Formation and characterization of ultrafine nanophosphors of lithium tetraborate (Li2B4O7) for personnel and medical dosimetry

The present study demonstrates an innovative single-step thermal synthesis of nano-sized lithium tetraborate dosimeter and its characterization. The optimum calcination temperature and time for the synthesis of the nanoparticles material was 750 °C and 2 h, respectively. Characterization of the samp...

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Main Authors: Khalilzadeh, Nasrin, Saion, Elias, Mirabolghasemi, Hamed, Soltani, Nayereh, Shaari, Abdul Halim, Hashim, Mansor, Mod Ali, Noriah, Dehzangi, Arash
Format: Article
Language:English
Published: Elsevier 2016
Online Access:http://psasir.upm.edu.my/id/eprint/52316/
http://psasir.upm.edu.my/id/eprint/52316/1/Formation%20and%20characterization%20of%20ultrafine%20nanophosphors%20of%20lithium%20tetraborate%20%28Li2B4O7%29%20for%20personnel%20and%20medical%20dosimetry.pdf
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author Khalilzadeh, Nasrin
Saion, Elias
Mirabolghasemi, Hamed
Soltani, Nayereh
Shaari, Abdul Halim
Hashim, Mansor
Mod Ali, Noriah
Dehzangi, Arash
author_facet Khalilzadeh, Nasrin
Saion, Elias
Mirabolghasemi, Hamed
Soltani, Nayereh
Shaari, Abdul Halim
Hashim, Mansor
Mod Ali, Noriah
Dehzangi, Arash
author_sort Khalilzadeh, Nasrin
building UPM Institutional Repository
collection Online Access
description The present study demonstrates an innovative single-step thermal synthesis of nano-sized lithium tetraborate dosimeter and its characterization. The optimum calcination temperature and time for the synthesis of the nanoparticles material was 750 °C and 2 h, respectively. Characterization of the samples was carried out using X-ray diffractometry (XRD), Fourier transform infrared (FT-IR) spectroscopy, transmission electron microscopy (TEM), and thermoluminescence (TL). FT-IR, XRD and TEM results confirmed the formation of pure nano-crystalline lithium tetraborate. The product showed a linear response over a wide range of doses from 10−1 to 1.5 × 102 Gy. Moreover, the samples illustrate non-energy dependence among a wide range energy interval from 24 keV up to 1250 keV and almost no fading during one month storage.
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spelling upm-523162017-06-05T05:42:32Z http://psasir.upm.edu.my/id/eprint/52316/ Formation and characterization of ultrafine nanophosphors of lithium tetraborate (Li2B4O7) for personnel and medical dosimetry Khalilzadeh, Nasrin Saion, Elias Mirabolghasemi, Hamed Soltani, Nayereh Shaari, Abdul Halim Hashim, Mansor Mod Ali, Noriah Dehzangi, Arash The present study demonstrates an innovative single-step thermal synthesis of nano-sized lithium tetraborate dosimeter and its characterization. The optimum calcination temperature and time for the synthesis of the nanoparticles material was 750 °C and 2 h, respectively. Characterization of the samples was carried out using X-ray diffractometry (XRD), Fourier transform infrared (FT-IR) spectroscopy, transmission electron microscopy (TEM), and thermoluminescence (TL). FT-IR, XRD and TEM results confirmed the formation of pure nano-crystalline lithium tetraborate. The product showed a linear response over a wide range of doses from 10−1 to 1.5 × 102 Gy. Moreover, the samples illustrate non-energy dependence among a wide range energy interval from 24 keV up to 1250 keV and almost no fading during one month storage. Elsevier 2016 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/52316/1/Formation%20and%20characterization%20of%20ultrafine%20nanophosphors%20of%20lithium%20tetraborate%20%28Li2B4O7%29%20for%20personnel%20and%20medical%20dosimetry.pdf Khalilzadeh, Nasrin and Saion, Elias and Mirabolghasemi, Hamed and Soltani, Nayereh and Shaari, Abdul Halim and Hashim, Mansor and Mod Ali, Noriah and Dehzangi, Arash (2016) Formation and characterization of ultrafine nanophosphors of lithium tetraborate (Li2B4O7) for personnel and medical dosimetry. Journal of Materials Research and Technology, 5 (3). pp. 206-212. ISSN 2238-7854 http://www.sciencedirect.com/science/article/pii/S2238785415001118 10.1016/j.jmrt.2015.11.002
spellingShingle Khalilzadeh, Nasrin
Saion, Elias
Mirabolghasemi, Hamed
Soltani, Nayereh
Shaari, Abdul Halim
Hashim, Mansor
Mod Ali, Noriah
Dehzangi, Arash
Formation and characterization of ultrafine nanophosphors of lithium tetraborate (Li2B4O7) for personnel and medical dosimetry
title Formation and characterization of ultrafine nanophosphors of lithium tetraborate (Li2B4O7) for personnel and medical dosimetry
title_full Formation and characterization of ultrafine nanophosphors of lithium tetraborate (Li2B4O7) for personnel and medical dosimetry
title_fullStr Formation and characterization of ultrafine nanophosphors of lithium tetraborate (Li2B4O7) for personnel and medical dosimetry
title_full_unstemmed Formation and characterization of ultrafine nanophosphors of lithium tetraborate (Li2B4O7) for personnel and medical dosimetry
title_short Formation and characterization of ultrafine nanophosphors of lithium tetraborate (Li2B4O7) for personnel and medical dosimetry
title_sort formation and characterization of ultrafine nanophosphors of lithium tetraborate (li2b4o7) for personnel and medical dosimetry
url http://psasir.upm.edu.my/id/eprint/52316/
http://psasir.upm.edu.my/id/eprint/52316/
http://psasir.upm.edu.my/id/eprint/52316/
http://psasir.upm.edu.my/id/eprint/52316/1/Formation%20and%20characterization%20of%20ultrafine%20nanophosphors%20of%20lithium%20tetraborate%20%28Li2B4O7%29%20for%20personnel%20and%20medical%20dosimetry.pdf