Preparation of zinc layered hydroxides-cinnamaldehyde nanocomposites and its physico-chemical study

Cinnamaldehyde (CINN) is an organic guest anion, the main constituent of cinnamon oil was intercalated into zinc layered hydroxides (ZLHs) by ion exchange method. CINN has been reported can killed mosquito larvae. The powder X-Ray diffraction (PXRD) indicates a successful intercalation of CINN into...

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Main Authors: Jamaluddin, Nurul Jannah, Saidi, Nurul Adila, Mohamad Jaafar, Adila
Format: Article
Language:English
Published: UPSI Press 2017
Online Access:http://psasir.upm.edu.my/id/eprint/62832/
http://psasir.upm.edu.my/id/eprint/62832/1/Preparation%20of%20zinc%20layered%20hydroxides.pdf
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author Jamaluddin, Nurul Jannah
Saidi, Nurul Adila
Mohamad Jaafar, Adila
author_facet Jamaluddin, Nurul Jannah
Saidi, Nurul Adila
Mohamad Jaafar, Adila
author_sort Jamaluddin, Nurul Jannah
building UPM Institutional Repository
collection Online Access
description Cinnamaldehyde (CINN) is an organic guest anion, the main constituent of cinnamon oil was intercalated into zinc layered hydroxides (ZLHs) by ion exchange method. CINN has been reported can killed mosquito larvae. The powder X-Ray diffraction (PXRD) indicates a successful intercalation of CINN into the interlayer galleries of ZLHs matrix when 1.0 g of ZnO with 0.08M of CINN was used forming zinc layered hydroxides-cinnamaldehyde (ZCINN) exhibiting basal spacing expansion, 21.2Å. Fourier transform infrared (FTIR) results supported and confirmed the intercalation of CINN as both ZnO and CINN functional groups appeared in ZCINN spectrum. The thermal stability property of the ZCINN was enhanced as compared to the anion, CINN. Field emission scanning electron microscopy (FESEM) image of ZnO showed a nonuniform granular-like structure transforming into flaky structure with various sizes after intercalation of CINN took place. These results indicate that it is possible to design and develop the nanocomposites containing larvicide for further investigations.
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spelling upm-628322022-11-10T04:11:16Z http://psasir.upm.edu.my/id/eprint/62832/ Preparation of zinc layered hydroxides-cinnamaldehyde nanocomposites and its physico-chemical study Jamaluddin, Nurul Jannah Saidi, Nurul Adila Mohamad Jaafar, Adila Cinnamaldehyde (CINN) is an organic guest anion, the main constituent of cinnamon oil was intercalated into zinc layered hydroxides (ZLHs) by ion exchange method. CINN has been reported can killed mosquito larvae. The powder X-Ray diffraction (PXRD) indicates a successful intercalation of CINN into the interlayer galleries of ZLHs matrix when 1.0 g of ZnO with 0.08M of CINN was used forming zinc layered hydroxides-cinnamaldehyde (ZCINN) exhibiting basal spacing expansion, 21.2Å. Fourier transform infrared (FTIR) results supported and confirmed the intercalation of CINN as both ZnO and CINN functional groups appeared in ZCINN spectrum. The thermal stability property of the ZCINN was enhanced as compared to the anion, CINN. Field emission scanning electron microscopy (FESEM) image of ZnO showed a nonuniform granular-like structure transforming into flaky structure with various sizes after intercalation of CINN took place. These results indicate that it is possible to design and develop the nanocomposites containing larvicide for further investigations. UPSI Press 2017-06 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/62832/1/Preparation%20of%20zinc%20layered%20hydroxides.pdf Jamaluddin, Nurul Jannah and Saidi, Nurul Adila and Mohamad Jaafar, Adila (2017) Preparation of zinc layered hydroxides-cinnamaldehyde nanocomposites and its physico-chemical study. EDUCATUM Journal of Science, Mathematics and Technology, 4 (1). 34 - 40. ISSN 2289-7070; ESSN: 2462-2451 https://ejournal.upsi.edu.my/index.php/EJSMT/article/view/56/48 10.37134/ejsmt.vol4.1.5.2017
spellingShingle Jamaluddin, Nurul Jannah
Saidi, Nurul Adila
Mohamad Jaafar, Adila
Preparation of zinc layered hydroxides-cinnamaldehyde nanocomposites and its physico-chemical study
title Preparation of zinc layered hydroxides-cinnamaldehyde nanocomposites and its physico-chemical study
title_full Preparation of zinc layered hydroxides-cinnamaldehyde nanocomposites and its physico-chemical study
title_fullStr Preparation of zinc layered hydroxides-cinnamaldehyde nanocomposites and its physico-chemical study
title_full_unstemmed Preparation of zinc layered hydroxides-cinnamaldehyde nanocomposites and its physico-chemical study
title_short Preparation of zinc layered hydroxides-cinnamaldehyde nanocomposites and its physico-chemical study
title_sort preparation of zinc layered hydroxides-cinnamaldehyde nanocomposites and its physico-chemical study
url http://psasir.upm.edu.my/id/eprint/62832/
http://psasir.upm.edu.my/id/eprint/62832/
http://psasir.upm.edu.my/id/eprint/62832/
http://psasir.upm.edu.my/id/eprint/62832/1/Preparation%20of%20zinc%20layered%20hydroxides.pdf