Efficient waste Gallus domesticus shell derived calcium-based catalyst for biodiesel production

In this study, waste shells derived calcium-based catalysts were synthesized via wet-impregnation process in the presence of Mo-Zr mixed salt. The synthesized catalysts were characterized using CO2-TPD, XRD, BET surface measurement, SEM and EDX spectrometry, respectively. This heterogeneous catalyst...

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Main Authors: Mansir, Nasar, Teo, Siow Hwa, Rashid, Umer, Yap, Taufiq Yun Hin
Format: Article
Language:English
Published: Elsevier 2018
Online Access:http://psasir.upm.edu.my/id/eprint/72538/
http://psasir.upm.edu.my/id/eprint/72538/1/Efficient%20waste%20Gallus%20domesticus%20.pdf
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author Mansir, Nasar
Teo, Siow Hwa
Rashid, Umer
Yap, Taufiq Yun Hin
author_facet Mansir, Nasar
Teo, Siow Hwa
Rashid, Umer
Yap, Taufiq Yun Hin
author_sort Mansir, Nasar
building UPM Institutional Repository
collection Online Access
description In this study, waste shells derived calcium-based catalysts were synthesized via wet-impregnation process in the presence of Mo-Zr mixed salt. The synthesized catalysts were characterized using CO2-TPD, XRD, BET surface measurement, SEM and EDX spectrometry, respectively. This heterogeneous catalyst was used to synthesize biodiesel via transesterification of waste cooking palm oil (WCPO) to fatty acid methyl ester in the presence of methanol. The catalyst demonstrated a superior catalytic performance in transesterification reaction, yielded 90.1% in 3 h. Reusability of this waste shell derived catalyst was examined and results showed that the prepared catalysts are able to be reused up to 3 times with yield of more than 70% after the third cycles. Therefore, this new modified calcium-based catalyst exhibited outstanding activity and durability in the synthesis of biodiesel. The as-synthesized catalyst is recyclable and reusable, which successfully reduces the biodiesel production cost.
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institution Universiti Putra Malaysia
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publishDate 2018
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spelling upm-725382020-10-22T11:16:31Z http://psasir.upm.edu.my/id/eprint/72538/ Efficient waste Gallus domesticus shell derived calcium-based catalyst for biodiesel production Mansir, Nasar Teo, Siow Hwa Rashid, Umer Yap, Taufiq Yun Hin In this study, waste shells derived calcium-based catalysts were synthesized via wet-impregnation process in the presence of Mo-Zr mixed salt. The synthesized catalysts were characterized using CO2-TPD, XRD, BET surface measurement, SEM and EDX spectrometry, respectively. This heterogeneous catalyst was used to synthesize biodiesel via transesterification of waste cooking palm oil (WCPO) to fatty acid methyl ester in the presence of methanol. The catalyst demonstrated a superior catalytic performance in transesterification reaction, yielded 90.1% in 3 h. Reusability of this waste shell derived catalyst was examined and results showed that the prepared catalysts are able to be reused up to 3 times with yield of more than 70% after the third cycles. Therefore, this new modified calcium-based catalyst exhibited outstanding activity and durability in the synthesis of biodiesel. The as-synthesized catalyst is recyclable and reusable, which successfully reduces the biodiesel production cost. Elsevier 2018-01 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/72538/1/Efficient%20waste%20Gallus%20domesticus%20.pdf Mansir, Nasar and Teo, Siow Hwa and Rashid, Umer and Yap, Taufiq Yun Hin (2018) Efficient waste Gallus domesticus shell derived calcium-based catalyst for biodiesel production. Fuel, 211. 67 - 75. ISSN 0016-2361 https://www.sciencedirect.com/science/article/abs/pii/S0016236117311146 10.1016/j.fuel.2017.09.014
spellingShingle Mansir, Nasar
Teo, Siow Hwa
Rashid, Umer
Yap, Taufiq Yun Hin
Efficient waste Gallus domesticus shell derived calcium-based catalyst for biodiesel production
title Efficient waste Gallus domesticus shell derived calcium-based catalyst for biodiesel production
title_full Efficient waste Gallus domesticus shell derived calcium-based catalyst for biodiesel production
title_fullStr Efficient waste Gallus domesticus shell derived calcium-based catalyst for biodiesel production
title_full_unstemmed Efficient waste Gallus domesticus shell derived calcium-based catalyst for biodiesel production
title_short Efficient waste Gallus domesticus shell derived calcium-based catalyst for biodiesel production
title_sort efficient waste gallus domesticus shell derived calcium-based catalyst for biodiesel production
url http://psasir.upm.edu.my/id/eprint/72538/
http://psasir.upm.edu.my/id/eprint/72538/
http://psasir.upm.edu.my/id/eprint/72538/
http://psasir.upm.edu.my/id/eprint/72538/1/Efficient%20waste%20Gallus%20domesticus%20.pdf