spelling upm-867592021-11-16T03:20:31Z http://psasir.upm.edu.my/id/eprint/86759/ Microwave-assisted green synthesis of Ag nanoparticles using leaves of Melia Dubia (Neem) and its antibacterial activities Mudhafar, Mustafa Zainol, Ismail Jaafar, Che Nor Aiza H. A., Alsailawi Majhool, Alhussein Arkan The biosynthesis methods of nanosilver are of interest due to its low cost and environmental friendliness compared with chemical and physical methods. This study will conduct a green synthesis of nanosilver by decreasing the AgNO3 using leaf extract with the presence of stabilized microwave irradiation and collagen. Melia dubia leaves, and hydrolyzed fish scale collagen were utilized as reducing and stabilizing agents, respectively. Ag nanoparticles (AgNPs) were synthesized and characterized via Uv-Vis spectroscopy, scanning electron microscope (SEM) that attached with energydispersive X-ray, X-ray diffraction (XRD), and antibacterial activities. Results showed that the spherical shape of AgNPs was formed with particle size ranging from 72 nm and 100 nm. UV–vis analysis revealed that the absorbance peak was observed at 446 nm, which corresponded to AgNPs. XRD analysis confirmed the natural crystalline of AgNPs with a particle size of 84.8 nm. The antimicrobial analysis was conducted using Staphylococcus aureus and Escherichia coli as Gram-positive and -negative bacteria, respectively. Results showed the inhibition zone against both bacteria, which indicated excellent antimicrobial properties of the samples. Akademia Baru Publishing 2020-01 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/86759/1/Microwave%20assisted%20green.pdf Mudhafar, Mustafa and Zainol, Ismail and Jaafar, Che Nor Aiza and H. A., Alsailawi and Majhool, Alhussein Arkan (2020) Microwave-assisted green synthesis of Ag nanoparticles using leaves of Melia Dubia (Neem) and its antibacterial activities. Journal of Advanced Research in Fluid Mechanics and Thermal Sciences, 65 (1). 121 - 129. ISSN 2289 - 7879 https://www.akademiabaru.com/submit/index.php/arfmts/article/view/2782
spellingShingle Mudhafar, Mustafa
Zainol, Ismail
Jaafar, Che Nor Aiza
H. A., Alsailawi
Majhool, Alhussein Arkan
Microwave-assisted green synthesis of Ag nanoparticles using leaves of Melia Dubia (Neem) and its antibacterial activities
title Microwave-assisted green synthesis of Ag nanoparticles using leaves of Melia Dubia (Neem) and its antibacterial activities
title_full Microwave-assisted green synthesis of Ag nanoparticles using leaves of Melia Dubia (Neem) and its antibacterial activities
title_fullStr Microwave-assisted green synthesis of Ag nanoparticles using leaves of Melia Dubia (Neem) and its antibacterial activities
title_full_unstemmed Microwave-assisted green synthesis of Ag nanoparticles using leaves of Melia Dubia (Neem) and its antibacterial activities
title_short Microwave-assisted green synthesis of Ag nanoparticles using leaves of Melia Dubia (Neem) and its antibacterial activities
title_sort microwave-assisted green synthesis of ag nanoparticles using leaves of melia dubia (neem) and its antibacterial activities
url http://psasir.upm.edu.my/id/eprint/86759/
http://psasir.upm.edu.my/id/eprint/86759/
http://psasir.upm.edu.my/id/eprint/86759/1/Microwave%20assisted%20green.pdf