Green formation of spherical and dendritic silver nanostructures under microwave irradiation without reducing agent

The rapid and green formation of spherical and dendritic silver nanostructures based on microwave irradiation time was investigated. Silver nanoparticles were successfully fabricated by reduction of Ag+ in a water medium and using polyvinylpyrrolidone (PVP) as the stabilizing agent and without the u...

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Main Authors: Noroozi, Monir, Zakaria, Azmi, Abd. Moksin, Mohd Maarof, Abdul Wahab, Zaidan, Abedini, Alam
Format: Article
Language:English
Published: MDPI 2012
Online Access:http://psasir.upm.edu.my/id/eprint/77984/
http://psasir.upm.edu.my/id/eprint/77984/1/77984.pdf
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author Noroozi, Monir
Zakaria, Azmi
Abd. Moksin, Mohd Maarof
Abdul Wahab, Zaidan
Abedini, Alam
author_facet Noroozi, Monir
Zakaria, Azmi
Abd. Moksin, Mohd Maarof
Abdul Wahab, Zaidan
Abedini, Alam
author_sort Noroozi, Monir
building UPM Institutional Repository
collection Online Access
description The rapid and green formation of spherical and dendritic silver nanostructures based on microwave irradiation time was investigated. Silver nanoparticles were successfully fabricated by reduction of Ag+ in a water medium and using polyvinylpyrrolidone (PVP) as the stabilizing agent and without the use of any other reducing agent, and were compared with those synthesized by conventional heating method. UV–vis absorption spectrometry, transmission electron microscopy (TEM), atomic absorption spectroscopy (AAS) and photon correlation spectroscopy (PCS) measurements, indicated that increasing the irradiation time enhanced the concentration of silver nanoparticles and slightly increased the particle size. There was a lack of large silver nanoparticles at a high concentration, but interestingly, the formation and growth of silver dendrite nanostructures appeared. Compared to conventional heating methods, the silver nanoparticle suspension produced by irradiated microwaves was more stable over a six-month period in aqueous solution without any signs of precipitation.
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spelling upm-779842020-06-01T03:11:46Z http://psasir.upm.edu.my/id/eprint/77984/ Green formation of spherical and dendritic silver nanostructures under microwave irradiation without reducing agent Noroozi, Monir Zakaria, Azmi Abd. Moksin, Mohd Maarof Abdul Wahab, Zaidan Abedini, Alam The rapid and green formation of spherical and dendritic silver nanostructures based on microwave irradiation time was investigated. Silver nanoparticles were successfully fabricated by reduction of Ag+ in a water medium and using polyvinylpyrrolidone (PVP) as the stabilizing agent and without the use of any other reducing agent, and were compared with those synthesized by conventional heating method. UV–vis absorption spectrometry, transmission electron microscopy (TEM), atomic absorption spectroscopy (AAS) and photon correlation spectroscopy (PCS) measurements, indicated that increasing the irradiation time enhanced the concentration of silver nanoparticles and slightly increased the particle size. There was a lack of large silver nanoparticles at a high concentration, but interestingly, the formation and growth of silver dendrite nanostructures appeared. Compared to conventional heating methods, the silver nanoparticle suspension produced by irradiated microwaves was more stable over a six-month period in aqueous solution without any signs of precipitation. MDPI 2012 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/77984/1/77984.pdf Noroozi, Monir and Zakaria, Azmi and Abd. Moksin, Mohd Maarof and Abdul Wahab, Zaidan and Abedini, Alam (2012) Green formation of spherical and dendritic silver nanostructures under microwave irradiation without reducing agent. International Journal of Molecular Sciences, 13 (7). pp. 8086-8096. ISSN 1661-6596; ESSN: 1422-0067 https://www.mdpi.com/1422-0067/13/7/8086 10.3390/ijms13078086
spellingShingle Noroozi, Monir
Zakaria, Azmi
Abd. Moksin, Mohd Maarof
Abdul Wahab, Zaidan
Abedini, Alam
Green formation of spherical and dendritic silver nanostructures under microwave irradiation without reducing agent
title Green formation of spherical and dendritic silver nanostructures under microwave irradiation without reducing agent
title_full Green formation of spherical and dendritic silver nanostructures under microwave irradiation without reducing agent
title_fullStr Green formation of spherical and dendritic silver nanostructures under microwave irradiation without reducing agent
title_full_unstemmed Green formation of spherical and dendritic silver nanostructures under microwave irradiation without reducing agent
title_short Green formation of spherical and dendritic silver nanostructures under microwave irradiation without reducing agent
title_sort green formation of spherical and dendritic silver nanostructures under microwave irradiation without reducing agent
url http://psasir.upm.edu.my/id/eprint/77984/
http://psasir.upm.edu.my/id/eprint/77984/
http://psasir.upm.edu.my/id/eprint/77984/
http://psasir.upm.edu.my/id/eprint/77984/1/77984.pdf