Microstructural, mechanical, and physicochemical behaviours of alkali pre-treated oil palm stalk fibres

The effect of alkali pre-treatment (sodium hydroxide, NaOH) on the microstructural, mechanical, and chemical composition of oil palm stalk fibres (OPSF) is reported for future bioconversion processes. The OPSF was pre-treated with various concentrations of NaOH (5, 10, 20, 30, and 40% w/v). Scanning...

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Main Authors: Baharuddin, Azhari Samsu, Mohammed, Mohd Afandi P., Mat Lazim, Azwan, Loo, Yu Xiang, Hanipah, Suhaiza Hanim
Format: Article
Language:English
Published: North Carolina University 2015
Online Access:http://psasir.upm.edu.my/id/eprint/45477/
http://psasir.upm.edu.my/id/eprint/45477/1/PALM.pdf
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author Baharuddin, Azhari Samsu
Mohammed, Mohd Afandi P.
Mat Lazim, Azwan
Loo, Yu Xiang
Hanipah, Suhaiza Hanim
author_facet Baharuddin, Azhari Samsu
Mohammed, Mohd Afandi P.
Mat Lazim, Azwan
Loo, Yu Xiang
Hanipah, Suhaiza Hanim
author_sort Baharuddin, Azhari Samsu
building UPM Institutional Repository
collection Online Access
description The effect of alkali pre-treatment (sodium hydroxide, NaOH) on the microstructural, mechanical, and chemical composition of oil palm stalk fibres (OPSF) is reported for future bioconversion processes. The OPSF was pre-treated with various concentrations of NaOH (5, 10, 20, 30, and 40% w/v). Scanning electron microscopy analysis revealed that 5% w/v alkali concentration caused complete removal of silica bodies and waxy layers, whereas pronounced degradation of the fibres occurred at 40% w/v NaOH concentration. Mechanical test results showed that the maximum elastic modulus of untreated OPSF was 2.5 GPa and the modulus was not sensitive to alkali concentration. Permanent set (plastic strain) and viscoelastic behaviours of OPSF were observed from the loading-unloading and stress relaxation test results, respectively. Agreement was observed between the Prony series viscoelastic model and test results, which provided further evidence of the viscoelastic behaviour of OPSF.
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institution Universiti Putra Malaysia
institution_category Local University
language English
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publishDate 2015
publisher North Carolina University
recordtype eprints
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spelling upm-454772021-01-23T21:29:30Z http://psasir.upm.edu.my/id/eprint/45477/ Microstructural, mechanical, and physicochemical behaviours of alkali pre-treated oil palm stalk fibres Baharuddin, Azhari Samsu Mohammed, Mohd Afandi P. Mat Lazim, Azwan Loo, Yu Xiang Hanipah, Suhaiza Hanim The effect of alkali pre-treatment (sodium hydroxide, NaOH) on the microstructural, mechanical, and chemical composition of oil palm stalk fibres (OPSF) is reported for future bioconversion processes. The OPSF was pre-treated with various concentrations of NaOH (5, 10, 20, 30, and 40% w/v). Scanning electron microscopy analysis revealed that 5% w/v alkali concentration caused complete removal of silica bodies and waxy layers, whereas pronounced degradation of the fibres occurred at 40% w/v NaOH concentration. Mechanical test results showed that the maximum elastic modulus of untreated OPSF was 2.5 GPa and the modulus was not sensitive to alkali concentration. Permanent set (plastic strain) and viscoelastic behaviours of OPSF were observed from the loading-unloading and stress relaxation test results, respectively. Agreement was observed between the Prony series viscoelastic model and test results, which provided further evidence of the viscoelastic behaviour of OPSF. North Carolina University 2015 Article PeerReviewed text en http://psasir.upm.edu.my/id/eprint/45477/1/PALM.pdf Baharuddin, Azhari Samsu and Mohammed, Mohd Afandi P. and Mat Lazim, Azwan and Loo, Yu Xiang and Hanipah, Suhaiza Hanim (2015) Microstructural, mechanical, and physicochemical behaviours of alkali pre-treated oil palm stalk fibres. Bioresources, 10 (2). pp. 2783-2796. ISSN 1930-2126 https://ojs.cnr.ncsu.edu/index.php/BioRes/article/view/BioRes_10_2_2783_Yu_Microstructural_Alkali_Oil_Palm/3445
spellingShingle Baharuddin, Azhari Samsu
Mohammed, Mohd Afandi P.
Mat Lazim, Azwan
Loo, Yu Xiang
Hanipah, Suhaiza Hanim
Microstructural, mechanical, and physicochemical behaviours of alkali pre-treated oil palm stalk fibres
title Microstructural, mechanical, and physicochemical behaviours of alkali pre-treated oil palm stalk fibres
title_full Microstructural, mechanical, and physicochemical behaviours of alkali pre-treated oil palm stalk fibres
title_fullStr Microstructural, mechanical, and physicochemical behaviours of alkali pre-treated oil palm stalk fibres
title_full_unstemmed Microstructural, mechanical, and physicochemical behaviours of alkali pre-treated oil palm stalk fibres
title_short Microstructural, mechanical, and physicochemical behaviours of alkali pre-treated oil palm stalk fibres
title_sort microstructural, mechanical, and physicochemical behaviours of alkali pre-treated oil palm stalk fibres
url http://psasir.upm.edu.my/id/eprint/45477/
http://psasir.upm.edu.my/id/eprint/45477/
http://psasir.upm.edu.my/id/eprint/45477/1/PALM.pdf