Effect of deposition time on the morphology and structural properties of indium antimonide nanowires (InSb) by template assisted electrodeposition

Semiconductor InSb nanowire have been synthesized by the typical three-electrode electrochemical cell. The deposition is from tartaric acid aqueous solution into anodic alumina oxide (AAO) at different time deposition varies from 15 to 40 mins with constant deposition potential of -1.5 V. The morpho...

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Main Authors: Khairudin, Azelah, Paiman, Suriati
Format: Article
Language:English
Published: Malaysian Solid State Science and Technology Society 2016
Online Access:http://psasir.upm.edu.my/id/eprint/54002/
http://psasir.upm.edu.my/id/eprint/54002/1/Effect%20of%20deposition%20time%20on%20the%20morphology%20and%20structural%20properties%20of%20indium%20antimonide%20nanowires%20%28InSb%29%20by%20template%20assisted%20electrodeposition.pdf
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author Khairudin, Azelah
Paiman, Suriati
author_facet Khairudin, Azelah
Paiman, Suriati
author_sort Khairudin, Azelah
building UPM Institutional Repository
collection Online Access
description Semiconductor InSb nanowire have been synthesized by the typical three-electrode electrochemical cell. The deposition is from tartaric acid aqueous solution into anodic alumina oxide (AAO) at different time deposition varies from 15 to 40 mins with constant deposition potential of -1.5 V. The morphology and structural properties of InSb nanowires were studied using XRD and FESEM equipped with EDX. The nanowires have diameter varying and the length of the template assisted InSb nanowires varied from the deposition time of 15 to 40 mins, from 100 to 200 nm respectively. The length of synthesized InSb nanowires increases from 1.8 to 5.5 μm with the increasing deposition time of 15 to 40 min. The XRD analysis shows that the diffraction peaks of nanowires are on a plane (111) and (220). Based on the elemental composition from the EDX, almost stoichiometric composition with ratio 1:1.1 was achieved for the samples deposited for 35 and 40 minutes.
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spelling upm-540022022-04-11T06:05:30Z http://psasir.upm.edu.my/id/eprint/54002/ Effect of deposition time on the morphology and structural properties of indium antimonide nanowires (InSb) by template assisted electrodeposition Khairudin, Azelah Paiman, Suriati Semiconductor InSb nanowire have been synthesized by the typical three-electrode electrochemical cell. The deposition is from tartaric acid aqueous solution into anodic alumina oxide (AAO) at different time deposition varies from 15 to 40 mins with constant deposition potential of -1.5 V. The morphology and structural properties of InSb nanowires were studied using XRD and FESEM equipped with EDX. The nanowires have diameter varying and the length of the template assisted InSb nanowires varied from the deposition time of 15 to 40 mins, from 100 to 200 nm respectively. The length of synthesized InSb nanowires increases from 1.8 to 5.5 μm with the increasing deposition time of 15 to 40 min. The XRD analysis shows that the diffraction peaks of nanowires are on a plane (111) and (220). Based on the elemental composition from the EDX, almost stoichiometric composition with ratio 1:1.1 was achieved for the samples deposited for 35 and 40 minutes. Malaysian Solid State Science and Technology Society 2016 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/54002/1/Effect%20of%20deposition%20time%20on%20the%20morphology%20and%20structural%20properties%20of%20indium%20antimonide%20nanowires%20%28InSb%29%20by%20template%20assisted%20electrodeposition.pdf Khairudin, Azelah and Paiman, Suriati (2016) Effect of deposition time on the morphology and structural properties of indium antimonide nanowires (InSb) by template assisted electrodeposition. Journal of Solid State Science and Technology, 24 (1). pp. 275-281. ISSN 0127-9645 https://myjms.mohe.gov.my/index.php/masshp/article/view/2509
spellingShingle Khairudin, Azelah
Paiman, Suriati
Effect of deposition time on the morphology and structural properties of indium antimonide nanowires (InSb) by template assisted electrodeposition
title Effect of deposition time on the morphology and structural properties of indium antimonide nanowires (InSb) by template assisted electrodeposition
title_full Effect of deposition time on the morphology and structural properties of indium antimonide nanowires (InSb) by template assisted electrodeposition
title_fullStr Effect of deposition time on the morphology and structural properties of indium antimonide nanowires (InSb) by template assisted electrodeposition
title_full_unstemmed Effect of deposition time on the morphology and structural properties of indium antimonide nanowires (InSb) by template assisted electrodeposition
title_short Effect of deposition time on the morphology and structural properties of indium antimonide nanowires (InSb) by template assisted electrodeposition
title_sort effect of deposition time on the morphology and structural properties of indium antimonide nanowires (insb) by template assisted electrodeposition
url http://psasir.upm.edu.my/id/eprint/54002/
http://psasir.upm.edu.my/id/eprint/54002/
http://psasir.upm.edu.my/id/eprint/54002/1/Effect%20of%20deposition%20time%20on%20the%20morphology%20and%20structural%20properties%20of%20indium%20antimonide%20nanowires%20%28InSb%29%20by%20template%20assisted%20electrodeposition.pdf