The influence of samarium doping in Bi1.6 (Pb0.4)Sr2- xSmxCa2Cu3Oy prepared by coprecipitation method

The influence of Sm doping on the phase formation, normal state properties and microstructure development of Bi-2223 superconductors was systematically investigated. Samarium was incorporated in the strontium site with x ranging from 0.00 to 0.30 prepared via coprecipitation technique. The four poin...

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Main Authors: Hamadneh, Imad (Moh'd Khair) Rashid, Shaari, Abdul Halim, Lee, C. K., Daud, W. M., Hassan, Z. A.
Format: Article
Language:English
Published: Malaysian Solid State Science and Technology Society 2003
Online Access:http://psasir.upm.edu.my/id/eprint/42206/
http://psasir.upm.edu.my/id/eprint/42206/1/The%20influence%20of%20samarium%20doping%20in%20Bi1.6%20%28Pb0.4%29Sr2-%20xSmxCa2Cu3Oy%20prepared%20by%20coprecipitation%20method.pdf
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author Hamadneh, Imad (Moh'd Khair) Rashid
Shaari, Abdul Halim
Lee, C. K.
Daud, W. M.
Hassan, Z. A.
author_facet Hamadneh, Imad (Moh'd Khair) Rashid
Shaari, Abdul Halim
Lee, C. K.
Daud, W. M.
Hassan, Z. A.
author_sort Hamadneh, Imad (Moh'd Khair) Rashid
building UPM Institutional Repository
collection Online Access
description The influence of Sm doping on the phase formation, normal state properties and microstructure development of Bi-2223 superconductors was systematically investigated. Samarium was incorporated in the strontium site with x ranging from 0.00 to 0.30 prepared via coprecipitation technique. The four point probe measurements showed the loss in metallic behaviour for the samples with Sm doped above x=0.2. XRD results showed the decrease of the volume percentage of the 2223 phase followed by increasing in the density of the lattice. The SEM micrographs showed the decrease in the grain size for all samples containing samarium. The temperature dependence of ac susceptibility data shows the shifting towards lower temperature as the Sm concentration increases presence of low Tconset phase. The imaginary component, χ”, shows a decrease in the intergranular coupling peak, Tp, towards lower temperature as the Sm concentration increases. Samarium did not enhance the Tc(R=0) but gradually decreases its value from 102. K to 52 K for x=0.00 to x=0.20 respectively.
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spelling upm-422062016-04-12T04:31:30Z http://psasir.upm.edu.my/id/eprint/42206/ The influence of samarium doping in Bi1.6 (Pb0.4)Sr2- xSmxCa2Cu3Oy prepared by coprecipitation method Hamadneh, Imad (Moh'd Khair) Rashid Shaari, Abdul Halim Lee, C. K. Daud, W. M. Hassan, Z. A. The influence of Sm doping on the phase formation, normal state properties and microstructure development of Bi-2223 superconductors was systematically investigated. Samarium was incorporated in the strontium site with x ranging from 0.00 to 0.30 prepared via coprecipitation technique. The four point probe measurements showed the loss in metallic behaviour for the samples with Sm doped above x=0.2. XRD results showed the decrease of the volume percentage of the 2223 phase followed by increasing in the density of the lattice. The SEM micrographs showed the decrease in the grain size for all samples containing samarium. The temperature dependence of ac susceptibility data shows the shifting towards lower temperature as the Sm concentration increases presence of low Tconset phase. The imaginary component, χ”, shows a decrease in the intergranular coupling peak, Tp, towards lower temperature as the Sm concentration increases. Samarium did not enhance the Tc(R=0) but gradually decreases its value from 102. K to 52 K for x=0.00 to x=0.20 respectively. Malaysian Solid State Science and Technology Society 2003 Article PeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/42206/1/The%20influence%20of%20samarium%20doping%20in%20Bi1.6%20%28Pb0.4%29Sr2-%20xSmxCa2Cu3Oy%20prepared%20by%20coprecipitation%20method.pdf Hamadneh, Imad (Moh'd Khair) Rashid and Shaari, Abdul Halim and Lee, C. K. and Daud, W. M. and Hassan, Z. A. (2003) The influence of samarium doping in Bi1.6 (Pb0.4)Sr2- xSmxCa2Cu3Oy prepared by coprecipitation method. Solid State Science and Technology, 11 (1). pp. 139-146. ISSN 0128-7389 http://masshp.net/journal/all%20journal/VOLUME%2011%20NO.%201,%202003/htm/Vol.%2011,%20No%201%20%282003%29%20139-146.htm
spellingShingle Hamadneh, Imad (Moh'd Khair) Rashid
Shaari, Abdul Halim
Lee, C. K.
Daud, W. M.
Hassan, Z. A.
The influence of samarium doping in Bi1.6 (Pb0.4)Sr2- xSmxCa2Cu3Oy prepared by coprecipitation method
title The influence of samarium doping in Bi1.6 (Pb0.4)Sr2- xSmxCa2Cu3Oy prepared by coprecipitation method
title_full The influence of samarium doping in Bi1.6 (Pb0.4)Sr2- xSmxCa2Cu3Oy prepared by coprecipitation method
title_fullStr The influence of samarium doping in Bi1.6 (Pb0.4)Sr2- xSmxCa2Cu3Oy prepared by coprecipitation method
title_full_unstemmed The influence of samarium doping in Bi1.6 (Pb0.4)Sr2- xSmxCa2Cu3Oy prepared by coprecipitation method
title_short The influence of samarium doping in Bi1.6 (Pb0.4)Sr2- xSmxCa2Cu3Oy prepared by coprecipitation method
title_sort influence of samarium doping in bi1.6 (pb0.4)sr2- xsmxca2cu3oy prepared by coprecipitation method
url http://psasir.upm.edu.my/id/eprint/42206/
http://psasir.upm.edu.my/id/eprint/42206/
http://psasir.upm.edu.my/id/eprint/42206/1/The%20influence%20of%20samarium%20doping%20in%20Bi1.6%20%28Pb0.4%29Sr2-%20xSmxCa2Cu3Oy%20prepared%20by%20coprecipitation%20method.pdf