Qualitative phytochemical screening and GC-MS profiling of Azadirachta excelsa leaf extract

Azadirachta excelsa is traditionally used by the locals to treat diabetes mellitus but the active compounds of the leaves have not been identified yet. Hence, the aim of the study was to identify the components of Azadirachta excelsa leaf extract by qualitative phytochemical screening and gas chroma...

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Main Authors: Shafie, Nurul 'Izzati, Samsulrizal, Nurdiana, Ahmad Sopian, Nurfarhana, Rajion, Mohamed Ali, Goh, Yong Meng, Md. Ajat, Mohd Mokrish, Ahmad, Hafandi
Format: Article
Language:English
Published: Malaysian Society of Applied Biology 2015
Online Access:http://psasir.upm.edu.my/id/eprint/46055/
http://psasir.upm.edu.my/id/eprint/46055/1/Qualitative%20phytochemical%20screening%20and%20GC-MS%20profiling%20of%20Azadirachta%20excelsa%20leaf%20extract.pdf
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author Shafie, Nurul 'Izzati
Samsulrizal, Nurdiana
Ahmad Sopian, Nurfarhana
Rajion, Mohamed Ali
Goh, Yong Meng
Md. Ajat, Mohd Mokrish
Ahmad, Hafandi
author_facet Shafie, Nurul 'Izzati
Samsulrizal, Nurdiana
Ahmad Sopian, Nurfarhana
Rajion, Mohamed Ali
Goh, Yong Meng
Md. Ajat, Mohd Mokrish
Ahmad, Hafandi
author_sort Shafie, Nurul 'Izzati
building UPM Institutional Repository
collection Online Access
description Azadirachta excelsa is traditionally used by the locals to treat diabetes mellitus but the active compounds of the leaves have not been identified yet. Hence, the aim of the study was to identify the components of Azadirachta excelsa leaf extract by qualitative phytochemical screening and gas chromatography-mass spectrometry (GC-MS). Five grams of leaf extract were extracted using various solvents for phytochemical screening, while another five grams of ethanolic leaf extract was subjected for GC-MS analysis where the mass spectra of the compounds detected were matched with the National Institute of Standards and Technology (NIST) library. The results showed the presence of flavonoids, condensed tannin, triterpenes and steroids in phytochemical screening tests, while GC-MS analysis revealed the presence of seven major compounds in the ethanolic leaf extract. The major component of A.excelsa ethanolic leaf extract was 9, 12, 15-octadecatrienoic acid (42.34%), followed by pentadecanoic acid, 14-methyl-, methyl ester (28.99%), phytol (10.63%), 9, 12, 15-octadecatrien-1-ol (5.37%), octadecanoic acid, methyl ester (4.36%), 9, 12-octadecadienoic acid, methyl ester (4.24%) and hexadecanoic acid, ethyl ester (4.06%). Therefore, the findings of this study form a basis for the characterization of the compounds and allow researchers to investigate the potential of this plant in treating diabetes mellitus.
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spelling upm-460552022-03-28T07:11:33Z http://psasir.upm.edu.my/id/eprint/46055/ Qualitative phytochemical screening and GC-MS profiling of Azadirachta excelsa leaf extract Shafie, Nurul 'Izzati Samsulrizal, Nurdiana Ahmad Sopian, Nurfarhana Rajion, Mohamed Ali Goh, Yong Meng Md. Ajat, Mohd Mokrish Ahmad, Hafandi Azadirachta excelsa is traditionally used by the locals to treat diabetes mellitus but the active compounds of the leaves have not been identified yet. Hence, the aim of the study was to identify the components of Azadirachta excelsa leaf extract by qualitative phytochemical screening and gas chromatography-mass spectrometry (GC-MS). Five grams of leaf extract were extracted using various solvents for phytochemical screening, while another five grams of ethanolic leaf extract was subjected for GC-MS analysis where the mass spectra of the compounds detected were matched with the National Institute of Standards and Technology (NIST) library. The results showed the presence of flavonoids, condensed tannin, triterpenes and steroids in phytochemical screening tests, while GC-MS analysis revealed the presence of seven major compounds in the ethanolic leaf extract. The major component of A.excelsa ethanolic leaf extract was 9, 12, 15-octadecatrienoic acid (42.34%), followed by pentadecanoic acid, 14-methyl-, methyl ester (28.99%), phytol (10.63%), 9, 12, 15-octadecatrien-1-ol (5.37%), octadecanoic acid, methyl ester (4.36%), 9, 12-octadecadienoic acid, methyl ester (4.24%) and hexadecanoic acid, ethyl ester (4.06%). Therefore, the findings of this study form a basis for the characterization of the compounds and allow researchers to investigate the potential of this plant in treating diabetes mellitus. Malaysian Society of Applied Biology 2015 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/46055/1/Qualitative%20phytochemical%20screening%20and%20GC-MS%20profiling%20of%20Azadirachta%20excelsa%20leaf%20extract.pdf Shafie, Nurul 'Izzati and Samsulrizal, Nurdiana and Ahmad Sopian, Nurfarhana and Rajion, Mohamed Ali and Goh, Yong Meng and Md. Ajat, Mohd Mokrish and Ahmad, Hafandi (2015) Qualitative phytochemical screening and GC-MS profiling of Azadirachta excelsa leaf extract. Malaysian Applied Biology, 44 (3). pp. 87-92. ISSN 0126-8643 https://jms.mabjournal.com/index.php/mab/article/view/2023
spellingShingle Shafie, Nurul 'Izzati
Samsulrizal, Nurdiana
Ahmad Sopian, Nurfarhana
Rajion, Mohamed Ali
Goh, Yong Meng
Md. Ajat, Mohd Mokrish
Ahmad, Hafandi
Qualitative phytochemical screening and GC-MS profiling of Azadirachta excelsa leaf extract
title Qualitative phytochemical screening and GC-MS profiling of Azadirachta excelsa leaf extract
title_full Qualitative phytochemical screening and GC-MS profiling of Azadirachta excelsa leaf extract
title_fullStr Qualitative phytochemical screening and GC-MS profiling of Azadirachta excelsa leaf extract
title_full_unstemmed Qualitative phytochemical screening and GC-MS profiling of Azadirachta excelsa leaf extract
title_short Qualitative phytochemical screening and GC-MS profiling of Azadirachta excelsa leaf extract
title_sort qualitative phytochemical screening and gc-ms profiling of azadirachta excelsa leaf extract
url http://psasir.upm.edu.my/id/eprint/46055/
http://psasir.upm.edu.my/id/eprint/46055/
http://psasir.upm.edu.my/id/eprint/46055/1/Qualitative%20phytochemical%20screening%20and%20GC-MS%20profiling%20of%20Azadirachta%20excelsa%20leaf%20extract.pdf