Pectin characterization and factors affecting pectin extraction from Citrus grandis L. Osbeck (Pummelo) peels

Microwave-assisted extraction (MAE) and ultrasound-assisted extraction (UAE) have been developed to increase the yield and quality of various plantbased constituents with shorter time of extraction. This research aimed to study the effect of four (4) factors towards the quantity and quality of pecti...

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Main Author: Ismail @ Khori, Noor Jannah Firdouse
Format: Thesis
Language:English
Published: 2015
Online Access:http://psasir.upm.edu.my/id/eprint/64746/
http://psasir.upm.edu.my/id/eprint/64746/1/FSTM%202015%2014IR.pdf
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author Ismail @ Khori, Noor Jannah Firdouse
author_facet Ismail @ Khori, Noor Jannah Firdouse
author_sort Ismail @ Khori, Noor Jannah Firdouse
building UPM Institutional Repository
collection Online Access
description Microwave-assisted extraction (MAE) and ultrasound-assisted extraction (UAE) have been developed to increase the yield and quality of various plantbased constituents with shorter time of extraction. This research aimed to study the effect of four (4) factors towards the quantity and quality of pectin extracted from pummelo peels, using two (2) level factorial designs, utilizing UAE, MAE and water bath extraction (WBE) methods. Factors manipulated were time, pH, sample-to-solvent ratio and temperature. MAE, UAE and conventional methods were able to extract pectin up to 78.98 % in a minute, 38.7% in 10 minutes and 68.26% in 30 minutes, respectively. Pectin from MAE method significantly has the highest DE (60.41 ± 0.37) followed by WBE method (55.99 ± 1.22) and UAE method (54.64 ± 0.503). The galacturonic acid (GalA) content of pectin extracted using MAE was significantly the highest (82.71% ± 1.77) compared to UAE and WBE methods (67.37 ± 1.88 and 55.99 ± 1.22 respectively). This study showed that pummelo peels of Ledang variety contained high methoxyl pectin (DE > 50%) with GalA content of more than 65%. MAE was the most efficient method to produce high methoxyl pectin with high content of GalA.
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spelling upm-647462018-09-06T04:53:57Z http://psasir.upm.edu.my/id/eprint/64746/ Pectin characterization and factors affecting pectin extraction from Citrus grandis L. Osbeck (Pummelo) peels Ismail @ Khori, Noor Jannah Firdouse Microwave-assisted extraction (MAE) and ultrasound-assisted extraction (UAE) have been developed to increase the yield and quality of various plantbased constituents with shorter time of extraction. This research aimed to study the effect of four (4) factors towards the quantity and quality of pectin extracted from pummelo peels, using two (2) level factorial designs, utilizing UAE, MAE and water bath extraction (WBE) methods. Factors manipulated were time, pH, sample-to-solvent ratio and temperature. MAE, UAE and conventional methods were able to extract pectin up to 78.98 % in a minute, 38.7% in 10 minutes and 68.26% in 30 minutes, respectively. Pectin from MAE method significantly has the highest DE (60.41 ± 0.37) followed by WBE method (55.99 ± 1.22) and UAE method (54.64 ± 0.503). The galacturonic acid (GalA) content of pectin extracted using MAE was significantly the highest (82.71% ± 1.77) compared to UAE and WBE methods (67.37 ± 1.88 and 55.99 ± 1.22 respectively). This study showed that pummelo peels of Ledang variety contained high methoxyl pectin (DE > 50%) with GalA content of more than 65%. MAE was the most efficient method to produce high methoxyl pectin with high content of GalA. 2015-04 Thesis NonPeerReviewed text en http://psasir.upm.edu.my/id/eprint/64746/1/FSTM%202015%2014IR.pdf Ismail @ Khori, Noor Jannah Firdouse (2015) Pectin characterization and factors affecting pectin extraction from Citrus grandis L. Osbeck (Pummelo) peels. Masters thesis, Universiti Putra Malaysia.
spellingShingle Ismail @ Khori, Noor Jannah Firdouse
Pectin characterization and factors affecting pectin extraction from Citrus grandis L. Osbeck (Pummelo) peels
title Pectin characterization and factors affecting pectin extraction from Citrus grandis L. Osbeck (Pummelo) peels
title_full Pectin characterization and factors affecting pectin extraction from Citrus grandis L. Osbeck (Pummelo) peels
title_fullStr Pectin characterization and factors affecting pectin extraction from Citrus grandis L. Osbeck (Pummelo) peels
title_full_unstemmed Pectin characterization and factors affecting pectin extraction from Citrus grandis L. Osbeck (Pummelo) peels
title_short Pectin characterization and factors affecting pectin extraction from Citrus grandis L. Osbeck (Pummelo) peels
title_sort pectin characterization and factors affecting pectin extraction from citrus grandis l. osbeck (pummelo) peels
url http://psasir.upm.edu.my/id/eprint/64746/
http://psasir.upm.edu.my/id/eprint/64746/1/FSTM%202015%2014IR.pdf