Subsolidus solution and oxide ionic conductivity of Nd-substituted bismuth yttria fluorites

Pure phase Bi1.6Y0.4-xNdxO3 solid solution with x = 0.00, 0.10 and 0.20 was successfully synthesised via conventional solid state method at 850°C in 21 h. The materials were refined and fully indexed with space group Fm-3m and lattice parameters, a ranging from 5.5124(1) Å to 5.5289(4) Å. Variation...

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Main Authors: Rahman, N., Tan, Kar Ban, Zainal, Zulkarnain, Khaw, Chwin Chieh, Chon, Mun Ping
Format: Article
Language:English
Published: Penerbit Universiti Kebangsaan Malaysia 2015
Online Access:http://psasir.upm.edu.my/id/eprint/42219/
http://psasir.upm.edu.my/id/eprint/42219/1/Subsolidus%20solution%20and%20oxide%20ionic%20conductivity%20of%20Nd-substituted%20bismuth%20yttria%20fluorites.pdf
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author Rahman, N.
Tan, Kar Ban
Zainal, Zulkarnain
Khaw, Chwin Chieh
Chon, Mun Ping
author_facet Rahman, N.
Tan, Kar Ban
Zainal, Zulkarnain
Khaw, Chwin Chieh
Chon, Mun Ping
author_sort Rahman, N.
building UPM Institutional Repository
collection Online Access
description Pure phase Bi1.6Y0.4-xNdxO3 solid solution with x = 0.00, 0.10 and 0.20 was successfully synthesised via conventional solid state method at 850°C in 21 h. The materials were refined and fully indexed with space group Fm-3m and lattice parameters, a ranging from 5.5124(1) Å to 5.5289(4) Å. Variation of the lattice parameters of these materials were found in an almost linear correlation with increasing Nd2O3 dopant concentration. Thermal analysis of Bi1.6Y0.4-xNdxO3 solid solution showed no thermal event that associated with any phase transition or weight loss within the studied temperature range of 35 to 900°C. The electrical properties of the samples were investigated by ac impedance analyser, HP4192 at temperature ranging from 25 to 800°C over frequency of 5 Hz to 13 MHz. Bi1.6Y0.3Nd0.1O3 exhibited the highest oxide ion conductivity among the synthesised samples in Bi1.6Y0.4-xNdxO3 solid solution.
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spelling upm-422192016-04-12T04:49:50Z http://psasir.upm.edu.my/id/eprint/42219/ Subsolidus solution and oxide ionic conductivity of Nd-substituted bismuth yttria fluorites Rahman, N. Tan, Kar Ban Zainal, Zulkarnain Khaw, Chwin Chieh Chon, Mun Ping Pure phase Bi1.6Y0.4-xNdxO3 solid solution with x = 0.00, 0.10 and 0.20 was successfully synthesised via conventional solid state method at 850°C in 21 h. The materials were refined and fully indexed with space group Fm-3m and lattice parameters, a ranging from 5.5124(1) Å to 5.5289(4) Å. Variation of the lattice parameters of these materials were found in an almost linear correlation with increasing Nd2O3 dopant concentration. Thermal analysis of Bi1.6Y0.4-xNdxO3 solid solution showed no thermal event that associated with any phase transition or weight loss within the studied temperature range of 35 to 900°C. The electrical properties of the samples were investigated by ac impedance analyser, HP4192 at temperature ranging from 25 to 800°C over frequency of 5 Hz to 13 MHz. Bi1.6Y0.3Nd0.1O3 exhibited the highest oxide ion conductivity among the synthesised samples in Bi1.6Y0.4-xNdxO3 solid solution. Penerbit Universiti Kebangsaan Malaysia 2015 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/42219/1/Subsolidus%20solution%20and%20oxide%20ionic%20conductivity%20of%20Nd-substituted%20bismuth%20yttria%20fluorites.pdf Rahman, N. and Tan, Kar Ban and Zainal, Zulkarnain and Khaw, Chwin Chieh and Chon, Mun Ping (2015) Subsolidus solution and oxide ionic conductivity of Nd-substituted bismuth yttria fluorites. Sains Malaysiana, 44 (7). pp. 1003-1009. ISSN 0026-6039 http://www.ukm.my/jsm/malay_journals/jilid44bil7_2015/Jilid44Bil7_2015ms1003-1009.html
spellingShingle Rahman, N.
Tan, Kar Ban
Zainal, Zulkarnain
Khaw, Chwin Chieh
Chon, Mun Ping
Subsolidus solution and oxide ionic conductivity of Nd-substituted bismuth yttria fluorites
title Subsolidus solution and oxide ionic conductivity of Nd-substituted bismuth yttria fluorites
title_full Subsolidus solution and oxide ionic conductivity of Nd-substituted bismuth yttria fluorites
title_fullStr Subsolidus solution and oxide ionic conductivity of Nd-substituted bismuth yttria fluorites
title_full_unstemmed Subsolidus solution and oxide ionic conductivity of Nd-substituted bismuth yttria fluorites
title_short Subsolidus solution and oxide ionic conductivity of Nd-substituted bismuth yttria fluorites
title_sort subsolidus solution and oxide ionic conductivity of nd-substituted bismuth yttria fluorites
url http://psasir.upm.edu.my/id/eprint/42219/
http://psasir.upm.edu.my/id/eprint/42219/
http://psasir.upm.edu.my/id/eprint/42219/1/Subsolidus%20solution%20and%20oxide%20ionic%20conductivity%20of%20Nd-substituted%20bismuth%20yttria%20fluorites.pdf