Hydrothermal growth of ZnO nanorods for photoelectrochemical cell: effect of growth time and temperature

A thin layer of zinc oxide (ZnO) film was predeposited onto indium tin oxide (ITO) glass via dip-coating method followed by hydrothermal growth. Pretreated ITO glasses were dipped into precursor solution containing zinc acetate, diethanolamine (DEA) and ethanol. After three layers of ZnO seed layers...

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Main Authors: Mohd Fudzi, Laimy, Zainal, Zulkarnain, Lim, Hong Ngee
Format: Conference or Workshop Item
Language:English
Published: 2017
Online Access:http://psasir.upm.edu.my/id/eprint/64424/
http://psasir.upm.edu.my/id/eprint/64424/1/MST%20poster%20111117%2026.pdf
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author Mohd Fudzi, Laimy
Zainal, Zulkarnain
Lim, Hong Ngee
author_facet Mohd Fudzi, Laimy
Zainal, Zulkarnain
Lim, Hong Ngee
author_sort Mohd Fudzi, Laimy
building UPM Institutional Repository
collection Online Access
description A thin layer of zinc oxide (ZnO) film was predeposited onto indium tin oxide (ITO) glass via dip-coating method followed by hydrothermal growth. Pretreated ITO glasses were dipped into precursor solution containing zinc acetate, diethanolamine (DEA) and ethanol. After three layers of ZnO seed layers were deposited, the samples were annealed at 350 °C. This was followed by 4 hours hydrothermal growth in silicon oil bath at two different temperatures, 90 °C and 120 °C. The morphological, structural and compositional properties of the prepared films were characterized using field emission scanning electron microscopy (FESEM), energy dispersive x-ray spectroscopy (EDX) and ultraviolet-visible spectroscopy (UV-Vis). Current density and photoelectrochemical conversion efficiencies were evaluated by in electrolyte mixture of sodium sulfide (Na2S) and sodium sulfite (Na2SO3) alkaline aqueous solution.
first_indexed 2025-11-15T11:18:46Z
format Conference or Workshop Item
id upm-64424
institution Universiti Putra Malaysia
institution_category Local University
language English
last_indexed 2025-11-15T11:18:46Z
publishDate 2017
recordtype eprints
repository_type Digital Repository
spelling upm-644242018-07-05T09:31:16Z http://psasir.upm.edu.my/id/eprint/64424/ Hydrothermal growth of ZnO nanorods for photoelectrochemical cell: effect of growth time and temperature Mohd Fudzi, Laimy Zainal, Zulkarnain Lim, Hong Ngee A thin layer of zinc oxide (ZnO) film was predeposited onto indium tin oxide (ITO) glass via dip-coating method followed by hydrothermal growth. Pretreated ITO glasses were dipped into precursor solution containing zinc acetate, diethanolamine (DEA) and ethanol. After three layers of ZnO seed layers were deposited, the samples were annealed at 350 °C. This was followed by 4 hours hydrothermal growth in silicon oil bath at two different temperatures, 90 °C and 120 °C. The morphological, structural and compositional properties of the prepared films were characterized using field emission scanning electron microscopy (FESEM), energy dispersive x-ray spectroscopy (EDX) and ultraviolet-visible spectroscopy (UV-Vis). Current density and photoelectrochemical conversion efficiencies were evaluated by in electrolyte mixture of sodium sulfide (Na2S) and sodium sulfite (Na2SO3) alkaline aqueous solution. 2017 Conference or Workshop Item PeerReviewed text en http://psasir.upm.edu.my/id/eprint/64424/1/MST%20poster%20111117%2026.pdf Mohd Fudzi, Laimy and Zainal, Zulkarnain and Lim, Hong Ngee (2017) Hydrothermal growth of ZnO nanorods for photoelectrochemical cell: effect of growth time and temperature. In: 5th International Symposium on Applied Engineering and Sciences (SAES2017), 14-15 Nov. 2017, Universiti Putra Malaysia. (p. 26).
spellingShingle Mohd Fudzi, Laimy
Zainal, Zulkarnain
Lim, Hong Ngee
Hydrothermal growth of ZnO nanorods for photoelectrochemical cell: effect of growth time and temperature
title Hydrothermal growth of ZnO nanorods for photoelectrochemical cell: effect of growth time and temperature
title_full Hydrothermal growth of ZnO nanorods for photoelectrochemical cell: effect of growth time and temperature
title_fullStr Hydrothermal growth of ZnO nanorods for photoelectrochemical cell: effect of growth time and temperature
title_full_unstemmed Hydrothermal growth of ZnO nanorods for photoelectrochemical cell: effect of growth time and temperature
title_short Hydrothermal growth of ZnO nanorods for photoelectrochemical cell: effect of growth time and temperature
title_sort hydrothermal growth of zno nanorods for photoelectrochemical cell: effect of growth time and temperature
url http://psasir.upm.edu.my/id/eprint/64424/
http://psasir.upm.edu.my/id/eprint/64424/1/MST%20poster%20111117%2026.pdf