Effect delignification on the physical, thermal, chemical and structural properties of sugar palm fibre

Eco-friendly composites can be prepared by substituting man-made synthetic fibres with various types of cellulosic fibres. Sugar palm-derived nanocrystalline cellulose is a potential substitute. The most important factor in determining a good nanofiller reinforcement agent that can be used in compos...

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Main Authors: Rushdan, Ahamd Ilyas, Salit, Mohd Sapuan, Ishak, Mohamad Ridzwan, Zainudin, Edi Syams
Format: Article
Language:English
Published: College of Natural Resources 2017
Online Access:http://psasir.upm.edu.my/id/eprint/61541/
http://psasir.upm.edu.my/id/eprint/61541/1/Effect%20delignification%20on%20the%20physical%2C%20thermal%2C%20chemical%20and%20structural%20properties%20of%20sugar%20palm%20fibre.pdf
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author Rushdan, Ahamd Ilyas
Salit, Mohd Sapuan
Ishak, Mohamad Ridzwan
Zainudin, Edi Syams
author_facet Rushdan, Ahamd Ilyas
Salit, Mohd Sapuan
Ishak, Mohamad Ridzwan
Zainudin, Edi Syams
author_sort Rushdan, Ahamd Ilyas
building UPM Institutional Repository
collection Online Access
description Eco-friendly composites can be prepared by substituting man-made synthetic fibres with various types of cellulosic fibres. Sugar palm-derived nanocrystalline cellulose is a potential substitute. The most important factor in determining a good nanofiller reinforcement agent that can be used in composites is the character of the nanofiller itself, which is affected during a preliminary treatment. Thus, to gain better nanofiller properties, the delignification (NaClO2 and CH3COOH) and mercerization (NaOH) treatments must be optimized. The main objective of this study was to identify the effects of the delignification and mercerization treatments on sugar palm fibre (SPF). In addition, the characteristics of the SPF for the preparation of the hydrolysis treatment to produce nanocrystalline cellulose (NCC) for reinforcement in polymer composites were examined. Sugar palm cellulose (SPC) was extracted from the SPF, and its structural composition, thermal stability, functional groups, and degree of crystallinity were determined via field emission scanning electron microscopy (FESEM), thermogravimetric analysis (TGA), Fourier transform infrared (FTIR) spectroscopy, and X-ray diffraction (XRD), respectively. The density, moisture content, chemical composition, and structure of the SPC were also analysed.
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spelling upm-615412022-05-25T02:49:49Z http://psasir.upm.edu.my/id/eprint/61541/ Effect delignification on the physical, thermal, chemical and structural properties of sugar palm fibre Rushdan, Ahamd Ilyas Salit, Mohd Sapuan Ishak, Mohamad Ridzwan Zainudin, Edi Syams Eco-friendly composites can be prepared by substituting man-made synthetic fibres with various types of cellulosic fibres. Sugar palm-derived nanocrystalline cellulose is a potential substitute. The most important factor in determining a good nanofiller reinforcement agent that can be used in composites is the character of the nanofiller itself, which is affected during a preliminary treatment. Thus, to gain better nanofiller properties, the delignification (NaClO2 and CH3COOH) and mercerization (NaOH) treatments must be optimized. The main objective of this study was to identify the effects of the delignification and mercerization treatments on sugar palm fibre (SPF). In addition, the characteristics of the SPF for the preparation of the hydrolysis treatment to produce nanocrystalline cellulose (NCC) for reinforcement in polymer composites were examined. Sugar palm cellulose (SPC) was extracted from the SPF, and its structural composition, thermal stability, functional groups, and degree of crystallinity were determined via field emission scanning electron microscopy (FESEM), thermogravimetric analysis (TGA), Fourier transform infrared (FTIR) spectroscopy, and X-ray diffraction (XRD), respectively. The density, moisture content, chemical composition, and structure of the SPC were also analysed. College of Natural Resources 2017 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/61541/1/Effect%20delignification%20on%20the%20physical%2C%20thermal%2C%20chemical%20and%20structural%20properties%20of%20sugar%20palm%20fibre.pdf Rushdan, Ahamd Ilyas and Salit, Mohd Sapuan and Ishak, Mohamad Ridzwan and Zainudin, Edi Syams (2017) Effect delignification on the physical, thermal, chemical and structural properties of sugar palm fibre. BioResources, 12 (4). 8734 - 8754. ISSN 1930-2126 https://ojs.cnr.ncsu.edu/index.php/BioRes/article/view/BioRes_12_4_8734_Ilyas_Delignification_Sugar_Palm_Fibre
spellingShingle Rushdan, Ahamd Ilyas
Salit, Mohd Sapuan
Ishak, Mohamad Ridzwan
Zainudin, Edi Syams
Effect delignification on the physical, thermal, chemical and structural properties of sugar palm fibre
title Effect delignification on the physical, thermal, chemical and structural properties of sugar palm fibre
title_full Effect delignification on the physical, thermal, chemical and structural properties of sugar palm fibre
title_fullStr Effect delignification on the physical, thermal, chemical and structural properties of sugar palm fibre
title_full_unstemmed Effect delignification on the physical, thermal, chemical and structural properties of sugar palm fibre
title_short Effect delignification on the physical, thermal, chemical and structural properties of sugar palm fibre
title_sort effect delignification on the physical, thermal, chemical and structural properties of sugar palm fibre
url http://psasir.upm.edu.my/id/eprint/61541/
http://psasir.upm.edu.my/id/eprint/61541/
http://psasir.upm.edu.my/id/eprint/61541/1/Effect%20delignification%20on%20the%20physical%2C%20thermal%2C%20chemical%20and%20structural%20properties%20of%20sugar%20palm%20fibre.pdf