Sonochemical method for the synthesis of silver nanoparticles in κ-carrageenan from silver salt at different concentrations

A green sonochemical method was developed for preparing silver nanoparticles (Ag-NPs) in j-carrageenan in different concentrations of AgNO3. The j-carrageenan was used as an eco-friendly stabilizer and ultrasonic irradiation as a green reducing agent. The number of Ag-NPs increased with increasing c...

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Main Authors: Elsupikhe, Randa Fawzi, Shameli, Kamyar, Ahmad, Mansor B.
Format: Article
Language:English
Published: Springer 2015
Online Access:http://psasir.upm.edu.my/id/eprint/46343/
http://psasir.upm.edu.my/id/eprint/46343/1/Sonochemical%20method%20for%20the%20synthesis%20of%20silver%20nanoparticles%20in%20%CE%BA-carrageenan%20from%20silver%20salt%20at%20different%20concentrations_New.pdf
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author Elsupikhe, Randa Fawzi
Shameli, Kamyar
Ahmad, Mansor B.
author_facet Elsupikhe, Randa Fawzi
Shameli, Kamyar
Ahmad, Mansor B.
author_sort Elsupikhe, Randa Fawzi
building UPM Institutional Repository
collection Online Access
description A green sonochemical method was developed for preparing silver nanoparticles (Ag-NPs) in j-carrageenan in different concentrations of AgNO3. The j-carrageenan was used as an eco-friendly stabilizer and ultrasonic irradiation as a green reducing agent. The number of Ag-NPs increased with increasing concentrations of AgNO3. Formation of Ag/j-carrageenan was determined by UV–visible spectroscopy where the surface plasmon absorption maximum was observed at 410–416 nm. XRD analysis showed the Ag-NPs are of a face-centered cubic structure. TEM images showed the well-dispersed Ag-NPs with an average particle size \5 nm. SEM images showed the spherical shape of the Ag-NPs. The FT-IR spectrum indicated the presence of j-carrageenan in capping the Ag-NPs. The use of photo irradiation provides a green and economic method features to the synthesis reported in this study.
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spelling upm-463432022-06-17T08:23:57Z http://psasir.upm.edu.my/id/eprint/46343/ Sonochemical method for the synthesis of silver nanoparticles in κ-carrageenan from silver salt at different concentrations Elsupikhe, Randa Fawzi Shameli, Kamyar Ahmad, Mansor B. A green sonochemical method was developed for preparing silver nanoparticles (Ag-NPs) in j-carrageenan in different concentrations of AgNO3. The j-carrageenan was used as an eco-friendly stabilizer and ultrasonic irradiation as a green reducing agent. The number of Ag-NPs increased with increasing concentrations of AgNO3. Formation of Ag/j-carrageenan was determined by UV–visible spectroscopy where the surface plasmon absorption maximum was observed at 410–416 nm. XRD analysis showed the Ag-NPs are of a face-centered cubic structure. TEM images showed the well-dispersed Ag-NPs with an average particle size \5 nm. SEM images showed the spherical shape of the Ag-NPs. The FT-IR spectrum indicated the presence of j-carrageenan in capping the Ag-NPs. The use of photo irradiation provides a green and economic method features to the synthesis reported in this study. Springer 2015-11 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/46343/1/Sonochemical%20method%20for%20the%20synthesis%20of%20silver%20nanoparticles%20in%20%CE%BA-carrageenan%20from%20silver%20salt%20at%20different%20concentrations_New.pdf Elsupikhe, Randa Fawzi and Shameli, Kamyar and Ahmad, Mansor B. (2015) Sonochemical method for the synthesis of silver nanoparticles in κ-carrageenan from silver salt at different concentrations. Research on Chemical Intermediates, 41 (11). pp. 8515-8525. ISSN 0922-6168; ESSN: 1568-5675 https://link.springer.com/article/10.1007/s11164-014-1907-z 10.1007/s11164-014-1907-z
spellingShingle Elsupikhe, Randa Fawzi
Shameli, Kamyar
Ahmad, Mansor B.
Sonochemical method for the synthesis of silver nanoparticles in κ-carrageenan from silver salt at different concentrations
title Sonochemical method for the synthesis of silver nanoparticles in κ-carrageenan from silver salt at different concentrations
title_full Sonochemical method for the synthesis of silver nanoparticles in κ-carrageenan from silver salt at different concentrations
title_fullStr Sonochemical method for the synthesis of silver nanoparticles in κ-carrageenan from silver salt at different concentrations
title_full_unstemmed Sonochemical method for the synthesis of silver nanoparticles in κ-carrageenan from silver salt at different concentrations
title_short Sonochemical method for the synthesis of silver nanoparticles in κ-carrageenan from silver salt at different concentrations
title_sort sonochemical method for the synthesis of silver nanoparticles in κ-carrageenan from silver salt at different concentrations
url http://psasir.upm.edu.my/id/eprint/46343/
http://psasir.upm.edu.my/id/eprint/46343/
http://psasir.upm.edu.my/id/eprint/46343/
http://psasir.upm.edu.my/id/eprint/46343/1/Sonochemical%20method%20for%20the%20synthesis%20of%20silver%20nanoparticles%20in%20%CE%BA-carrageenan%20from%20silver%20salt%20at%20different%20concentrations_New.pdf