Optimization of headspace sampling using solid-phase microextraction (SPME) for volatile components in starfruit juice
Volatiles are important flavor compounds of fruit juices and beverages. In this study, a headspace Solid-phase microextraction (SPME) gas chromatography-mass spectrometry (GC-MS) was used to analyze volatile components in starfruit juices. Several experimental parameters (e.g. adsorption temperatu...
| Main Authors: | , , |
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| Format: | Conference or Workshop Item |
| Language: | English |
| Published: |
Federation of Engineering Institutions of Islamic Countries
2006
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| Online Access: | http://psasir.upm.edu.my/id/eprint/39613/ http://psasir.upm.edu.my/id/eprint/39613/1/39613.pdf |
| _version_ | 1848849191354236928 |
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| author | Abdullah, Abdul Ghani Liew Sulaiman, Nasri Aruora, M. K. |
| author_facet | Abdullah, Abdul Ghani Liew Sulaiman, Nasri Aruora, M. K. |
| author_sort | Abdullah, Abdul Ghani Liew |
| building | UPM Institutional Repository |
| collection | Online Access |
| description | Volatiles are important flavor compounds of fruit juices and beverages. In this study, a headspace Solid-phase
microextraction (SPME) gas chromatography-mass spectrometry (GC-MS) was used to analyze volatile
components in starfruit juices. Several experimental parameters (e.g. adsorption temperature, adsorption time
and sample volume) were optimized to improve sampling efficiency in two aspects; maximum adsorption and
selective adsorption of volatile components onto SPME fiber. The following conditions was found to be optimal
for selectivity and sensitivity: adsorption temperature of 50oC for 30 min with a 65 μm divinylbenzene
/polydimethylsiloxane (DVB/PDMS) coated fiber with and sample volume of 15 g in a 30 ml vial. The proposed
technique could be applied for the analysis volatile compounds that contribute to starfruit juices flavor in
different cultivars and also their ripening stages. |
| first_indexed | 2025-11-15T09:46:28Z |
| format | Conference or Workshop Item |
| id | upm-39613 |
| institution | Universiti Putra Malaysia |
| institution_category | Local University |
| language | English |
| last_indexed | 2025-11-15T09:46:28Z |
| publishDate | 2006 |
| publisher | Federation of Engineering Institutions of Islamic Countries |
| recordtype | eprints |
| repository_type | Digital Repository |
| spelling | upm-396132015-08-20T07:03:33Z http://psasir.upm.edu.my/id/eprint/39613/ Optimization of headspace sampling using solid-phase microextraction (SPME) for volatile components in starfruit juice Abdullah, Abdul Ghani Liew Sulaiman, Nasri Aruora, M. K. Volatiles are important flavor compounds of fruit juices and beverages. In this study, a headspace Solid-phase microextraction (SPME) gas chromatography-mass spectrometry (GC-MS) was used to analyze volatile components in starfruit juices. Several experimental parameters (e.g. adsorption temperature, adsorption time and sample volume) were optimized to improve sampling efficiency in two aspects; maximum adsorption and selective adsorption of volatile components onto SPME fiber. The following conditions was found to be optimal for selectivity and sensitivity: adsorption temperature of 50oC for 30 min with a 65 μm divinylbenzene /polydimethylsiloxane (DVB/PDMS) coated fiber with and sample volume of 15 g in a 30 ml vial. The proposed technique could be applied for the analysis volatile compounds that contribute to starfruit juices flavor in different cultivars and also their ripening stages. Federation of Engineering Institutions of Islamic Countries 2006 Conference or Workshop Item NonPeerReviewed application/pdf en http://psasir.upm.edu.my/id/eprint/39613/1/39613.pdf Abdullah, Abdul Ghani Liew and Sulaiman, Nasri and Aruora, M. K. (2006) Optimization of headspace sampling using solid-phase microextraction (SPME) for volatile components in starfruit juice. In: Seminar on Engineering and Technology (SET2006) , 4-5 Sept. 2006, Putrajaya, Malaysia. (pp. 249-255). |
| spellingShingle | Abdullah, Abdul Ghani Liew Sulaiman, Nasri Aruora, M. K. Optimization of headspace sampling using solid-phase microextraction (SPME) for volatile components in starfruit juice |
| title | Optimization of headspace sampling using solid-phase microextraction (SPME) for volatile components in starfruit juice |
| title_full | Optimization of headspace sampling using solid-phase microextraction (SPME) for volatile components in starfruit juice |
| title_fullStr | Optimization of headspace sampling using solid-phase microextraction (SPME) for volatile components in starfruit juice |
| title_full_unstemmed | Optimization of headspace sampling using solid-phase microextraction (SPME) for volatile components in starfruit juice |
| title_short | Optimization of headspace sampling using solid-phase microextraction (SPME) for volatile components in starfruit juice |
| title_sort | optimization of headspace sampling using solid-phase microextraction (spme) for volatile components in starfruit juice |
| url | http://psasir.upm.edu.my/id/eprint/39613/ http://psasir.upm.edu.my/id/eprint/39613/1/39613.pdf |