Optimization of mechanical properties for polyoxymethylene/glass fiber/polytetrafluoroethylene composites using response surface methodology

This paper investigated the effects of polytetrafluoroethylene (PTFE) micro-particles on mechanical properties of polyoxymethylene (POM) composites. Since PTFE is immiscible with most polymers, the surface was etched using sodium naphthalene salt in tetrahydrofuran to increase its surface energy. Th...

Full description

Bibliographic Details
Main Authors: Kunnan Singh, Jasbir Singh, Ching, Yern Chee, Abdullah, Luqman Chuah, Ching, Kuan Yong, Razali, Shaifulazuar, Seng, Neon Gan
Format: Article
Language:English
Published: M D P I AG 2018
Online Access:http://psasir.upm.edu.my/id/eprint/75162/
http://psasir.upm.edu.my/id/eprint/75162/1/Optimization%20of%20mechanical%20properties%20for%20polyoxymethylene.pdf
_version_ 1848857619612041216
author Kunnan Singh, Jasbir Singh
Ching, Yern Chee
Abdullah, Luqman Chuah
Ching, Kuan Yong
Razali, Shaifulazuar
Seng, Neon Gan
author_facet Kunnan Singh, Jasbir Singh
Ching, Yern Chee
Abdullah, Luqman Chuah
Ching, Kuan Yong
Razali, Shaifulazuar
Seng, Neon Gan
author_sort Kunnan Singh, Jasbir Singh
building UPM Institutional Repository
collection Online Access
description This paper investigated the effects of polytetrafluoroethylene (PTFE) micro-particles on mechanical properties of polyoxymethylene (POM) composites. Since PTFE is immiscible with most polymers, the surface was etched using sodium naphthalene salt in tetrahydrofuran to increase its surface energy. The effects of two variables, namely PTFE content and PTFE etch time, on the mechanical properties of the composite were studied. Experiments were designed in accordance to response surface methodology (RSM) using central composite design (CCD). Samples were prepared with different compositions of PTFE (1.7, 4.0, 9.5, 15.0, or 17.3 wt %) at different PTFE etch times (2.9, 5.0, 10.0, 15.0, or 17.1 min). Four mechanical properties of the POM/GF/PTFE composites, that is, strength, stiffness, toughness, and hardness, were characterized as a function of two studied variables. The dependency of these mechanical properties on the PTFE etch conditions was analyzed using analysis of variance (ANOVA). Overall desirability, D global index, was computed based on the combination of these mechanical properties for POM/GF/PTFE composites. The D global index was found to be 87.5%, when PTFE content and PTFE etch time were 6.5% and 10 min, respectively. Good correlation between experimental and RSM models was obtained using normal probability plots.
first_indexed 2025-11-15T12:00:26Z
format Article
id upm-75162
institution Universiti Putra Malaysia
institution_category Local University
language English
last_indexed 2025-11-15T12:00:26Z
publishDate 2018
publisher M D P I AG
recordtype eprints
repository_type Digital Repository
spelling upm-751622019-11-27T04:08:24Z http://psasir.upm.edu.my/id/eprint/75162/ Optimization of mechanical properties for polyoxymethylene/glass fiber/polytetrafluoroethylene composites using response surface methodology Kunnan Singh, Jasbir Singh Ching, Yern Chee Abdullah, Luqman Chuah Ching, Kuan Yong Razali, Shaifulazuar Seng, Neon Gan This paper investigated the effects of polytetrafluoroethylene (PTFE) micro-particles on mechanical properties of polyoxymethylene (POM) composites. Since PTFE is immiscible with most polymers, the surface was etched using sodium naphthalene salt in tetrahydrofuran to increase its surface energy. The effects of two variables, namely PTFE content and PTFE etch time, on the mechanical properties of the composite were studied. Experiments were designed in accordance to response surface methodology (RSM) using central composite design (CCD). Samples were prepared with different compositions of PTFE (1.7, 4.0, 9.5, 15.0, or 17.3 wt %) at different PTFE etch times (2.9, 5.0, 10.0, 15.0, or 17.1 min). Four mechanical properties of the POM/GF/PTFE composites, that is, strength, stiffness, toughness, and hardness, were characterized as a function of two studied variables. The dependency of these mechanical properties on the PTFE etch conditions was analyzed using analysis of variance (ANOVA). Overall desirability, D global index, was computed based on the combination of these mechanical properties for POM/GF/PTFE composites. The D global index was found to be 87.5%, when PTFE content and PTFE etch time were 6.5% and 10 min, respectively. Good correlation between experimental and RSM models was obtained using normal probability plots. M D P I AG 2018 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/75162/1/Optimization%20of%20mechanical%20properties%20for%20polyoxymethylene.pdf Kunnan Singh, Jasbir Singh and Ching, Yern Chee and Abdullah, Luqman Chuah and Ching, Kuan Yong and Razali, Shaifulazuar and Seng, Neon Gan (2018) Optimization of mechanical properties for polyoxymethylene/glass fiber/polytetrafluoroethylene composites using response surface methodology. Polymers, 10 (3). pp. 1-25. ISSN 2073-4360 https://www.mdpi.com/2073-4360/10/3/338 10.3390/polym10030338
spellingShingle Kunnan Singh, Jasbir Singh
Ching, Yern Chee
Abdullah, Luqman Chuah
Ching, Kuan Yong
Razali, Shaifulazuar
Seng, Neon Gan
Optimization of mechanical properties for polyoxymethylene/glass fiber/polytetrafluoroethylene composites using response surface methodology
title Optimization of mechanical properties for polyoxymethylene/glass fiber/polytetrafluoroethylene composites using response surface methodology
title_full Optimization of mechanical properties for polyoxymethylene/glass fiber/polytetrafluoroethylene composites using response surface methodology
title_fullStr Optimization of mechanical properties for polyoxymethylene/glass fiber/polytetrafluoroethylene composites using response surface methodology
title_full_unstemmed Optimization of mechanical properties for polyoxymethylene/glass fiber/polytetrafluoroethylene composites using response surface methodology
title_short Optimization of mechanical properties for polyoxymethylene/glass fiber/polytetrafluoroethylene composites using response surface methodology
title_sort optimization of mechanical properties for polyoxymethylene/glass fiber/polytetrafluoroethylene composites using response surface methodology
url http://psasir.upm.edu.my/id/eprint/75162/
http://psasir.upm.edu.my/id/eprint/75162/
http://psasir.upm.edu.my/id/eprint/75162/
http://psasir.upm.edu.my/id/eprint/75162/1/Optimization%20of%20mechanical%20properties%20for%20polyoxymethylene.pdf