Study of dissolved copper (ii) speciation at Pulau Pangkor, Perak, Peninsular Malaysia

The profile of seawater samples was analyzed from a few selected stations at Pulau Pangkor, Perak for dissolved copper speciation analysis in order to determine the concentration level of toxic cupric ions (Cu ²⁺ ) in seawater. The concentration of natural organic Cu(II)-ligand binding (CuL) and its...

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Main Authors: Godon, Edrianna, Mohamed, Khairul Nizam, Yusoff, M. K., Surimin, A., Gani, M. A., Wahab, Z. A.
Format: Article
Language:English
Published: Forestry Department Peninsular Malaysia 2019
Online Access:http://psasir.upm.edu.my/id/eprint/82289/
http://psasir.upm.edu.my/id/eprint/82289/1/Study%20of%20dissolved%20copper%20%28ii%29%20speciation%20at%20Pulau%20Pangkor%2C%20Perak%2C%20Peninsular%20Malaysia.pdf
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author Godon, Edrianna
Mohamed, Khairul Nizam
Yusoff, M. K.
Surimin, A.
Gani, M. A.
Wahab, Z. A.
author_facet Godon, Edrianna
Mohamed, Khairul Nizam
Yusoff, M. K.
Surimin, A.
Gani, M. A.
Wahab, Z. A.
author_sort Godon, Edrianna
building UPM Institutional Repository
collection Online Access
description The profile of seawater samples was analyzed from a few selected stations at Pulau Pangkor, Perak for dissolved copper speciation analysis in order to determine the concentration level of toxic cupric ions (Cu ²⁺ ) in seawater. The concentration of natural organic Cu(II)-ligand binding (CuL) and its conditional stability constant (Log K’CuL) in each sample was determined by using competitive ligand exchange–adsorptive cathodic stripping voltammetry (CLE-AdCSV) method with salicylaldoxime (SA) as competitive ligand. Our present data have recorded a total dissolved Cu concentration [dCu] ranged between 3.14–7.12 nM and 3.10–9.11 nM at a surface layer and at 15-meter depth, respectively. An organic ligand concentration [CuL] at the surface layer ranges between 4.41-13.25 nM, with its conditional stability constants (log K'CuL) between 11.55-12.17. However, at 15-meter depth, the [CuL] was recorded between 5.90-11.14 nM with log K'CuL ranged 10.93-12.84. On the other hands, a free Cu ion activity, pCu (pCu = −log[Cu ²⁺ ]), was ranged from 8.97-10.35, and was slightly less compared to the pCu values that have been recorded in other coastal waters (>12). The free [Cu ²⁺ ] was ranged between 10 ⁻⁹ –10 ⁻¹¹ pM, which was slightly below the toxicity threshold (10 ⁻⁸ pM). This initial study has suggested that dCu was largely complexed by organic ligands (>99.6%), both strong organic ligand (L1: LogK>12) at surface and weak organic ligand (L2: LogK<11) at the deeper layer. The presence of these two classes of ligands have buffering the free Cu ²⁺ ions, yielding a non-toxic Cu to the microorganisms.
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publisher Forestry Department Peninsular Malaysia
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spelling upm-822892020-10-16T20:39:04Z http://psasir.upm.edu.my/id/eprint/82289/ Study of dissolved copper (ii) speciation at Pulau Pangkor, Perak, Peninsular Malaysia Godon, Edrianna Mohamed, Khairul Nizam Yusoff, M. K. Surimin, A. Gani, M. A. Wahab, Z. A. The profile of seawater samples was analyzed from a few selected stations at Pulau Pangkor, Perak for dissolved copper speciation analysis in order to determine the concentration level of toxic cupric ions (Cu ²⁺ ) in seawater. The concentration of natural organic Cu(II)-ligand binding (CuL) and its conditional stability constant (Log K’CuL) in each sample was determined by using competitive ligand exchange–adsorptive cathodic stripping voltammetry (CLE-AdCSV) method with salicylaldoxime (SA) as competitive ligand. Our present data have recorded a total dissolved Cu concentration [dCu] ranged between 3.14–7.12 nM and 3.10–9.11 nM at a surface layer and at 15-meter depth, respectively. An organic ligand concentration [CuL] at the surface layer ranges between 4.41-13.25 nM, with its conditional stability constants (log K'CuL) between 11.55-12.17. However, at 15-meter depth, the [CuL] was recorded between 5.90-11.14 nM with log K'CuL ranged 10.93-12.84. On the other hands, a free Cu ion activity, pCu (pCu = −log[Cu ²⁺ ]), was ranged from 8.97-10.35, and was slightly less compared to the pCu values that have been recorded in other coastal waters (>12). The free [Cu ²⁺ ] was ranged between 10 ⁻⁹ –10 ⁻¹¹ pM, which was slightly below the toxicity threshold (10 ⁻⁸ pM). This initial study has suggested that dCu was largely complexed by organic ligands (>99.6%), both strong organic ligand (L1: LogK>12) at surface and weak organic ligand (L2: LogK<11) at the deeper layer. The presence of these two classes of ligands have buffering the free Cu ²⁺ ions, yielding a non-toxic Cu to the microorganisms. Forestry Department Peninsular Malaysia 2019 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/82289/1/Study%20of%20dissolved%20copper%20%28ii%29%20speciation%20at%20Pulau%20Pangkor%2C%20Perak%2C%20Peninsular%20Malaysia.pdf Godon, Edrianna and Mohamed, Khairul Nizam and Yusoff, M. K. and Surimin, A. and Gani, M. A. and Wahab, Z. A. (2019) Study of dissolved copper (ii) speciation at Pulau Pangkor, Perak, Peninsular Malaysia. Malaysian Forester, 82 (1). pp. 27-36. ISSN 0302-2935
spellingShingle Godon, Edrianna
Mohamed, Khairul Nizam
Yusoff, M. K.
Surimin, A.
Gani, M. A.
Wahab, Z. A.
Study of dissolved copper (ii) speciation at Pulau Pangkor, Perak, Peninsular Malaysia
title Study of dissolved copper (ii) speciation at Pulau Pangkor, Perak, Peninsular Malaysia
title_full Study of dissolved copper (ii) speciation at Pulau Pangkor, Perak, Peninsular Malaysia
title_fullStr Study of dissolved copper (ii) speciation at Pulau Pangkor, Perak, Peninsular Malaysia
title_full_unstemmed Study of dissolved copper (ii) speciation at Pulau Pangkor, Perak, Peninsular Malaysia
title_short Study of dissolved copper (ii) speciation at Pulau Pangkor, Perak, Peninsular Malaysia
title_sort study of dissolved copper (ii) speciation at pulau pangkor, perak, peninsular malaysia
url http://psasir.upm.edu.my/id/eprint/82289/
http://psasir.upm.edu.my/id/eprint/82289/1/Study%20of%20dissolved%20copper%20%28ii%29%20speciation%20at%20Pulau%20Pangkor%2C%20Perak%2C%20Peninsular%20Malaysia.pdf